Patents by Inventor Katsuro Kuroki
Katsuro Kuroki has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 5840131Abstract: A process for producing a grain-oriented electrical steel sheet excellent in the glass film and the magnetic properties by coating a steel sheet with an annealing separator, finish annealing the steel sheet, and baking an insulating coating agent, which comprises coating the steel sheet having been decarburization annealed with an annealing separator prepared by allowing 100 parts by weight of MgO to contain, in the course from the step of producing MgO to the stage of preparing a slurry in the step of coating the steel sheet with MgO, halogens selected from F, Cl, Br and I or compounds of the halogens in an amount of 0.015 to 0.120 part by weight in terms of F, Cl, Br and I, and finish annealing the steel sheet.Type: GrantFiled: May 17, 1997Date of Patent: November 24, 1998Assignee: Nippon Steel CorporationInventors: Kenichi Yakashiro, Hotaka Honma, Maremizu Ishibashi, Akira Sakaida, Tomoji Kumano, Koji Yamasaki, Katsuro Kuroki, Osamu Tanaka
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Patent number: 5782998Abstract: In order to provide a very low iron loss, it is necessary to render the surface of a steel sheet smooth (specular). In the present invention, this is effected in a finish annealing furnace to simultaneously attain a high magnetic flux density and a specular surface. Specifically, after the completion of decarburization annealing, a steel material is pickled to remove an oxide layer present on the surface of the steel sheet, coated with an annealing separator comprising a substance nonreactive or less reactive with SiO.sub.2 and then subjected to finish annealing to provide a grain oriented electrical steel sheet having a specular surface. Magnetic domain division and tension coating of the steel sheet can provide a low iron loss value. In the finish annealing, since no time is required for dehydration, the annealing time can be shortened.Type: GrantFiled: January 7, 1994Date of Patent: July 21, 1998Assignee: Nippon Steel CorporationInventors: Yoshiyuki Ushigami, Takeo Nagashima, Shuichi Yamazaki, Hiroyasu Fujii, Yozo Suga, Tadashi Nakayama, Katsuro Kuroki, Yosuke Kurosaki
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Process for production of grain oriented electrical steel sheet having excellent magnetic properties
Patent number: 5512110Abstract: In the present invention, grain oriented electrical steel sheets provided by heating a slab comprising, by weight percent, 0.025 to 0.075% of C, 3.4 to 5.0% of Si, 0.015 to 0.080% of sol. Al, 0.0030 to 0.013% of N, 0.014% or less of (S+0.405 Se) and 0.05 to 0.8% of Mn, sol. Al (%)/Si (%) being 0.0080 or more, the balance consisting of Fe and unavoidable impurities at a temperature below 1280.degree. C., hot-rolling the heated slab, subjecting the hot-rolled steel sheet to cold rolling, subjecting the cold-rolled steel sheet to decarbonization annealing with regulating the average diameter of primary recrystallized grains of the steel sheet subjected to decarbonization annealing to 18 to 35 .mu.Type: GrantFiled: June 6, 1995Date of Patent: April 30, 1996Assignee: Nippon Steel CorporationInventors: Yasunari Yoshitomi, Katsuro Kuroki, Yukio Matsuo, Hiroaki Masui, Yoshio Nakamura, Maremizu Ishibashi, Tsuyoshi Kawano, Tsutomu Haratani, Yoshiyuki Ushigami -
Patent number: 5507883Abstract: A grain oriented electrical steel sheet having no significant glass film and having a high magnetic flux density and an excellent iron loss property, comprising, in terms of by weight, 2.5 to 4.5% of Si, the steel sheet having, as oxides on its surface, a glass film comprising 0.6 g/m.sup.2 or less in total of forsterite and spinel composed of MgO, SiO.sub.2 and Al.sub.2 O.sub.3 and an insulating coating having a thickness of 6 .mu.m or less, the face tension imparted on the surface of the steel sheet by the coating being in the range of from 0.5 to 2.0 kg/mm.sup.2. In the final box annealing of the steel sheet after primary recrystallization annealing, use is made of an annealing separator comprising 100 parts by weight of MgO and, added thereto, 2 to 30 parts by weight of at least one member selected from the group consisting of chlorides, carbonates, nitrates, sulfates and sulfides of Li, K, Bi, Na, Ba, Ca, Mg, Zn, Fe, Zr, Sr, Sn, Al, etc.Type: GrantFiled: June 9, 1994Date of Patent: April 16, 1996Assignee: Nippon Steel CorporationInventors: Osamu Tanaka, Hiroaki Masui, Hotaka Honma, Katsuro Kuroki, Tsutomu Haratani, Yoichi Mishima, Maremizu Ishibashi, Yoshio Nakamura
