Patents by Inventor Katsuyuki Wada

Katsuyuki Wada has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11459431
    Abstract: As a method for producing a polyacrylic acid (salt)-based water absorbent resin particle which less generates fine powder and has an excellent impact resistance and a high moisture content even in a case where the polyacrylic acid (salt)-based water absorbent resin particle is produced on a large scale, employed is a production method including the steps of: (a) adding a surface crosslinking agent solution to water absorbent resin powder to obtain a mixture; (b) reacting the mixture; and, thereafter (c) adding an aqueous liquid to at least one selected from the group consisting of (i) the water absorbent resin powder during the step (b) and (ii) the water absorbent resin powder after the step (b), an atmospheric dew point being not lower than 20° C. in the step (c), and a temperature of the water absorbent resin powder being higher than the atmospheric dew point in the step (c).
    Type: Grant
    Filed: June 17, 2020
    Date of Patent: October 4, 2022
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Hidenori Wada, Motohiro Imura, Katsuyuki Wada, Seiji Kato
  • Publication number: 20200317872
    Abstract: As a method for producing a polyacrylic acid (salt)-based water absorbent resin particle which less generates fine powder and has an excellent impact resistance and a high moisture content even in a case where the polyacrylic acid (salt)-based water absorbent resin particle is produced on a large scale, employed is a production method including the steps of: (a) adding a surface crosslinking agent solution to water absorbent resin powder to obtain a mixture; (b) reacting the mixture; and, thereafter (c) adding an aqueous liquid to at least one selected from the group consisting of (i) the water absorbent resin powder during the step (b) and (ii) the water absorbent resin powder after the step (b), an atmospheric dew point being not lower than 20° C. in the step (c), and a temperature of the water absorbent resin powder being higher than the atmospheric dew point in the step (c).
    Type: Application
    Filed: June 17, 2020
    Publication date: October 8, 2020
    Applicant: NIPPON SHOKUBAI CO., LTD.
    Inventors: Hidenori WADA, Motohiro IMURA, Katsuyuki WADA, Seiji KATO
  • Publication number: 20200023625
    Abstract: The present invention provides a water-absorbing sheet suitable for a hygienic material such as a disposable diaper. The water-absorbing sheet in accordance with an aspect of the present invention includes: a first base material; a second base material; and a particulate water-absorbing agent sandwiched between the first base material and the second base material, at least one of the first base material and the second base material being a water-permeable base material, and at least part of the particulate water-absorbing agent satisfying the following physical properties (1), (2), and (3): (1) a centrifuge retention capacity (CRC) is 30 g/g to 50 g/g; (2) a mass average particle diameter (D50) is 200 ?m to 600 ?m; and (3) a DRC index defined by the following Formula (a) is 43 or less: DRC index=(49?DRC5 min)/(D50/1000)?? Formula (a).
    Type: Application
    Filed: February 22, 2018
    Publication date: January 23, 2020
    Inventors: Kazushi TORII, Kunihiko ISHIZAKI, Kazushi HORIE, Ryuichi HIRAOKA, Takahiro KITANO, Yasuhisa NAKAJIMA, Hiroyuki IKEUCHI, Katsuyuki WADA
  • Patent number: 10525445
    Abstract: A water absorbent resin (water absorbing agent) and method for producing it are provided which improve, in a water absorbent article (in particular, a diaper) including a water absorbent resin as a water absorbing agent, the absolute absorption amount (g), liquid absorbing times (in particular, liquid absorbing times at the second instance and later), re-wet (g), and diffusion distance (%) of the water absorbent article. A particulate water absorbing agent of the present invention has a CRC, a proportion of particles with sizes of 600 ?m to 150 ?m as defined through a standard-sieve classification, an SST, and the value of the difference between an FST and the SST each within a predetermined range.
    Type: Grant
    Filed: November 30, 2018
    Date of Patent: January 7, 2020
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Manabu Ueda, Takahiro Kitano, Yoshitaka Ikeuchi, Hiroyuki Ikeuchi, Katsuyuki Wada
  • Patent number: 10363339
    Abstract: An object of the present invention is to provide (i) a water absorbent agent composition which has an excellent additional function (a deodorizing function in particular), which stably carries out the additional function even after being stored for a long term, and which is less stressful to skin when used as an absorbent article, (ii) a method for producing the water absorbent agent composition, and (iii) an absorbent core and an absorbent article. The water absorbent agent composition contains: a polycarboxylic acid (salt)-based water absorbent resin as a main component; a natural ingredient; and a temporal deterioration preventing agent. Further, a water absorbent agent composition is produced by simultaneously or separately mixing a natural ingredient and a temporal deterioration preventing agent with a water absorbent resin which is a crosslinked polymer of unsaturated monomers having carboxylic acid and/or a salt thereof.
