Abstract: A method for forming a bi-layer coating on a substrate is disclosed herein. The method includes placing the substrate in a chemical vapor deposition (CVD) furnace, the substrate including a surface, applying a reactant vapor to the surface of the substrate to form a first coating, applying methyl trichlorosilane (MTS) to the substrate after applying the reactant vapor to the substrate, and heating the CVD furnace, including the substrate, to a first temperature to form a second coating.

Abstract: A method for forming an oxidation protection system on a carbon-carbon composite structure can comprise applying a boron slurry to the carbon-carbon composite structure, wherein the boron slurry comprises a boron compound, a first glass mixture, a first glass former, a first glass modifier, and a first carrier fluid, the first glass mixture including a first glass compound and a second glass compound, the first glass compound having a first viscosity-temperature profile that is at least one order of magnitude below a second viscosity-temperature profile of the second glass compound; applying a silicon slurry to the carbon-carbon composite structure, wherein the silicon slurry comprises a silicon compound, a third glass compound, a second glass former, a second glass modifier, and a second carrier fluid; and heating the carbon-carbon composite structure.

Abstract: A single stage OPF-to-carbon preform shape forming method includes positioning an oxidized PAN fiber preform with a female forming tool, positioning a vacuum bag over the oxidized PAN fiber preform, and vacuum forming the oxidized PAN fiber preform into a shaped body. The vacuum formed shaped body (while still in the shape forming fixture) may be loaded into a carbonization furnace and carbonized. The vacuum bag may be burned away in the carbonization furnace during carbonization.

Abstract: A single stage OPF-to-carbon preform shape forming method includes positioning an oxidized PAN fiber preform with a female forming tool, positioning a vacuum bag over the oxidized PAN fiber preform, and vacuum forming the oxidized PAN fiber preform into a shaped body. The vacuum formed shaped body (while still in the shape forming fixture) may be loaded into a carbonization furnace and carbonized. The vacuum bag may be burned away in the carbonization furnace during carbonization.

Abstract: A shape forming tool for pre-carbonization compression of a fibrous preform includes a female forming tool comprising a die recess, a first die half configured to be received by the die recess, a second die half configured to be received by the die recess, an expander tool coupled between the first die half and the second die half. The expander tool is configured to move the first die half laterally toward a first side of the female forming tool away from the second die half to compress the fibrous preform between the first die half and the female forming tool. The expander tool is further configured to move the second die half laterally toward a second side of the female forming tool away from the first die half to compress the fibrous preform between the second die half and the female forming tool.

Abstract: A shape forming tool for pre-carbonization compression of a fibrous preform includes a female forming tool comprising a die recess, a support structure moveable with respect to the female forming tool, and at least one bladder coupled to the support structure and configured to be received into the die recess. The support structure is configured to move the bladder(s) with respect to the female forming tool. The bladder(s) is/are configured to be inflated to apply a compressive force to compress and form a fibrous preform between the bladder(s) and the female forming tool.

Abstract: A system is provided for measuring a thickness of a preform material. The system includes a material detection device and a controller, wherein the controller is configured to: receive, from the material detection device, a signal indicating a presence of the preform material; responsive to receiving the signal, receive a first set of measurements along at least a portion of a length of the preform material; convert the first set of measurements into a second set of measurements; and record the second set of measurements.

Abstract: A method of forming a composite component is provided. The method includes locating a fibrous preform, providing a slurry, mixing the slurry with sacrificial fibers, injecting the slurry into the fibrous preform, heating the fibrous preform, forming channels in the fibrous preform, and densifying the fibrous preform. The sacrificial fibers are suspended in the fibrous preform along an injection pathway such that heating the sacrificial fibers forms the channels along the injection pathway as the sacrificial fibers are burned away.

Abstract: A method of forming a composite component is provided. The method includes locating a fibrous preform, providing a slurry, mixing the slurry with sacrificial fibers, injecting the slurry into the fibrous preform, heating the fibrous preform, forming channels in the fibrous preform, and densifying the fibrous preform. The sacrificial fibers are suspended in the fibrous preform along an injection pathway such that heating the sacrificial fibers forms the channels along the injection pathway as the sacrificial fibers are burned away.

Abstract: A single stage OPF-to-carbon preform shape forming method includes positioning an oxidized PAN fiber preform with a female forming tool, positioning a vacuum bag over the oxidized PAN fiber preform, and vacuum forming the oxidized PAN fiber preform into a shaped body. The vacuum formed shaped body (while still in the shape forming fixture) may be loaded into a carbonization furnace and carbonized. The vacuum bag may be burned away in the carbonization furnace during carbonization.

Abstract: During a manufacturing method, a preform is arranged with a plurality of grips. The preform includes a stack of a plurality of layers of material. The grips are disposed along a periphery of the stack. The preform is formed into a shaped body. The forming includes pressing a die against the stack and gripping the stack with the grips during the pressing of the die. The gripping includes asynchronously gripping the stack with at least some of the grips.

Abstract: A method for manufacturing a C/C part includes fabricating an oxidized PAN fiber preform comprising a stack of sheets of multi-axial, non-crimp, OPF fabric. The method includes positioning the oxidized PAN fiber preform with a female forming tool, the female forming tool comprising a die recess, and forming the oxidized PAN fiber preform into a shaped body. The shaped body is removed from the female forming tool and moved into a graphite fixture for carbonization. The carbonized shaped body may also be densified into the final C/C part. The carbonized shaped body can also be placed in a perforated graphite fixture for densification and removed from the perforated graphite fixture between densification processes for machining and for facilitating further densification.

Abstract: A shape forming tool for pre-carbonization compression of a fibrous preform is provided, comprising a female forming tool, a first plug, a second plug, and a wedge, each configured to be received by a die recess of the female forming tool. A first tapered surface of the wedge is configured to engage the first plug and the second tapered surface of the wedge is configured to engage the second plug. In response to the first tapered surface of the wedge engaging the first plug and the second tapered surface of the wedge engaging the second plug, the first plug and the second plug, respectively, are configured to move laterally towards opposing sides of the female forming tool and/or vertically toward a bottom side of the female forming tool to compress the fibrous preform into a shaped body.

Abstract: A carbon/carbon part and a process for making carbon/carbon parts is provided. The process involves forming steps, carbonization steps and densification steps. The forming steps may include needling fibrous layers to form fibers that extend in three directions. The carbonization steps may include applying pressure to increase the fiber volume ratio of the fibrous preform. The densification steps may include filling the voids of the fibrous preform with a carbon matrix.

Abstract: An apparatus and method for densifying porous structures inside a furnace using pressure gradient CVI/CVD. The apparatus includes a stack of porous structures where each porous structure has an aperture therethrough. The apparatus also includes at least one ring-like spacer disposed within the stack of porous structures between neighboring porous structures. The ring-like spacer encircles the apertures of the neighboring porous structures. The stack of porous structures and the at least one ring-like spacer define an enclosed cavity including each porous structure aperture. A channel provides fluid communication between the enclosed cavity and an outer volume defined by the interior surface of the furnace.

Abstract: A rotary needling process including a multitude of felting needles repeatedly driven into a fibrous structure disposed on a surface of a needle penetrable support as the support is rotated about an axis of rotation.

Abstract: The invention provides a composition of matter comprising silicon, silicon carbide and boron carbide as a coating for protecting carbon substrates from degradation at elevated temperatures. The invention also provides a method for forming a protective coating on carbon substrates by utilizing the aforesaid composition of matter.