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Patent number: 5261972Abstract: The present invention discloses a process for producing a grain-oriented electrical steel strip having a high magnetic flux density. The process comprises hot-rolling a steel ingot comprising basic ingredients and, added thereto, 0.02 to 0.15% of Sn at a temperature of 1200.degree. C. or below, annealing the hot-rolled strip, cold-rolling the annealed strip with a final rolling reduction of 80% or more and subjecting the cold-rolled strip to decarburization annealing, a nitriding treatment and finish annealing, wherein the temperature, T.degree.C., of annealing of the hot-rolled strip is set so as to fall within the range 1240-2.1.times.Al.sub.R <T<1310-1.8.times.Al.sub.R (wherein Al.sub.R =acid soluble [Al]-27/14.times.[N]) and the strip is soaked for 180 sec or less, maintained at a temperature in the range of from 800.degree. to 950.degree. C. for 30 to 300 sec and then quenched.The grain-oriented electrical steel strip thus produced is not influenced by the variation in the [Al] and [N].Type: GrantFiled: October 22, 1992Date of Patent: November 16, 1993Assignee: Nippon Steel CorporationInventors: Katsuro Kuroki, Yasunari Yoshitomi, Hiroaki Masui, Tsutomu Haratani
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Patent number: 5049205Abstract: The present invention relates to a process for preparing a unidirectional silicon steel sheet having a high magnetic flux density which comprises heating a silicon steel slab comprising by weight 0.025 to 0.075% of carbon, 2.5 to 4.5% of silicon, 0.015% or less of sulfur, 0.010 to 0.050% of acid-soluble aluminum, 0.0010 to 0.012% of nitrogen, 0.050 to 0.45% of manganese and 0.01 to 0.10% of tin and optionally 0.0005 to 0.0080% of boron with the balance being iron and unavoidable impurities, at 1200.degree. C.Type: GrantFiled: September 27, 1990Date of Patent: September 17, 1991Assignee: Nippon Steel CorporationInventors: Nobuyuki Takahashi, Katsuro Kuroki, Yozo Suga, Kiyoshi Ueno
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Patent number: 4994120Abstract: Disclosed is a process for the preparation of a grain oriented electrical steel sheet having a high flux desnity, which comprises hot-rolling a slab comprising 1.5 to 4.8% by weight of Si, 0.012 to 0.050 by weight of acid-soluble Al, up to 0.012% by weight of at least one member selected from S and Se, 0.0010 to 0.0120% by weight of N, Mn in an amount of up to 0.45% by weight which satisfies the requirement of Mn/(S+Se).gtoreq.4.0 and 0.005 to 0.0080% by weight of B, with the balance comprising Fe and unavoidable impurities, and optionally, further comprising 0.0020 to 0.Type: GrantFiled: November 18, 1988Date of Patent: February 19, 1991Assignee: Nippon Steel CorporationInventors: Nobuyuki Takahashi, Yozo Suga, Katsuro Kuroki, Satoshi Arai
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Patent number: 4992114Abstract: The present invention provides a grain-oriented electrical steel sheet having a thickness of up to 0.17 mm and excellent product magnetic characteristics. The present invention is characterized in that a silicon containing acid-soluble Al, N and Sn is used as the starting material, the N and acid-soluble Al contents in the slab are adjusted to 0.0050 to 0.0100% and {(27/14).times.N (%)+0.0035} to {(27/14).times.N (%)+0.0100}%, respectively, the thickness of the hot-rolled sheet is adjusted so that the thickness reduction ratio at the one-stage cold-rolling is 85 to 92%, and the Nas AlN content in the hot-rolled steel sheet is controlled to 0.0005 to 0.0020%.Type: GrantFiled: March 16, 1989Date of Patent: February 12, 1991Assignee: Nippon Steel CorporationInventors: Shozaburo Nakashima, Katsuro Kuroki, Koji Yamasaki
