Patents by Inventor Je Kyun Lee

Je Kyun Lee has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11485892
    Abstract: Provided is a method for producing a silica aerogel blanket having high thermal insulation and high strength, wherein an acicular metal-silica composite is added to a step of preparing a silica precursor solution during the production of the silica aerogel blanket to produce a silica aerogel blanket having characteristics of high thermal insulation, high strength, high thermal resistance and low dust.
    Type: Grant
    Filed: August 29, 2018
    Date of Patent: November 1, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Tae Gyeong Kang, Je Kyun Lee, Kyoung Shil Oh, Hyun Woo Jeon
  • Patent number: 11478770
    Abstract: Provided are a method of preparing a metal oxide-silica composite aerogel, and a metal oxide-silica composite aerogel having an excellent weight reduction property prepared by the method. The method includes a step of adding an acid catalyst to a first water glass solution to prepare an acidic water glass solution (step 1); a step of adding a metal ion solution to the acidic water glass solution to prepare a precursor solution (step 2); and a step of adding a second water glass solution to the precursor solution and performing a gelation reaction (step 3) to yield a metal oxide-silica composite wet gel, wherein, in steps 2 and 3, bubbling of an inert gas is performed during the adding of the metal ion solution or the second water glass solution, respectively.
    Type: Grant
    Filed: September 7, 2018
    Date of Patent: October 25, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Jong Hun Kim, Je Kyun Lee
  • Patent number: 11452979
    Abstract: A method for producing a plate type metal-silica composite aerogel and a plate type metal-silica composite aerogel produced thereby in which the metal salt concentration and the basic catalyst concentration are adjusted to form a plate type intermediate first, and then an appropriate amount of a water glass solution is added, thereby enabling the plate type metal-silica composite aerogel to be produced in a short time under conditions of low temperature and atmospheric pressure, so that the process is simpler than the conventional production method, and the cost is reduced, which is excellent in economy. Also provided is a plate type metal-silica composite aerogel, which is produced by the claimed method and has excellent dispersibility that requires no additional surface modifier.
    Type: Grant
    Filed: October 10, 2017
    Date of Patent: September 27, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Tae Gyeong Kang, Je Kyun Lee, Jong Hun Kim
  • Patent number: 11377360
    Abstract: A method of preparing acicular metal-silica composite aerogel particles by adjusting an aspect ratio of the acicular shape through the adjustment of concentrations of an acidic solution, a solution including a metal salt, and a water glass solution which are reactants, and acicular metal-silica composite aerogel particles prepared thereby. The method prepares acicular metal-silica composite aerogel particles in a short period of time under mild conditions of low temperature and atmospheric pressure, the process is simple, and production costs are reduced in comparison to a conventional preparation method, and thus, productivity and economic efficiency are excellent. When the acicular metal-silica composite aerogel particles are used as an additive of a polymer resin, physical properties, such as viscosity and thixotropy, are improved.
    Type: Grant
    Filed: November 1, 2017
    Date of Patent: July 5, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Hyun Woo Jeon, Je Kyun Lee
  • Publication number: 20220144652
    Abstract: Provided is a method of preparing a metal oxide-silica composite aerogel and a metal oxide-silica composite aerogel having an excellent weight reduction property prepared by the method. The method comprises adding an acid catalyst to a first water glass solution to prepare an acidic water glass solution (step 1); adding a metal ion solution to the acidic water glass solution to prepare a precursor solution (step 2); and adding a second water glass solution to the precursor solution and performing a gelation reaction (step 3).
    Type: Application
    Filed: January 26, 2022
    Publication date: May 12, 2022
    Inventors: Jong Hun KIM, Je Kyun LEE
  • Patent number: 11312103
    Abstract: Provided is a composite thermal insulation sheet including an aerogel and a method for manufacturing the same. The methods yield an ultra-thin aerogel composite sheet having characteristics of low dust, high strength and high thermal insulation, thereby having an increased applicability thereof to an electronic device.
    Type: Grant
    Filed: August 21, 2018
    Date of Patent: April 26, 2022
    Assignees: LG Chem, Ltd., LG Electronics Inc.
    Inventors: Kyoung Shil Oh, Je Kyun Lee, Byoung Wook Han, Yong Seog Jeon, Sang Woo Park, Joong Nyon Kim
  • Patent number: 11279622
    Abstract: The present invention relates to a method for producing a silica aerogel and a silica aerogel produced thereby. The present invention provides a two-step process of a nucleation step of forming silica colloid particles by using a low-concentration silica precursor and a growth step of further adding a relatively high-concentration silica precursor to form a silica wet gel by using the silica colloid particles as a seed. Thus, the present invention provides a method for producing a silica aerogel of which mechanical stability is improved to enhance pore characteristics, and physical properties are readily controllable, and also provides a silica aerogel produced thereby.
