Abstract: The present invention can provide the nonaqueous electrolytic secondary battery excellent in cycle life characteristics and characteristics in discharge at a high rate as well as in safety in overcharge without reducing the discharge capacity by using the positive active material, which is obtained from starting materials containing Na and S by a simple production step such as water-washing treatment after synthesis and which contains less than 0.1% by weight of the sulfate group (SO42−), less than 0.024% by weight of Na and/or less than 0.13% by weight of lithium sodium sulfate (LiNaSO4).

Abstract: In a method according to the present invention for manufacturing a nickel-metal-hydride battery, a positive electrode including nickel hydroxide, a negative electrode including a hydrogen occlusion alloy, and a separator are assembled, and the assembled components are placed in a battery vessel. The battery vessel is filled with an alkali electrolyte, and the vessel is sealed so as to produce a sealed nickel-metal-hydride battery. Thereafter, a formation step including at least one charging/discharging cycle of the nickel-metal-hydride battery is carried out, and after the formation step, the nickel-metal-hydride battery is charged. After the charging, the nickel-metal-hydride battery is left in a charged state for from one day until a time when there is no discharge capacity due to self-discharge.