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Patent number: 4979996Abstract: The present invention relates to an improvement in the technique of heating an electrical steel slab at a low temperature. A grain-oriented electrical steel sheet having excellent magnetic characteristics and film characteristics is prepared by the process characterized in that a slab comprising, as main ingredients, up to 0.012% by weight of S, 0.010 to 0.060% by weight of acid-soluble Al, up to 0.010% by weight of N, 0.08 to 0.45% by weight of Mn, and 0.015 to 0.045% by weight is used as the starting slab, and after the decarburization annealing, the nitriding treatment is carried out at a temperature of 500.degree. to 900.degree. C. in an atmosphere having an NH.sub.3 gas concentration of at least 1000 ppm, while running the strip.Type: GrantFiled: April 19, 1989Date of Patent: December 25, 1990Assignee: Nippon Steel CorporationInventors: Hisashi Kobayashi, Katsuro Kuroki, Masayoshi Minakuchi, Kenichi Yakashiro
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Patent number: 4979997Abstract: A process for producing a grain-oriented steel sheet having superior magnetic and surface film characteristics, which comprises the steps of: heating to a temperature of 1200.degree. C. or lower an electrical steel slab comprising 0.025 to 0.075 wt % C, 2.5 to 4.5 wt % Si, 0.012 wt % or less S, 0.010 to 0.060 wt % acid-soluble Al, 0.010 wt % or less N, 0.080 to 0.045 wt % Mn, and the balance consisting of Fe and unavoidable impurities; hot-rolling the heated slab to form a hot-rolled steel sheet; cold-rolling the hot-rolled sheet to a final product sheet thickness by single cold rolling step or by two or more steps of cold rolling with an intermediate annealing therebetween; decarburization-annealing the cold-rolled sheet under a condition such that decarburization alone is effected until primary-recrystallized grains grow to an average grain size of at least 15 .mu.Type: GrantFiled: May 21, 1990Date of Patent: December 25, 1990Assignee: Nippon Steel CorporationInventors: Hisashi Kobayashi, Katsuro Kuroki, Osamu Tanaka
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Patent number: 4948433Abstract: Disclosed is a process for preparing a thin grain oriented electrical steel sheet having a final thickness of 0.05 to 0.25 mm from a silicon steel slab comprising 0.050 to 0.120% by weight of C, 2.8 to 4.0% by weight of Si and 0.05 to 0.25% by weight of Sn, wherein the starting silicon slab further comprises up to 0.035% by weight of S and 0.005 to 0.035% by weight of Se, with the proviso that the total amount of S and Se is in the range of 0.015 to 0.060% by weight, 0.050 to 0.090% by weight of Mn, with the proviso that the Mn content is in the range of {1.5.times.[content (% by weight) of S+content (% by weight) of Se[} to {4.5.times.[content (% by weight) of S+content (% by weight) of Se[} % by weight, 0.0050 to 0.0100% by weight of N, and {[27/14].times.content (% by weight) of N+0.0030} to {[27/14].times.content (% by weight) of N+0.0150} % by weight of acid-soluble Al.Type: GrantFiled: November 8, 1988Date of Patent: August 14, 1990Assignee: Nippon Steel CorporationInventors: Shozaburo Nakashima, Katsuro Kuroki, Kiyoshi Ueno
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Patent number: 4938807Abstract: Disclosed is a process for the preparation of a grain oriented silicon steel about sheet having a high flux density, which comprises hot-rolling a slab comprising 1.5 to 4.8% by weight of Si, 0.012 to 0.050% by weight of Al, 0.0010 to 0.0120% by weight of N, 0.0020 to 0.0150% by weight of Ti, up to 0.45% by weight of Mn and up to 0.012% by weight of at least one member selected S and Se, which satisfies the requirement 0.06 to 0.6 of Ti/N (at % ratio) and Mn/(S+Se).gtoreq.4.0 (weight ratio) with the balance comprising Fe and unavoidable impurities, to cold-rolling, performing decarburization annealing, coating an annealing separator on the steel sheet surface, then performing finish annealing, and performing a nitriding treatment of the steel sheet during the period of from the point of termination of final cold rolling to the point of initiation of secondary recrystallization at the finish annealing step.Type: GrantFiled: January 25, 1989Date of Patent: July 3, 1990Assignee: Nippon Steel CorporationInventors: Nobuyuki Takahashi, Yozo Suga, Katsuro Kuroki
