Abstract: To measure the phase behavior of a fluid in a porous medium such as a tight gas shale, one illustrative method involves: (a) loading the fluid into a sample cell containing the porous medium; (b) setting a pressure and a temperature for the fluid in the sample cell; (c) applying an RF pulse sequence to the fluid in the sample cell to acquire an NMR signal; (d) deriving from the NMR signal an NMR parameter distribution that depends on the pressure and the temperature; (e) determining whether a fluid phase is present based on the NMR parameter distribution; (f) repeating operations (c) through (f) to determine the presence or absence of the fluid phase at multiple points along a pressure-temperature path that crosses a phase boundary; and (g) providing an estimated location of the phase boundary based on the presence or absence of the fluid phase at said points.

Abstract: To measure the phase behavior of a fluid in a porous medium such as a tight gas shale, one illustrative method involves: (a) loading the fluid into a sample cell containing the porous medium; (b) setting a pressure and a temperature for the fluid in the sample cell; (c) applying an RF pulse sequence to the fluid in the sample cell to acquire an NMR signal; (d) deriving from the NMR signal an NMR parameter distribution that depends on the pressure and the temperature; (e) determining whether a fluid phase is present based on the NMR parameter distribution; (f) repeating operations (c) through (f) to determine the presence or absence of the fluid phase at multiple points along a pressure-temperature path that crosses a phase boundary; and (g) providing an estimated location of the phase boundary based on the presence or absence of the fluid phase at said points.

Abstract: A core sample holder assembly for performing a laboratory magnetic resonance measurement of a core sample taken from a hydrocarbon containing formation is provided. The assembly comprises a pressure chamber provided by a hull and one or more flanges are sealingly coupled with the hull. A flexible core sample holder sleeve is arranged within the pressure chamber and is sealingly coupled with at least one of the flanges. An overburden fluid injection port is in fluid communication with an annular space between the hull and the flexible sleeve and is configured to inject overburden fluid into an annular space between the hull and the flexible sleeve. A pressure regulator is configured to maintain the overburden fluid in the annular space at an elevated pressure. A radio-frequency antenna, within the pressure chamber and wrapped around the sample holder sleeve, is configured to receive an electromagnetic-signal from the core sample. In use, the core sample is arranged substantially within the sleeve.

Abstract: A core sample holder assembly for performing a laboratory magnetic resonance measurement of a core sample taken from a hydrocarbon containing formation is provided. The assembly comprises a pressure chamber provided by a hull and one or more flanges are sealingly coupled with the hull. A flexible core sample holder sleeve is arranged within the pressure chamber and is sealingly coupled with at least one of the flanges. An overburden fluid injection port is in fluid communication with an annular space between the hull and the flexible sleeve and is configured to inject overburden fluid into an annular space between the hull and the flexible sleeve. A pressure regulator is configured to maintain the overburden fluid in the annular space at an elevated pressure. A radio-frequency antenna, within the pressure chamber and wrapped around the sample holder sleeve, is configured to receive an electromagnetic-signal from the core sample. In use, the core sample is arranged substantially within the sleeve.