Abstract: The present invention relates to the technical field of nano-materials, and specifically provides a method for preparing multiphase heterojunction nanomaterials. The method comprises the following steps: providing a substrate loaded with a NiMoO4 precursor; dissolving a selenium powder in hydrazine hydrate, adding water or sodium molybdate aqueous solution, then adding the substrate loaded with a NiMoO4 precursor, and reacting at 180-200° C.; and after the reaction, obtaining the multiphase heterojunction nanomaterials. The present invention also provides a tetraphase heterojunction nanomaterial 1T/2H-MoSe2—H/R—NiSe, and a triphase heterojunction nanomaterial 1T/2H-MoSe2—H—NiSe prepared by the method, and use thereof as an electrocatalyst to catalyze a hydrogen evolution reaction under an alkaline condition.

Abstract: The invention discloses a method for preparing a Fe-doped MoS2 nano-material, which comprises the following steps: dissolving a ferric salt and ammonium tetrathiomolybdate in DMF and reacting at 180-200° C. for 6-24 hrs to obtain a Fe-doped MoS2 nano-material. The present invention also provides a Fe-doped MoS2 nano-material supported by nickel foam, which includes a nickel foam substrate and the Fe-doped MoS2 nano-material loaded on the nickel foam substrate. Furthermore, the present invention also provides a preparation method and use of the above materials. In the invention, the desired product can be obtained by a one-pot solvothermal reaction, and thus the operation is simple. There is no need to introduce a surfactant for morphological control during the preparation process, and the resulting product has a clean surface and is easy to wash.

Abstract: The invention discloses a method for preparing a Fe-doped MoS2 nano-material, which comprises the following steps: dissolving a ferric salt and ammonium tetrathiomolybdate in DMF and reacting at 180-200° C. for 6-24 hrs to obtain a Fe-doped MoS2 nano-material. The present invention also provides a Fe-doped MoS2 nano-material supported by nickel foam, which includes a nickel foam substrate and the Fe-doped MoS2 nano-material loaded on the nickel foam substrate. Furthermore, the present invention also provides a preparation method and use of the above materials. In the invention, the desired product can be obtained by a one-pot solvothermal reaction, and thus the operation is simple. There is no need to introduce a surfactant for morphological control during the preparation process, and the resulting product has a clean surface and is easy to wash.