    Type: Grant
    Filed: November 15, 2012
    Date of Patent: July 30, 2019
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Manabu Ueda, Hiroyuki Ikeuchi, Yasuhisa Nakashima, Katsuyuki Wada
  • Publication number: 20190091660
    Abstract: A water absorbent resin (water absorbing agent) and method for producing it are provided which improve, in a water absorbent article (in particular, a diaper) including a water absorbent resin as a water absorbing agent, the absolute absorption amount (g), liquid absorbing times (in particular, liquid absorbing times at the second instance and later), re-wet (g), and diffusion distance (%) of the water absorbent article. A particulate water absorbing agent of the present invention has a CRC, a proportion of particles with sizes of 600 ?m to 150 ?m as defined through a standard-sieve classification, an SST, and the value of the difference between an FST and the SST each within a predetermined range.
    Type: Application
    Filed: November 30, 2018
    Publication date: March 28, 2019
    Inventors: Manabu UEDA, Takahiro KITANO, Yoshitaka IKEUCHI, Hiroyuki IKEUCHI, Katsuyuki WADA
  • Patent number: 10196500
    Abstract: The present invention (a) provides, at low cost, a water absorbing agent (i) that has a suppressed amount of generated dust and a suppressed amount of dust that increases over time and (ii) that also has a high absorption capacity without load, a high absorption capacity under load, a high vertical diffusion absorbency under load, and a high absorbency in a short period of time, and (b) also provides a method for evaluating, in a short period of time, an amount of dust that increases over time. A particulate water absorbing agent of the present invention includes: a surface crosslinked polyacrylic acid (salt)-based water absorbent resin as a main component; a hydrophilic polymer compound; and a stabilizing agent.
    Type: Grant
    Filed: August 27, 2013
    Date of Patent: February 5, 2019
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Yasuhisa Nakashima, Katsuyuki Wada, Hiroyuki Ikeuchi, Manabu Ueda
  • Patent number: 10189009
    Abstract: A water absorbent resin (water absorbing agent) and method for producing it are provided which improve, in a water absorbent article (in particular, a diaper) including a water absorbent resin as a water absorbing agent, the absolute absorption amount (g), liquid absorbing times (in particular, liquid absorbing times at the second instance and later), re-wet (g), and diffusion distance (%) of the water absorbent article. A particulate water absorbing agent of the present invention has a CRC, a proportion of particles with sizes of 600 ?m to 150 ?m as defined through a standard-sieve classification, an SST, and the value of the difference between an FST and the SST each within a predetermined range.
    Type: Grant
    Filed: August 30, 2013
    Date of Patent: January 29, 2019
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Manabu Ueda, Takahiro Kitano, Yoshitaka Ikeuchi, Hiroyuki Ikeuchi, Katsuyuki Wada
  • Patent number: 9976001
    Abstract: Provided is a process for producing a water-absorbing resin powder which contains a given amount of water added thereto, has a low dust content, and has high material properties. When a water-absorbing resin powder which has undergone surface crosslinking is produced on an industrial scale, various problems concerning production are eliminated and a long-term stable operation is possible without causing a deterioration in the material properties of the resin. Even when the process is continued over a long period, the material properties are stabilized (decrease in standard deviation) or improved (improvement in AAP). The process for producing a water-absorbing resin comprises, in the following order, a first classification step for classifying a water-absorbing resin, a surface crosslinking step after the classification, a water addition step for adding water to the water-absorbing resin powder after or during the surface crosslinking, a second classification step, and a conveying step.
    Type: Grant
    Filed: February 10, 2011
    Date of Patent: May 22, 2018
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Sumio Okuda, Kunihiko Ishizaki, Katsuyuki Wada
  • Patent number: 9796853
    Abstract: A water-absorbent resin composition suffering exfoliation of additives from a water-absorbent resin only insignificantly and excelling in fluidity of powder after absorption of moisture and in deodorizing property and absorbent property as well is provided. The water-absorbent resin composition of this invention comprises a water-absorbent resin obtainable by polymerizing an unsaturated monomer having an acid group and/or a salt thereof; and complex oxide hydrate containing zinc and silicon, or zinc and aluminum, wherein the complex oxide hydrate contains zinc as main metal component, the mass ratio of the content of zinc and the content of silicon or aluminum is in the range of 50/50-99/1, and the absorption capacity at 60 minutes toward 0.90 mass % sodium chloride aqueous solution under the pressure of 1.9 kPa is not less than 20 g/g. Optionally, a plant component (C) can be added to the water absorbent resin composition.
