Abstract: A method and chemical composition and material structure for improving fretting wear in substrates, particularly carbon-carbon composite (CCC). The invention relates to trilayer coatings, comprising a base of hard ZrO2, a middle layer of Al2O3, and a top layer of lubricious ZnO. The coatings of the present invention exhibit conformality and pore-filling down to approximately 100 microns into a carbon-carbon composite to which they are applied. The methods for preparing the coatings include a chemical vapor infiltration route, such as an atomic layer deposition (ALD) process, to uniformly and conformally coat the porous and open structure of CCC with a solid lubricant trilayer of ZnO/Al2O3/ZrO2 that results in significant improvement (65%) in fretting wear.

Abstract: A method and composition for producing a monolithic hybrid composite consisting of a composite matrix, a reinforcement phase, and a solid/self-lubrication phase. The composition may comprise a graphite (“C”) phase and a titanium carbide (“TiC”) phase in a nickel (“Ni”) matrix. The process may include the step of blending pure Ni and pure titanium (“Ti”) powders with Ni-coated graphite powder using Laser Engineered Net Shaping (“LENS”).

Abstract: A method and chemical composition and material structure for improving fretting wear in substrates, particularly carbon-carbon composite (CCC). The invention relates to trilayer coatings, comprising a base of hard ZrO2, a middle layer of Al2O3, and atop layer of lubricious ZnO. The coatings of the present invention exhibit conformality and pore-filling down to approximately 100 microns into a carbon-carbon composite to which they are applied. The methods for preparing the coatings include a chemical vapor infiltration route, such as an atomic layer deposition (ALD) process, to uniformly and conformally coat the porous and open structure of CCC with a solid lubricant trilayer of ZnO/Al2O3/ZrO2 that results in significant improvement (65%) in fretting wear.

Abstract: A method for refining the microstructure of titanium alloys in a single thermomechanical processing step, wherein the titanium alloy comprises boron. In some embodiments, the method comprises the steps of first adding boron to the titanium alloy then subjecting the boron-containing titanium alloy to a thermomechanical processing step. Also provided is a method for achieving superplasticity in titanium alloys comprising the steps of selecting a boron-containing titanium alloy, determining the temperature and strain rate necessary to achieve beta superplasticity, and applying sufficient temperature and strain rate to the boron-containing titanium alloy to deform the alloy to the desired shape. Also provided methods of forming titanium alloy parts and the parts prepared by these methods.

Abstract: A method for refining the microstructure of titanium alloys in a single thermomechanical processing step, wherein the titanium alloy comprises boron. In some embodiments, the method comprises the steps of first adding boron to the titanium alloy then subjecting the boron-containing titanium alloy to a thermomechanical processing step. Also provided is a method for achieving superplasticity in titanium alloys comprising the steps of selecting a boron-containing titanium alloy, determining the temperature and strain rate necessary to achieve beta superplasticity, and applying sufficient temperature and strain rate to the boron-containing titanium alloy to deform the alloy to the desired shape. Also provided methods of forming titanium alloy parts and the parts prepared by these methods.

Abstract: A method for refining the microstructure of titanium alloys in a single thermomechanical processing step, wherein the titanium alloy comprises boron. In some embodiments, the method comprises the steps of first adding boron to the titanium alloy then subjecting the boron-containing titanium alloy to a thermomechanical processing step. Also provided is a method for achieving superplasticity in titanium alloys comprising the steps of selecting a boron-containing titanium alloy, determining the temperature and strain rate necessary to achieve beta superplasticity, and applying sufficient temperature and strain rate to the boron-containing titanium alloy to deform the alloy to the desired shape. Also provided methods of forming titanium alloy parts and the parts prepared by these methods.