    Type: Grant
    Filed: September 12, 2017
    Date of Patent: March 22, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Young Hun Kim, Je Kyun Lee
  • Patent number: 11279625
    Abstract: Provided is a method of preparing a metal oxide-silica composite aerogel and a metal oxide-silica composite aerogel having an excellent weight reduction property prepared by the method. The method comprises adding an acid catalyst to a first water glass solution to prepare an acidic water glass solution (step 1); adding a metal ion solution to the acidic water glass solution to prepare a precursor solution (step 2); and adding a second water glass solution to the precursor solution and performing a gelation reaction (step 3).
    Type: Grant
    Filed: September 7, 2018
    Date of Patent: March 22, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Jong Hun Kim, Je Kyun Lee
  • Patent number: 11274044
    Abstract: The present invention relates to a method for producing an aerogel blanket exhibiting excellent hydrophobicity at high temperatures and an aerogel blanket produced thereby. The present invention uses a mixture of silica sol and a hydrophobic aerogel powder as an aerogel precursor and thus can achieve hydrophobicity in the internal structure as well as on the surface of the aerogel included in the aerogel blanket. Accordingly, the aerogel blanket can attain high hydrophobicity and thus can exhibit excellent hydrophobicity retention ability even in high-temperature applications.
    Type: Grant
    Filed: March 8, 2017
    Date of Patent: March 15, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Mi Ri Kim, Kyoung Shil Oh, Je Kyun Lee, Young Hun Kim
  • Patent number: 11242255
    Abstract: Disclosed herein is a method of preparing a silica aerogel. The silica aerogel is prepared by adding a first water glass solution and an acid catalyst to a reactor to form a first silica wet gel. The method further includes adding a second water glass solution and an acid catalyst to the first silica wet gel. The method further includes adding a surface modifier solution to the first silica wet gel to form a second silica wet gel. The method further includes drying a silica wet gel including the first silica wet gel and the second silica wet gel. The prepared silica aerogel has a tap density of 0.032 to 0.070 g/mL and a carbon content of 11.2 to 12.1 wt %.
    Type: Grant
    Filed: February 19, 2020
    Date of Patent: February 8, 2022
    Assignee: LG CHEM, LTD.
    Inventors: Young Hun Kim, Je Kyun Lee
  • Patent number: 11220434
    Abstract: The present invention relates to a method of preparing ultra-pure silicon carbide in which a super-porous spherical silica aerogel is used as a silica raw material. By preparing the silica aerogel particles using low-cost water glass, a reaction area with respect to a carbon raw material is increased to enable low-temperature synthesis of silicon carbide, the size and shape of silicon carbide powder may be uniformly controlled to prepare ultra-pure silicon carbide, and economic efficiency and productivity of the silicon carbide synthesis may be improved. Thus, it is expected that the silicon carbide powder prepared by the preparation method of the present invention may be provided as an optimized raw material for the preparation of silicon carbide sintered body and single crystal (ingot).
    Type: Grant
    Filed: October 24, 2017
    Date of Patent: January 11, 2022
    Assignees: LG Chem, Ltd., Inha University Research And Business Foundation
    Inventors: Young Hun Kim, Je Kyun Lee, Hae Jin Hwang, Kyoung Jin Lee
  • Patent number: 11142463
    Abstract: The present invention relates to a method for producing a silica aerogel blanket, the method comprising recovering a supercritical waste liquid generated after performing a step of supercritical drying, neutralizing the recovered supercritical waste liquid by adding an acid thereto for recycling, and reusing the recycled supercritical waste liquid, and a silica aerogel blanket produced thereby.
    Type: Grant
    Filed: March 22, 2018
    Date of Patent: October 12, 2021
    Assignee: LG Chem, Ltd.
    Inventors: Mi Ri Kim, Je Kyun Lee, Kyoung Shil Oh
  • Publication number: 20210292176
    Abstract: A method of preparing acicular metal-silica composite aerogel particles by adjusting an aspect ratio of the acicular shape through the adjustment of concentrations of an acidic solution, a solution including a metal salt, and a water glass solution which are reactants, and acicular metal-silica composite aerogel particles prepared thereby. The method prepares acicular metal-silica composite aerogel particles in a short period of time under mild conditions of low temperature and atmospheric pressure, the process is simple, and production costs are reduced in comparison to a conventional preparation method, and thus, productivity and economic efficiency are excellent. When the acicular metal-silica composite aerogel particles are used as an additive of a polymer resin, physical properties, such as viscosity and thixotropy, are improved.
    Type: Application
    Filed: November 1, 2017
    Publication date: September 23, 2021
    Inventors: Hyun Woo JEON, Je Kyun LEE
  • Patent number: 11084728
    Abstract: The present invention relates to a method for producing a silica aerogel blanket, the method comprising recovering a supercritical waste liquid generated after performing a step of supercritical drying, neutralizing the recovered supercritical waste liquid by adding an acid thereto for recycling, and reusing the recycled supercritical waste liquid, and a silica aerogel blanket produced thereby.