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Patent number: 4863532Abstract: In a grain-oriented electromagnetic steel sheet which is produced by a process including a cold-rolling step(s), the final reduction ratio of the cold-rolling step(s) being high, a technical means for refining the secondary recrystallized grains is particularly important. One technical means is the incorporation of tin into silicon steel material. This, however, involves a problem because tin incorporated into silicon steel material deteriorates the surface coating which imparts tension to a grain-oriented electromagnetic steel sheet.The incorporation of copper into silicon steel material has been avoided since it causes secondary recrystallization to be unstable.The present invention is characterized by the combined incorporation of tin and copper into molten steel so as to simultaneously refine the secondary recrystallized grains and to form a good surface coating. The grain-oriented electromagnetic steel sheet of the present invention contains from 2.5% to less than 4.0% of silicon, from 0.03% to 0.Type: GrantFiled: April 8, 1988Date of Patent: September 5, 1989Assignee: Nippon Steel CorporationInventors: Katsuro Kuroki, Toshiya Wada, Shozaburo Nakashima
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Patent number: 4806176Abstract: The present invention relates to an improvement in the precipitation annealing of a hot-rolled steel sheet or strip which is carried out immediately before cold-rolling in the production of a grain-oriented electromagnetic steel sheet or strip. Conventionally, precipitation annealing is carried out by heating a steel strip to a temperature of from 750.degree. to 1200.degree. C. and then quenching it. The present invention proposes to control the cooling rate during primary cooling, i.e. from a holding temperature (T.sub.1 temperature) of from 1080.degree. to 1200.degree. C. down to an intermediate temperature (T.sub.2 temperature) of from 900.degree. to 980.degree. C., and to control the staying time during primary cooling so that excellent magnetic properties can be obtained regardless of the unavoidable variation in the Al and Si content. The present invention also proposes to control the rate of temperature elevation between 800.degree. C.Type: GrantFiled: May 25, 1982Date of Patent: February 21, 1989Assignee: Nippon Steel CorporationInventors: Jiro Harase, Katsuro Kuroki, Toshiya Wada, Shozaburo Nakashima
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Patent number: 4753692Abstract: In a grain-oriented electromagnetic steel sheet which is produced by a process including a cold-rolling step(s), the final reduction ratio of the cold-rolling step(s) being high, a technical means for refining the secondary recrystallized grains is particularly important. One technical means is the incorporation of tin into silicon steel material. This, however, involves a problem because tin incorporated into silicon steel material deteriorates the surface coating which imparts tension to a grain-oriented electromagnetic steel sheet.The incorporation of copper into silicon steel material has been avoided since it causes secondary recrystallization to be unstable.The present invention is characterized by the combined incorporation of tin and copper into molten steel so as to simultaneously refine the secondary recrystallized grains and to form a good surface coating. The grain-oriented electromagnetic steel sheet of the present invention contains from 2.5% to less than 4.0% of silicon, from 0.03% to 0.Type: GrantFiled: June 17, 1986Date of Patent: June 28, 1988Assignee: Nippon Steel CorporationInventors: Katsuro Kuroki, Toshiya Wada, Shozaburo Nakashima
