Abstract: A device for preparing ultra-high purity zinc based on intelligently-controlled zone melting, including a slide platform connected with a screw through a servo control system to control movement of a heating-cooling device. A quartz tube is provided inside an induction heater to protect a melting zone. An infrared thermometer is connected to the heater, and configured to monitor temperature within the melting zone, and control power of the heater. A ring magnetic stirrer with non-contact circumferential rotation cooperates with coil to stir zinc melt. A water-cooling copper jacket is connected to two ends of the heater to cool a zinc bar, and its water inlet and outlet are connected with a water chiller. The infrared thermometer monitors temperature of the zinc bar and controls water flow of the cooling system. A lifting device is connected with a base cabinet to change inclined angle of the zinc bar.

Abstract: A high-thermal conductivity composite material is AlNp/ZA27 composite material, including 2%, 4%, 6%, or 8% by volume of aluminum nitride (AlN) ceramic particles and zinc-aluminium-27 (ZA27) alloy. The ZA27 alloy includes 70.52-71.08% by weight of Zn, 25.58˜27.65% by weight of Al, 1.27˜3.45% by weight of Cu, and 0.50% or less by weight of Mg. In the preparation of the high-thermal conductivity composite material, an as-cast AlNp/ZA27 composite material is subjected to homogenizing annealing and reciprocating extrusion.

Abstract: An alkali metal ion modified titanium silicalite zeolite for gas phase epoxidation of propylene and hydrogen peroxide and a preparation method thereof. The method includes, at first step: preparing an alkali metal hydroxide modification solution; at second step: conducting controlled hydrothermal treatment on a TS-1 zeolite matrix by using an alkali metal hydroxide solution; and at third step: conducting post-treatment on the hydrothermally modified TS-1 zeolite, including solid-liquid separation, washing, drying and calcining. In the washing process, the modified TS-1 zeolite wet material is washed with a low concentration alkali metal hydroxide solution; alkali metal ions are reserved on the silicon hydroxyl of the modified titanium silicalite zeolite; and an infrared characteristic absorption band of a framework titanium active center modified by the alkali metal ions is in a range above 960 cm?1 and below 980 cm?1.

Abstract: An alkali metal ion modified titanium silicalite zeolite for gas phase epoxidation of propylene and hydrogen peroxide and a preparation method thereof. The method includes, at first step: preparing an alkali metal hydroxide modification solution; at second step: conducting controlled hydrothermal treatment on a TS-1 zeolite matrix by using an alkali metal hydroxide solution; and at third step: conducting post-treatment on the hydrothermally modified TS-1 zeolite, including solid-liquid separation, washing, drying and calcining. In the washing process, the modified TS-1 zeolite wet material is washed with a low concentration alkali metal hydroxide solution; alkali metal ions are reserved on the silicon hydroxyl of the modified titanium silicalite zeolite; and an infrared characteristic absorption band of a framework titanium active center modified by the alkali metal ions is in a range above 960 cm?1 and below 980 cm?1.

Abstract: An alkali metal ion modified titanium silicalite zeolite for gas phase epoxidation of propylene and hydrogen peroxide and a preparation method thereof. The method includes, at first step: preparing an alkali metal hydroxide modification solution; at second step: conducting controlled hydrothermal treatment on a TS-1 zeolite matrix by using an alkali metal hydroxide solution; and at third step: conducting post-treatment on the hydrothermally modified TS-1 zeolite, including solid-liquid separation, washing, drying and calcining. In the washing process, the modified TS-1 zeolite wet material is washed with a low concentration alkali metal hydroxide solution; alkali metal ions are reserved on the silicon hydroxyl of the modified titanium silicalite zeolite; and an infrared characteristic absorption band of a framework titanium active center modified by the alkali metal ions is in a range above 960 cm?1 and below 980 cm?1.

Abstract: A method for removing SOx from a gas by using a polyol composite solution is provided. The polyol composite solution is made by mixing a polyol with an organic acid and/or organic acid salt, the polyol composite solution is brought into contact with the gas containing SOx to absorb the SOx in the gas, wherein x=2 and/or 3, and the polyol refers to an organic compound other than ethylene glycol and polyethylene glycol, which contains simultaneously two or more than two hydroxyl groups in a same organic molecule.