    Type: Grant
    Filed: March 22, 2018
    Date of Patent: August 10, 2021
    Assignee: LG Chem, Ltd.
    Inventors: Mi Ri Kim, Je Kyun Lee, Kyoung Shil Oh
  • Patent number: 11078084
    Abstract: The present disclosure provides an aerogel precursor including an alkoxydisiloxane-based prepolymer and having a functional group derived from a hydrophobic sol-gel forming agent of the following Chemical Formula 1 on a surface thereof, and therefore, capable of enhancing high temperature thermal stability of an aerogel providing hydrophobic pores having uniform pore size distribution when preparing an aerogel, and an aerogel prepared using the same: (in Chemical Formula 1, M, R, R1 to R4 are the same as defined in the specification.
    Type: Grant
    Filed: December 15, 2016
    Date of Patent: August 3, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Hee Jung Choi, Kyoung Shil Oh, Yeong Rae Chang, Je Kyun Lee
  • Patent number: 11059262
    Abstract: The present invention relates to a method of preparing an aerogel blanket in which, a surface of a base material for a blanket is activated and roughness and porosity of the surface of the base material for a blanket are increased to increase adhesion performance of a silica aerogel by inducing etching of a surface of a base material for a blanket using an acidic solution, and mechanical flexibility is increased and the generation of dust is minimized by further performing a gel deformation process of introducing cracks into the aerogel, and a low-dust and high-insulation aerogel blanket prepared according to the present invention.
    Type: Grant
    Filed: February 3, 2017
    Date of Patent: July 13, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Kyoung Shil Oh, Je Kyun Lee, Dong Sik Bae, Jeong Hun Son
  • Patent number: 11014825
    Abstract: The present invention relates to a method for producing potassium titanate, and the present invention provides a method for producing potassium titanate which uses anatase-phased titanium dioxide to simplify the process by a hydrothermal method, and thus may improve economical efficiency and productivity, and in which the reaction temperature, the reaction time and the molar ratio of a precursor may be controlled to produce a high-purity potassium titanate whisker having a nano size of an uniform shape.
    Type: Grant
    Filed: October 25, 2017
    Date of Patent: May 25, 2021
    Assignees: LG CHEM, LTD., CHANGWON NATIONAL UNIVERSITY INDUSTRY ACADEMY COOPERATIONS CORPS
    Inventors: Jong Hun Kim, Je Kyun Lee, Dong Sik Bae, Yeon Bin Choi
  • Publication number: 20210147243
    Abstract: The present invention relates to a method for manufacturing an aerogel sheet. The method for manufacturing an aerogel sheet includes: a step (a) of preparing silica sol; a step (b) of preparing a gelling catalyst; a step (c) of injecting the silica sol, which is prepared in the step (a), to a surface of a blanket to impregnate the silica sol; and a step (d) of injecting the gelling catalyst, which is prepared in the step (b), to the surface of the blanket, into which the silica sol is impregnated, to gelate the silica sol.
    Type: Application
    Filed: October 6, 2020
    Publication date: May 20, 2021
    Inventors: Ye Hon KIM, Je Kyun LEE, Kyoung Shil OH
  • Publication number: 20210114887
    Abstract: Provided is a silica aerogel blanket capable of preventing deterioration of heat insulating performance while reducing dust generation, and method for manufacturing the same. The method manufactures a low-dust silica aerogel blanket by separately adding a silica sol to prevent an opacifying agent from being exposed to the surface of the silica aerogel blanket.
    Type: Application
    Filed: September 19, 2018
    Publication date: April 22, 2021
    Inventors: Myung Eun OH, Kyu Reon LEE, Je Kyun LEE
  • Patent number: 10941043
    Abstract: Provided are a method of preparing a metal oxide-silica composite aerogel which includes preparing a silicate solution by dissolving water glass at a concentration of 0.125 M to 3.0 M, after adding and mixing a metal salt solution having a metal ion concentration of 0.125 M to 3.0 M to the silicate solution, precipitating metal oxide-silica composite precipitates by adjusting a pH of a resulting mixture to be in a range of 3 to 9, and separating and drying the metal oxide-silica composite precipitates, wherein the metal salt solution includes a magnesium (Mg)-containing metal salt in an amount such that an amount of magnesium ions is greater than 50 mol % based on a total mole of metal ions in the metal salt solution, and a metal oxide-silica composite aerogel having low tap density and high specific surface area prepared by the method.
    Type: Grant
    Filed: June 1, 2016
    Date of Patent: March 9, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Jong Hun Kim, Je Kyun Lee