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Patent number: 4742706Abstract: A device for imparting strain to a steel sheet by which deformed regions spaced at a desired distance and having a minute linear shape are continuously formed, comprising: a strain imparting roll having projected portions on the surface thereof; a press roll provided opposite to the strain imparting roll; a row of a plurality of groups of back-up rolls for pressing against the press rolls, provided with spaces of a desired distance therebetween in a longitudinal direction of the press roll; and a fluid pressure cylinder connected to each group of the back-up rolls via a bearing, and a fluid supply source connected to the fluid pressure cylinder.Type: GrantFiled: April 29, 1986Date of Patent: May 10, 1988Assignees: Nippon Steel Corporation, Nittetsu Plant Designing CorporationInventors: Eiji Sasaki, Mitsuo Murata, Hisashi Kobayashi, Katsuro Kuroki, Hisao Kitsunezaki, Kengo Yoshioka, Mikio Nakamura
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Patent number: 4692193Abstract: A thin-gauge (0.10-0.23 mm thick) grain-oriented electrical steel sheet is produced by a process characterized by a decarburization which is carried out after the hot-rolling and before the final cold-rolling, after which the known, decarburization annealing and finishing annealing are carried out. The steel composition is adjusted to induce the secondary recrystallization by the AlN inhibitor. The reduction at the final cold-rolling is determined to be high to obtain a high magnetic flux density but tends to instabilize the secondary recrystallization unless the inventive decarburization is carried out.Type: GrantFiled: October 25, 1985Date of Patent: September 8, 1987Assignee: Nippon Steel CorporationInventors: Yasunari Yoshitomi, Katsuro Kuroki, Kenzo Iwayama
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Patent number: 4595426Abstract: Extremely low watt-loss of W.sub.17/50 .ltoreq.0.88 w/kg is provided by the combination of extremely low carbon, silicon and nitrogen contents; a thin sheet thickness of 0.15 to 0.23 mm; a high magnetic flux density B.sub.10 .gtoreq.1.89 T; and copresence of coarse and fine (2 mm or less) grains, the distance (ND) between the fine grains controlled to 2.0 to 8.0 mm.Type: GrantFiled: March 7, 1985Date of Patent: June 17, 1986Assignee: Nippon Steel CorporationInventors: Kenzo Iwayama, Yasunari Yoshitomi, Katsuro Kuroki
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Patent number: 4552596Abstract: In a method of producing a grain-oriented electromagnetic steel sheet, a laser beam is irradiated onto the steel sheet, which has been subjected to a final high temperature annealing in order to approximate the crystal orientation of the sheet in a (110) [001] orientation. Because of the laser beam irradiation, regions of high dislocation density are locally formed in the steel sheet and subdivide the magnetic domains, with the result that a low watt loss is achieved.Type: GrantFiled: August 17, 1982Date of Patent: November 12, 1985Assignee: Nippon Steel CorporationInventors: Tadashi Ichiyama, Shigehiro Yamaguchi, Tohru Iuchi, Katsuro Kuroki
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Patent number: 4548656Abstract: The watt loss of a grain-oriented electromagnetic steel sheet can be decreased by known methods in which serrations or scratches are locally formed on said steel sheet or a small ball or disc is rolled or rotated over said steel sheet. The known methods are disadvantageous in that the rate of production is low and in that said steel sheet has a marked unevenness.In the present invention, particles, e.g., steel shots, are projected onto substantially linear selected portions of a grain-oriented electromagnetic steel sheet, thereby producing strain on spot-formed regions. Spotlike indentations are formed in the steel sheet by the projection of steel shots onto the steel sheet.Type: GrantFiled: July 15, 1982Date of Patent: October 22, 1985Assignee: Nippon Steel CorporationInventors: Tetsuo Kimoto, Kiyoshi Orita, Katsuro Kuroki