    Type: Grant
    Filed: July 23, 2004
    Date of Patent: October 24, 2017
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Hiroko Ueda, Katsuyuki Wada, Yasuhisa Nakashima
  • Patent number: 9775927
    Abstract: A particulate water absorbing agent of the present invention is a water absorbing agent containing a water absorbing resin as a main component, the particulate water absorbing agent containing a polyvalent metal cation and satisfying: (1) the polyvalent metal cation is contained in an amount between 0.001 wt % and 5 wt % relative to the amount of the water absorbing agent; (2) an absorbency without pressure (CRC) is not less than 28 (g/g) and an absorbency against pressure (AAP 4.83 kPa) is not less than 10 (g/g); (3) the absorbency against pressure and the absorbency without pressure satisfy 77 ?AAP (4.83 kPa)+1.8×CRC?100; and (4) a moisture content of the water absorbing agent is between 5 wt % and 20 wt %. This provides a water absorbing agent which has blocking resistance after moisture absorption, is excellent in stability to shock and suppresses Re-Wet when used in a diaper.
    Type: Grant
    Filed: December 8, 2014
    Date of Patent: October 3, 2017
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Taishi Kobayashi, Motohiro Imura, Taku Iwamura, Katsuyuki Wada, Kozo Nogi, Yoshiro Mitsukami, Masato Abe, Hiroko Ueda, Koji Honda
  • Patent number: 9669386
    Abstract: A particulate water-absorbing agent containing a surface-crosslinked polyacrylic acid (salt)-type water-absorbing resin as a main component and at least one spacer selected from a polycation and water-insoluble fine particles. The particulate water-absorbing agent has a free swell capacity (FSC) of 55 to 65 g/g, an absorption against pressure (AAP—4.83 kPa) of 20 to 30 g/g, and a vertical diffusion absorption amount under pressure (VDAUP—4.83 kPa) of 30 to 80 g. Also disclosed is a method for producing a particulate water-absorbing agent, an absorbent core containing the particulate water-absorbing agent, and an absorbing article containing the absorbent core.
    Type: Grant
    Filed: September 30, 2011
    Date of Patent: June 6, 2017
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Katsuyuki Wada, Yasuhisa Nakashima
  • Patent number: 9308290
    Abstract: To improve the heat retention by diapers and other absorbents, a heat retention indicator 1 of a water-absorbing resin which is defined in the present invention needs be 3.0° C./min or less and also that particular requirements need be met to satisfy this condition. If the requirements are met, a water-absorbing resin, absorbent, and absorbent article can be provided which has a heat retention indicator 1 of 0 to 3.0° C./min or less and which exhibits excellent heat retention and absorption.
    Type: Grant
    Filed: September 18, 2013
    Date of Patent: April 12, 2016
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Katsuyuki Wada, Makoto Nagasawa, Kunihiko Ishizaki
  • Patent number: 9180220
    Abstract: A water absorbing agent of the present invention has an internal crosslinking structure obtained by polymerization of a water-soluble unsaturated monomer. The agent satisfies conditions (a) to (d): (a) the agent contains water-insoluble inorganic particles at an amount of from 10 ppm to 1,900 ppm inclusive; (b) the agent contains 5 mass % or less particles which have such a size that they can pass through a sieve having a mesh opening size of 150 ?m; (c) the agent has an absorbency against a pressure of 4.83 kPa (AAP) of 18 g/g or more; and (d) the water-insoluble inorganic particles reside on a surface of the water absorbing resin or near the surface.
    Type: Grant
    Filed: May 9, 2012
    Date of Patent: November 10, 2015
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Kazushi Torii, Hirofumi Shibata, Kazuki Kimura, Yasuhisa Nakashima, Motohiro Imura, Hiroko Ueda, Katsuyuki Wada
  • Publication number: 20150307667
    Abstract: As a method for producing a polyacrylic acid (salt)-based water absorbent resin particle which less generates fine powder and has an excellent impact resistance and a high moisture content even in a case where the polyacrylic acid (salt)-based water absorbent resin particle is produced on a large scale, employed is a production method including the steps of: (a) adding a surface crosslinking agent solution to water absorbent resin powder to obtain a mixture; (b) reacting the mixture; and, thereafter (c) adding an aqueous liquid to at least one selected from the group consisting of (i) the water absorbent resin powder during the step (b) and (ii) the water absorbent resin powder after the step (b), an atmospheric dew point being not lower than 20° C. in the step (c), and a temperature of the water absorbent resin powder being higher than the atmospheric dew point in the step (c).
    Type: Application
    Filed: December 3, 2013
    Publication date: October 29, 2015
    Applicant: NIPPON SHOKUBAI CO., LTD.
