Abstract: A process for producing a sulfamyl fluoride composition includes providing a solution comprising fluorosulfonic acid, urea and a solvent; reacting the solution at a reaction temperature from 80° C. to about 170° C. to produce a mixture including sulfamyl fluoride, bis(fluorosulfonyl) imide, ammonium fluorosulfate and the solvent; separating the ammonium fluorosulfate from the mixture; and separating the mixture into a sulfamyl fluoride composition and a recycle composition, the sulfamyl fluoride composition including a higher concentration of sulfamyl fluoride and bis(fluorosulfonyl) imide than the recycle composition. A mole ratio of the fluorosulfonic acid to the urea in the solution is from about 1.80:1 to about 2.00:1.

Abstract: A process for producing a sulfamyl fluoride composition includes providing a solution comprising fluorosulfonic acid, urea and a solvent; reacting the solution at a reaction temperature from 80° C. to about 170° C. to produce a mixture including sulfamyl fluoride, bis(fluorosulfonyl) imide, ammonium fluorosulfate and the solvent; separating the ammonium fluorosulfate from the mixture; and separating the mixture into a sulfamyl fluoride composition and a recycle composition, the sulfamyl fluoride composition including a higher concentration of sulfamyl fluoride and bis(fluorosulfonyl) imide than the recycle composition. A mole ratio of the fluorosulfonic acid to the urea in the solution is from about 1.80:1 to about 2.00:1.

Abstract: A process for producing a sulfamyl fluoride composition includes providing a solution comprising fluorosulfonic acid, urea and a solvent; reacting the solution at a reaction temperature from 80° C. to about 170° C. to produce a mixture including sulfamyl fluoride, bis(fluorosulfonyl) imide, ammonium fluorosulfate and the solvent; separating the ammonium fluorosulfate from the mixture; and separating the mixture into a sulfamyl fluoride composition and a recycle composition, the sulfamyl fluoride composition including a higher concentration of sulfamyl fluoride and bis(fluorosulfonyl) imide than the recycle composition. A mole ratio of the fluorosulfonic acid to the urea in the solution is from about 1.80:1 to about 2.00:1.

Abstract: The present disclosure provides a degreasing apparatus which may be made at least partially, or substantially, of at least one plastic material, for use with solvents having relatively low boiling points that are chemically compatible with plastic materials, such as 1233zd (1-chloro-3,3,3-trifluoro-propene, CF3CH?CHCl). Plastic degreasing apparatuses may comprise a tank comprising a side wall and a bottom wall, a partition coupled to a lower portion of the tank, dividing the tank into an immersion sump and a vaporizing sump, a heating element located within the vaporizing sump, and a condensing element positioned above the lower portion, wherein at least one of the side wall, the bottom wall, and the partition is made of a plastic material.