Patents by Inventor Kei UCHIYAMA

Kei UCHIYAMA has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20230340196
    Abstract: A method for producing bisphenol A (BPA) is provided. The method includes step A of degrading a polycarbonate resin in a solvent and distilling off the solvent to obtain a crude solution A; step B of subjecting acetone and phenol to dehydration condensation; step C of distilling off unreacted acetone and water to obtain a concentrated liquid C; step D of crystallizing the concentrated liquid C to obtain a slurry liquid, from which a mother liquor D is obtained; step H of obtaining a solution H1 or a solution H2 from the crude solution A and part of the mother liquor D; and step I of supplying the solution H1 or H2 to the step B or C. The solution H1 contains BPA obtained by degrading BPA contained in the crude solution A and the mother liquor D into phenol and isopropenylphenol and then rebonding phenol and isopropenylphenol, and the solution H2 contains phenol obtained by degrading BPA contained in the crude solution A and the mother liquor D into phenol and acetone.
    Type: Application
    Filed: June 27, 2023
    Publication date: October 26, 2023
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Kazuhisa Hatakeyama
  • Publication number: 20230322653
    Abstract: A method for producing a bisphenol or the like by using a chemical recycling method that is moderate, has a small environmental load, and can efficiently degrade a polycarbonate resin is provided. In addition, a method for producing a recycled polycarbonate resin or the like by using a useful substance such as the bisphenol or the like is provided. A method for producing a bisphenol, including degrading a polycarbonate resin in the presence of an aromatic monoalcohol, water, and a catalyst. A method for producing carbon dioxide, including recovering carbon dioxide generated by the method for producing a bisphenol. A method for producing a carbonic acid diester by using the carbon dioxide. A method for producing a recycled polycarbonate resin by using the bisphenol and/or the carbonic acid diester.
    Type: Application
    Filed: April 28, 2023
    Publication date: October 12, 2023
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Makoto Nakamura
  • Patent number: 11634373
    Abstract: Provided is a thermally stable bisphenol composition whose increase in the Hazen color number is suppressed even under higher temperature conditions. A bisphenol composition including an aryl alkyl sulfide or a dialkyl disulfide at 0.1 ppb by mass to 1% by mass with respect to a bisphenol. A bisphenol composition including an aryl alkyl sulfide or a dialkyl disulfide at a predetermined ratio is thermally stable in terms of the Hazen color number, and shows no coloring problem under high temperature conditions. By using such a bisphenol composition, a polycarbonate resin having an excellent color tone can be produced.
    Type: Grant
    Filed: February 21, 2020
    Date of Patent: April 25, 2023
    Assignee: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Kazuhisa Hatakeyama, Makoto Nakamura, Toshio Uchibori, Michitaka Ise
  • Patent number: 11427523
    Abstract: A bisphenol composition including a specific amount of aromatic alcohol sulfonate, and a simple method of producing it are provided. Also provided is a method of producing a polycarbonate resin in which, by using the bisphenol composition including a specific amount of aromatic alcohol sulfonate, melt polymerization reaction can be efficiently allowed to proceed to produce a polycarbonate resin having an excellent color tone. A bisphenol composition including an aromatic alcohol sulfonate at not less than 0.1 ppb by mass with respect to a bisphenol. A method of producing a bisphenol composition, including reacting a ketone or an aldehyde with an aromatic alcohol in the presence of sulfuric acid to produce a bisphenol composition. A method of producing a polycarbonate resin, including producing a polycarbonate resin using the bisphenol composition. A polycarbonate resin including a specific amount of aromatic alcohol sulfonate.
    Type: Grant
    Filed: February 21, 2020
    Date of Patent: August 30, 2022
    Assignee: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Takayuki Yoshida, Rie Konishi, Kazuo Hirowatari, Takaharu Oono
  • Publication number: 20220098135
    Abstract: A bisphenol composition includes 95% or more by mass of a bisphenol and 200 mass ppm or more of a compound represented by the following general formula (II): In formula (II), R21 and R22 denote a methyl group or a hydrogen atom; R22 is a methyl group when R21 is a hydrogen atom; R22 is a hydrogen atom when R21 is a methyl group; R23 to R25 independently denote a hydrogen atom or an alkyl group having 1 to 20 carbon atoms; and R23, R24, and R25 may be bonded or cross-linked between two of the groups. A method for producing a polycarbonate resin using the bisphenol composition is also described.
    Type: Application
    Filed: September 13, 2021
    Publication date: March 31, 2022
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Masashi Yokogi, Hiroki Shibata, Sora Tomita, Yuichi Yayama, Kenji Tsuruhara, Takayuki Yoshida, Yukie Nakashima, Rie Konishi, Kazuo Hirowatari
  • Publication number: 20210403641
    Abstract: A bisphenol composition including 95% or more by mass of a bisphenol, wherein a bisphenol represented by the following general formula (II) in the bisphenol composition constitutes 150 mass ppm or more, and the bisphenol composition has a methanol dissolution color (Hazen color number) of 2 or less, In formula (II), X denotes a single bond, —CR11R12—, —O—, —CO—, —S—, —SO—, or —SO2—, R11 and R12 independently denote a hydrogen atom or an alkyl group having 1 to 10 carbon atoms, and R11 and R12 may be bonded to each other to form a ring. A method for producing a polycarbonate resin using the bisphenol composition is also described.
    Type: Application
    Filed: September 13, 2021
    Publication date: December 30, 2021
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Masashi Yokogi, Hiroki Shibata, Sora Tomita, Yuichi Yayama, Kenji Tsuruhara, Takayuki Yoshida, Yukie Nakashima, Rie Konishi, Kazuo Hirowatari
  • Publication number: 20200190003
    Abstract: Provided is a thermally stable bisphenol composition whose increase in the Hazen color number is suppressed even under higher temperature conditions. A bisphenol composition including an aryl alkyl sulfide or a dialkyl disulfide at 0.1 ppb by mass to 1% by mass with respect to a bisphenol. A bisphenol composition including an aryl alkyl sulfide or a dialkyl disulfide at a predetermined ratio is thermally stable in terms of the Hazen color number, and shows no coloring problem under high temperature conditions. By using such a bisphenol composition, a polycarbonate resin having an excellent color tone can be produced.
    Type: Application
    Filed: February 21, 2020
    Publication date: June 18, 2020
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei UCHIYAMA, Kazuhisa HATAKEYAMA, Makoto NAKAMURA, Toshia UCHIBORI, Michitaka ISE
  • Publication number: 20200190004
    Abstract: A bisphenol composition including a specific amount of aromatic alcohol sulfonate, and a simple method of producing it are provided. Also provided is a method of producing a polycarbonate resin in which, by using the bisphenol composition including a specific amount of aromatic alcohol sulfonate, melt polymerization reaction can be efficiently allowed to proceed to produce a polycarbonate resin having an excellent color tone. A bisphenol composition including an aromatic alcohol sulfonate at not less than 0.1 ppb by mass with respect to a bisphenol. A method of producing a bisphenol composition, including reacting a ketone or an aldehyde with an aromatic alcohol in the presence of sulfuric acid to produce a bisphenol composition. A method of producing a polycarbonate resin, including producing a polycarbonate resin using the bisphenol composition. A polycarbonate resin including a specific amount of aromatic alcohol sulfonate.
    Type: Application
    Filed: February 21, 2020
    Publication date: June 18, 2020
    Applicant: MITSUBISHI CHEMICAL CORPORATION
    Inventors: Kei Uchiyama, Takayuki Yoshida, Rie Konishi, Kazuo Hirowatari, Takaharu Oono