    Inventors: Hidenori WADA, Motohiro IMURA, Katsuyuki WADA, Seiji KATO
  • Patent number: 9138505
    Abstract: Disclosed is a method for producing a water absorbent resin, by which a surface-crosslinked water absorbent resin having excellent physical properties can be efficiently obtained at low cost, while assuring high productivity. When the production scale is increased to a continuous production on a huge scale (for example, 1 t/hr or more), the physical properties are improved and stabilized (for example, standard deviation of the physical properties is reduced) by a surface-crosslinking treatment, and the absorption against pressure (AAP) and liquid permeability (SFC) are further improved.
    Type: Grant
    Filed: August 27, 2010
    Date of Patent: September 22, 2015
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Kozo Nogi, Kunihiko Ishizaki, Katsuyuki Wada
  • Patent number: 9115235
    Abstract: A water absorbing agent includes water absorbent resin particles which are obtained by polymerizing a water-soluble ethylenic unsaturated monomer and which internally include a cross-linked structure, wherein a pressurized void average radius index is 140 or more. As a result, it is possible to provide a water absorbing agent which essentially includes water absorbent resin particles and is suitable for use in a sanitary material. Specifically, it is possible to improve not only a performance for absorbing and retaining aqueous liquid without pressure or under pressure but also (i) a performance for quickly absorbing aqueous liquid with a great help of a performance of a fibrous material, (ii) a performance for dispersing the aqueous liquid after absorbing the aqueous liquid, and (iii) a performance for retaining the aqueous liquid after absorbing the aqueous liquid.
    Type: Grant
    Filed: August 31, 2007
    Date of Patent: August 25, 2015
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Hiroyuki Ikeuchi, Shigeru Sakamoto, Sayaka Machida, Katsuyuki Wada
  • Publication number: 20150217270
    Abstract: A water absorbent resin (water absorbing agent) and method for producing it are provided which improve, in a water absorbent article (in particular, a diaper) including a water absorbent resin as a water absorbing agent, the absolute absorption amount (g), liquid absorbing times (in particular, liquid absorbing times at the second instance and later), re-wet (g), and diffusion distance (%) of the water absorbent article. A particulate water absorbing agent of the present invention has a CRC, a proportion of particles with sizes of 600 ?m to 150 ?m as defined through a standard-sieve classification, an SST, and the value of the difference between an FST and the SST each within a predetermined range.
    Type: Application
    Filed: August 30, 2013
    Publication date: August 6, 2015
    Inventors: Manabu Ueda, Takahiro Kitano, Yoshitaka Ikeuchi, Hiroyuki Ikeuchi, Katsuyuki Wada
  • Publication number: 20150218341
    Abstract: The present invention (a) provides, at low cost, a water absorbing agent (i) that has a suppressed amount of generated dust and a suppressed amount of dust that increases over time and (ii) that also has a high absorption capacity without load, a high absorption capacity under load, a high vertical diffusion absorbency under load, and a high absorbency in a short period of time, and (b) also provides a method for evaluating, in a short period of time, an amount of dust that increases over time. A particulate water absorbing agent of the present invention includes: a surface crosslinked polyacrylic acid (salt)-based water absorbent resin as a main component; a hydrophilic polymer compound; and a stabilizing agent.
    Type: Application
    Filed: August 27, 2013
    Publication date: August 6, 2015
    Applicant: NIPPON SHOKUBAI CO., LTD.
    Inventors: Yasuhisa Nakashima, Katsuyuki Wada, Hiroyuki Ikeuchi, Manabu Ueda
  • Patent number: 9044525
    Abstract: Provided is a water absorbent resin having excellent liquid permeability, water absorbent speed, anti-impact stability, and weather resistance. Provided is a polyacrylic acid (salt)-based water absorbent resin powder in which the water absorption capacity without load (CRC) is 30 to 45 [g/g], the water absorption capacity under load (AAP 0.3) is 20 to 35 [g/g], the water absorption capacity under load (AAP 0.7) is 10 to 28 [g/g], and the weight average particle diameter (D50) is 300 to 500 ?m, characterized by including p-methoxyphenol; having a degradable soluble component (0.05% L-A (saline) for 2 hours/60° C., one hour extraction rinse/room temperature) of 40% by weight or less; and having a internal gas bubbles ratio of 0.1 to 2.5%, as specified by the following equation.
    Type: Grant
    Filed: June 29, 2012
    Date of Patent: June 2, 2015
    Assignee: NIPPON SHOKUBAI CO., LTD.
    Inventors: Kazushi Torii, Reiko Nakatsuru, Yasuhisa Nakashima, Katsuyuki Wada, Kunihiko Ishizaki