Patents by Inventor Julien SIALELLI

Julien SIALELLI has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11389785
    Abstract: It is provided a method for obtaining mesoporous silica particles with surface functionalisation comprising the steps of a) providing solutions of at least three precursors; wherein the pH of the mixture is adjusted to a range between 2 and 8 in a buffered system; b) Mixing the precursor solutions thereby allowing a reaction to take place at a temperature between 20 and 60° C., whereby surface functionalized mesoporous silica particles as solid reaction product are formed; c) Separating the surface functionalized mesoporous silica particles from the reaction mixture by centrifugation or filtration; d) Removing any pore structure directing agent present in the pores of the formed surface functionalized mesoporous silica particles by ultrasonication; e) followed by separation by centrifugation or filtration, washing and drying of the surface functionalized mesoporous silica particles.
    Type: Grant
    Filed: January 24, 2019
    Date of Patent: July 19, 2022
    Assignee: TECHNISCHE UNIVERSITÄT BERLIN
    Inventors: Maria Colmenares, Tomos Harris, Javier Silva Mora, Julien Sialelli
  • Publication number: 20220161240
    Abstract: A method for obtaining metal oxides supported on mesoporous silica particles includes a) providing a solution of at least one metal salt, b) providing a solution of at least one template forming agent of the general formula (I) Y3Si(CH2)n—X (I), wherein X is a complexing functional group; Y is —OH or a hydrolysable moiety selected from the group containing halogen, alkoxy, aryloxy, acyloxy, c) mixing the metal salt solution and the complex forming agent solution to obtain a metal precursor; d) adding at least one solution containing at least one pore structure directing agent to the metal precursor to obtain a metal precursor template mixture; e) adding at least one alkali silicate solution to the metal precursor template mixture at room temperature to obtain a silica-supported metal complex; and f) calcination of the silica-supported metal complex under air to obtain the supported metal oxide mesoporous silica particles.
    Type: Application
    Filed: May 7, 2020
    Publication date: May 26, 2022
    Applicant: TECHNISCHE UNIVERSITÄT BERLIN
    Inventors: Maria COLMENARES, Tomos HARRIS, Julien SIALELLI, Javier SILVA MORA, Arne THOMAS
  • Publication number: 20210031172
    Abstract: It is provided a method for obtaining mesoporous silica particles with surface functionalisation comprising the steps of a) providing solutions of at least three precursors; wherein the pH of the mixture is adjusted to a range between 2 and 8 in a buffered system; b) Mixing the precursor solutions thereby allowing a reaction to take place at a temperature between 20 and 60° C., whereby surface functionalized mesoporous silica particles as solid reaction product are formed; c) Separating the surface functionalized mesoporous silica particles from the reaction mixture by centrifugation or filtration; d) Removing any pore structure directing agent present in the pores of the formed surface functionalized mesoporous silica particles by ultrasonication; e) followed by separation by centrifugation or filtration, washing and drying of the surface functionalized mesoporous silica particles.
    Type: Application
    Filed: January 24, 2019
    Publication date: February 4, 2021
    Applicant: TECHNISCHE UNIVERSITÄT BERLIN
    Inventors: Maria COLMENARES, Tomos HARRIS, Javier SILVA MORA, Julien SIALELLI