Abstract: Provided is a mono-tin organic compound for the synthesis of sucrose-6-carboxylate. The compound has a structure shown in formula (1), wherein R1, R2, and R3 each are independently selected from the group consisting of C1 to C8 linear or branched saturated alkyl, C2 to C8 linear or branched unsaturated alkyl, C3 to C8 substituted or unsubstituted saturated cycloalkyl, C3 to C8 substituted or unsubstituted unsaturated cycloalkyl, and C6 to C12 aryl or substituted aryl; and R4 is selected from the group consisting of C1 to C6 linear or branched saturated alkyl and C6 to C12 aryl or substituted aryl.

Abstract: Provided are a supported catalyst and a method for synthesizing a sucrose-6-ester. The supported catalyst includes an active functional component and an inorganic carrier, wherein the active functional component is a compound shown in formula (1), wherein n is a natural number greater than or equal to 2; R is an atom linked to a surface of the inorganic carrier; and one or two of R1, R2, and R3 is/are hydrocarbyl, and the rest are independently any one selected from the group consisting of oxygen, hydroxyl, hydrocarbyloxy, and acetoxy.

Abstract: A production apparatus and a production method of sucrose-6-ester are provided. The production apparatus includes a tank, a rotary distillation device, and a condensation device, the tank includes a separation chamber and a reaction chamber; the condensation device is sheathed inside the rotary distillation device, and the rotary distillation device is slidably connected in the separation chamber; a turntable of the rotary distillation device is fixed on a top surface of a drum, and a first heating device is provided on an outer wall of the turntable; the condensation device includes a condenser pipe, a water receiving plate, and a condensate water box that are connected sequentially from top to bottom; the condensation device is sheathed inside the drum of the rotary distillation device in a non-contact manner, and the condenser pipe is arranged to penetrate through the turntable and contacts a top surface of the tank.

Abstract: Disclosed is a method for purifying sucralose, sequentially including: adding sucralose to ultrapure water, heating the resulting mixture for dissolution to obtain a dissolved solution, filtering the dissolved solution to obtain a filtrate, and then extracting the filtrate with an extraction solvent to remove non-polar impurities; subjecting the extracted recrystallization solution to concentration by evaporation to obtain a concentrated recrystallization solution with a preset concentration, and leaving the concentrated recrystallization solution to stand at a preset temperature for a preset time to produce a sucralose crystal nucleus in the concentrated recrystallization solution; subjecting the concentrated recrystallization solution containing the sucralose crystal nucleus to programmed cooling to obtain a recrystallization solution with a large amount of a sucralose crystal; and centrifuging the recrystallization solution with a large amount of a sucralose crystal to obtain a solid, and subjecting the so

Abstract: Disclosed are a device and a method for preparing a sucrose-6-ester. The device includes a tank body, a heating pipe, an annular cooling apparatus, and a motor, wherein the annular cooling device and the heating pipe are arranged in the tank body in nested manner; the annular cooling apparatus includes a condensation inner wall, a condenser pipe, and a condensation outer wall that are arranged in nested manner; a distillation chamber is formed between the heating pipe and the tank body, a condensation chamber is formed between the heating pipe and the condensation outer wall, and a hollow portion of the condensation inner wall forms a reaction chamber; the heating pipe and the condensation inner wall are drove by the motor to rotate; the heating pipe is provided with a vapor outlet; an evaporation residue channel is formed at an end of the heating pipe away from the feed inlet.

Abstract: The invention provides a DMF recycling method, the method comprises: neutralization step, extraction and crystallization step, layering step, evaporation step; a condensate obtained by evaporation of the upper layer liquid phase is recycled into the anti-solvent, a concentrated solution obtained by evaporation of the upper layer liquid phase and a condensate obtained by evaporation of the lower layer liquid phase are mixed to obtain a crude DMF solution for recycling of DMF. The recycling method overcomes the problem that acetic acid in the stock solution corrodes the equipment and produces impurities, so as to improve the recycling purity and reduce the equipment cost.

Abstract: A production apparatus of sucrose-6-ester is disclosed and includes a distillation separation tank, a reaction tank, and a condensated water collection tank, where the distillation separation tank is arranged above the reaction tank and the condensated water collection tank, and includes a shell and a heating-roller distillation device including a plurality of heating rollers arranged from top to bottom between front and rear side walls of the shell; two ends of the U-shaped plate are respectively fixed to bottoms of the front and rear side walls; a feed pipe is provided at a top of the shell, the condensated water outlet pipe is arranged at a bottom surface of the shell and is connected to the condensated water collection tank, and the liquid evaporation residue discharge pipe penetrates through the bottom surface of the shell, is connected to the U-shaped plate, and is connected to the reaction tank.

Abstract: Provided are a device and a method for producing a sucrose-6-ester. The device includes a shell, a film scraping apparatus, and a base, wherein the film scraping apparatus is arranged on the base, and the shell covers the film scraping apparatus and the base; the shell is provided with a reaction solution inlet and a condensated water outlet; the base is provided with a carboxylate feed pipe, a reaction product discharge pipe, and a reaction channel connected to the carboxylate feed pipe; the film scraping apparatus includes a temperature control unit, a rotary tube, and a plurality of scrapers arranged on an inner wall of the rotary tube, and an outer edge of each of the scrapers abuts against an outer wall of the temperature control unit; and the rotary tube is able to rotate around the temperature control unit.