Abstract: A method of separating certain components of a gas mixture in which the gas mixture is cooled and certain components are separated in a liquid or solid state characterized by introducing the gas mixture into a separator tank, adding a cooling agent such as a liquid or cold inert gas so as to cool the gas mixture and separating component in a solid state and subsequently fusing the separated solid into a liquid in a collecting tank. The concentrated gas mixture to be separated is directly removed from its place of use and directly supplied to the separator tank without allowing any further admixture of secondary air. The device for carrying out the method comprises an insulated tank to which air having entrained sulfer dioxide is introduced. The air flow is controlled so that it is oriented in a particular direction and it is passed beyond nozzles for injecting an inert gas such as liquid nitrogen into the interior of the insulated tank.