Abstract: A method for removing SOx from a gas by using a compound alcohol-amine solution is provided. The compound alcohol-amine solution is made by mixing ethylene glycol and/or polyethylene glycol with hydroxyl and/or carboxyl organic compound having basic group containing nitrogen. The compound alcohol-amine solution is contacted with the gas containing SOx to absorb the SOx in the gas, wherein x=2 and/or 3. The compound alcohol-amine solution with absorbed SOx is regenerated by one or more of heating method, vacuum method, gas stripping method, ultrasonic method, microwave method, and radiation method to release by-products of sulfur dioxide and sulfur trioxide, and the regenerated compound alcohol-amine solution is recycled for use. This method can be used for removing SOx from flue gas, burning gas, coke-oven gas, synthesis waste gas from dyestuff plants, sewage gas from chemical fiber plants, and other industrial raw material gases or waste gases containing SOx.

Abstract: A real-time double-beam in situ infrared spectrum system and a method thereof. The system comprises two identical infrared spectrometers and a double-beam infrared reactor cell, wherein the double-beam infrared reactor cell is formed by connecting a sample cell and a reference cell which are identical, the sample cell and the reference cell are at the same level and respectively correspond to a sample spectrometer and a reference spectrometer, the two infrared spectrometers are synchronously controlled by computers, to synchronously collect spectrograms of sample beams and background beams in real time, so as to obtain real information about a species on the catalyst surface changing with the reaction time, and eliminate gas molecule vibration spectrum interference in a real-time state and transmission spectrum interference generated under a heating condition.

Abstract: An ethylene glycol composite solution is used for removing SOx from a gas. The ethylene glycol composite solution is made by mixing ethylene glycol and/or polyethylene glycol with an organic acid and/or organic acid salt containing no nitrogen atom in a molecule. The ethylene glycol composite solution is brought into contact with the gas containing SOx to absorb the SOx in the gas. The ethylene glycol composite solution loaded with absorbed SOx is regenerated by heating, vacuuming, gas stripping, ultrasonic treatment, microwave treatment, or radiation treatment to release by-products of sulfur dioxide and sulfur trioxide, and the regenerated ethylene glycol composite solution is recycled for use.

Abstract: A method for removing SOx from a gas using an ethylene glycol composite solution is provided. The ethylene glycol composite solution is made by mixing ethylene glycol and/or polyethylene glycol with an organic acid and/or organic acid salt containing no nitrogen atom in a molecule, the ethylene glycol composite solution is brought into contact with the gas containing SOx to absorb the SOx in the gas, wherein x=2 and/or 3. The ethylene glycol composite solution with absorbed SOx is regenerated by one or more of a heating method, a vacuum method, a gas stripping method, an ultrasonication method, a microwave method, and a radiation method to release by-products of sulfur dioxide and sulfur trioxide, and the regenerated ethylene glycol composite solution is recycled for use. This method can be used for desulfurization of flue gas, burning gas, coke-oven gas, synthesis waste gas from dyestuff plants, sewage gas from chemical fiber plants, and other industrial raw material gases or waste gases containing SOx.

Abstract: A method for removing SOx from a gas by using a polyol composite solution is provided. The polyol composite solution is made by mixing a polyol with an organic acid and/or organic acid salt, the polyol composite solution is brought into contact with the gas containing SOx to absorb the SOx in the gas, wherein x=2 and/or 3, and the polyol refers to an organic compound other than ethylene glycol and polyethylene glycol, which contains simultaneously two or more than two hydroxyl groups in a same organic molecule.

Abstract: A method for removing SOx from a gas by using a compound alcohol-amine solution is provided. The compound alcohol-amine solution is made by mixing ethylene glycol and/or polyethylene glycol with hydroxyl and/or carboxyl organic compound having basic group containing nitrogen. The compound alcohol-amine solution is contacted with the gas containing SOx to absorb the SOx in the gas, wherein x=2 and/or 3. The compound alcohol-amine solution with absorbed SOx is regenerated by one or more of heating method, vacuum method, gas stripping method, ultrasonic method, microwave method, and radiation method to release by-products of sulfur dioxide and sulfur trioxide, and the regenerated compound alcohol-amine solution is recycled for use. This method can be used for removing SOx from flue gas, burning gas, coke-oven gas, synthesis waste gas from dyestuff plants, sewage gas from chemical fiber plants, and other industrial raw material gases or waste gases containing SOx.