Abstract: An apparatus is provided for the preparation of a dilute solution of a sample of a fluid comprising a valve means communicating with a dilution means, a line to the dilution means to supply diluent thereto from a reservoir, a line in communication with the valve means to remove diluted sample from the dilution means through the valve means, a line in communication with the dilution means having a valve for connection to a supply of compressed gas thereto or for connection to atmospheric pressure flow control means to control flow of diluent from the reservoir to the dilution means, and control means for controlling operation of the valve means, the valve and the flow control means. The apparatus is useful for obtaining dilute solutions of polymer cements for subsequent composition or property determination.

Abstract: An apparatus and a method of operating the apparatus are provided for obtaining a sample of polymer cement and for determining the polymer content of the cement and a molecular weight of the polymer. The apparatus comprises a valve means in combination with a dilution means whereby dilute polymer solution is supplied to a solution viscometer means and to a gel permeation chromatographic means. Operation of the apparatus is controlled by a micro computer. The apparatus and method are useful for determining the polymer content and polymer molecular weight of, for example, polybutadiene formed in a polymerization reactor.