Abstract: A mechanical alloying process wherein compacting of particulate feedstock is physically separate from subsequent comminuting improves control and consistency in mechanical alloying. The preferred compaction is by squeezing between rollers or other compacting means to produce a coherent mass such as a strip. The coherent mass (preferably rolled strip) is comminuted separately from the rolling or compression. This allows for a reduced temperature in comminuting or an atmosphere different from compacting or compressing. Compacting and comminuting are repeated to produce the desired extent of alloying and homogenization.

Abstract: Prealloyed powders, particularly of compositions which are difficult to work by conventional means, are subjected to forces such that strain energy is imparted thereto by virtue of which the prealloyed powders manifest low flow stress and a high degree of thermoplasticity.