Patents by Inventor Khalid Mustafa Osman Ortashi

Khalid Mustafa Osman Ortashi has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 10111441
    Abstract: The synthesis of a silver-PMMA nanocomposite film using herbal extract includes mixing an aqueous extract of Aristolochia bracteolate buds with an aqueous solution of silver nitrate, thereby reducing the silver ions to silver metal nanoparticles. A solution of the silver nanoparticles is added to a solution of PMMA [poly (methyl methacrylate)] in N?N-dimethylformamide (DMF) with stirring at 80° C. A brown solution of silver colloids develops, which is cast in a glass plate and the DMF is evaporated at room temperature, leaving a silver-PMMA nanocomposite film. Testing on water shows the silver-PMMA nanocomposite film prevents or inhibits growth of microbes, suggesting use as an antimicrobial or antibacterial agent, e.g., in water purification. In addition, testing by disc diffusion against E. coli and Bacillus cereus showed zones of inhibition, also suggesting use as an antimicrobial or antibacterial agent.
    Type: Grant
    Filed: April 18, 2018
    Date of Patent: October 30, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Dina Wafiq Awad Soliman
  • Patent number: 10052302
    Abstract: The green synthesis of a reduced graphene oxide (rGO) silica (SiO2) nanocomposite using Nigella sativa seed extract includes mixing a quantity of carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a first suspension; stirring the first suspension while maintaining a temperature of the suspension to about 35° C.; adding plant seeds extract to the first suspension while raising the temperature of the suspension to about 60° C.; adding a second oxidant to the suspension to form the reduced graphene oxide nanoparticles; isolating the reduced graphene oxide nanoparticles by centrifugation; suspending the reduced graphene oxide nanoparticles in water; adding a solution comprising tetraethyl orthosilicate (TEOS), concentrated aqueous ammonia solution and a plant seeds extract under ultrasonication; and increasing the temperature to about 90° C. to form reduced graphene oxide-silicon dioxide nanocomposite suspension.
    Type: Grant
    Filed: May 10, 2016
    Date of Patent: August 21, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Patent number: 9988276
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Grant
    Filed: May 17, 2017
    Date of Patent: June 5, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Patent number: 9975780
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Grant
    Filed: May 17, 2017
    Date of Patent: May 22, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Patent number: 9974749
    Abstract: The method of treating diabetic wounds using biosynthesized nanoparticles includes administering an effective amount of silver and gold nanoparticles to a patient in need thereof. The silver and gold nanocomposite is prepared by ‘biosynthesis”, i.e., by providing a first aqueous solution of a noble metal salt or a noble metal oxide; providing a second solution of an aqueous plant extract, and combining the first solution and the second solution to produce a solution including nanoparticles of the noble metal. The second solution includes a plant extract obtained from Solenostemma argel, Trigonella foenum-graecum and Cinnamomum cassia. The metal salt can include silver nitrate (AgNO3) and chloroauric acid (HAuCl4). Nanoparticles of gold and nanoparticles of silver are prepared separately, and then mixed to obtain a composition containing a gold and silver nanocomposite.
    Type: Grant
    Filed: October 7, 2015
    Date of Patent: May 22, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Mai Abdelrahman Elobeid Wagealla, Promy Virk, Khalid Mustafa Osman Ortashi
  • Patent number: 9889170
    Abstract: A method of preparing nanoparticles from desert date can include providing a metal salt solution comprising metal ions; providing desert date extract solution that comprises a reducing agent, and combining the metal ion solution and the desert date extract solution while stirring at a temperature in the range of 25° C. to 100° C. to produce metal or metal oxide nanoparticles. The metal nanoparticles can be gold nanoparticles. The metal oxide nanoparticles can be zinc oxide nanoparticles. The nanoparticles can be used to inhibit the growth or proliferation of a cancer cell and/or microorganisms.
    Type: Grant
    Filed: October 6, 2016
    Date of Patent: February 13, 2018
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Rabab Abd El Moneim Khalil El Dib, Awatif Ahmed Hendi, Shaza Mohamed Adel Al-Massarani, Khalid Mustafa Osman Ortashi
  • Patent number: 9850133
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Grant
    Filed: May 17, 2017
    Date of Patent: December 26, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Publication number: 20170327382
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Application
    Filed: May 17, 2017
    Publication date: November 16, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, AMEL LAREF
  • Publication number: 20170326097
    Abstract: The green synthesis of a reduced graphene oxide (rGO) silica (SiO2) nanocomposite using Nigella sativa seed extract includes mixing a quantity of carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into said solution to oxidize the soot and obtain a first suspension; stirring the first suspension while maintaining a temperature of said suspension to about 35° C.; adding plant seeds extract to the first suspension while raising the temperature of the suspension to about 60° C.; adding a second oxidant to said suspension to form the reduced graphene oxide nanoparticles; isolating the reduced graphene oxide nanoparticles by centrifugation; suspending the reduced graphene oxide nanoparticles in water; adding a solution comprising tetraethyl orthosilicate (TEOS), concentrated aqueous ammonia solution and a plant seeds extract under ultrasonication; and increasing the temperature to about 90° C.
    Type: Application
    Filed: May 10, 2016
    Publication date: November 16, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, AMEL LAREF
  • Publication number: 20170327381
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Application
    Filed: May 17, 2017
    Publication date: November 16, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, AMEL LAREF
  • Publication number: 20170327380
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Application
    Filed: May 17, 2017
    Publication date: November 16, 2017
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Patent number: 9815701
    Abstract: The synthesis of reduced graphene oxide nanoparticles includes the steps of: mixing soot with an acid to obtain a solution; adding a first oxidant gradually into the solution to oxidize the carbon source and obtain a suspension; stirring the suspension while maintaining a temperature of the suspension at about 35° C.; raising the temperature of the suspension to about 60° C.; adding water into the solution; adding a second oxidant into the suspension while stirring resulting in the oxidation of the carbon source to form the reduced graphene oxide nanoparticles; and isolating the resulting reduced graphene oxide nanoparticles by centrifugation. The acid is preferably an acid mixture including, for example, sulfuric acid (H2SO4) and phosphoric acid (H3PO4). The first and second oxidants can be potassium permanganate (KMnO4) or hydrogen peroxide (H2O2).
    Type: Grant
    Filed: February 24, 2017
    Date of Patent: November 14, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref, Nawal Ahmad Madkhali, Hajar Abdullah Aldakhil, Fatimah Yahya Mohammad Al-Abbas, Lena Jassim
  • Publication number: 20170301482
    Abstract: The flexible solar panel includes a polymer matrix and a plant extract incorporated in the polymer matrix. The plant extract can be an extract of chard (B. vulgaris subsp. cicla) including an organic dye. The plant extract can include chloroplasts. The polymer matrix may be formed from either poly(vinyl alcohol) or polystyrene. The flexible solar panel can be green.
    Type: Application
    Filed: April 13, 2016
    Publication date: October 19, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI
  • Patent number: 9789146
    Abstract: A method of preparing Adansonia digitata nanoparticles includes dissolving Adansonia digitata plant powder in an organic solvent to form a solution; spraying the solution in boiling water while applying ultrasonic energy to form a mixture; and stirring the mixture for at least about 15 minutes at a speed of about 200-800 rpm to obtain the Adansonia digitata nanoparticles.
    Type: Grant
    Filed: March 7, 2017
    Date of Patent: October 17, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi
  • Publication number: 20170294272
    Abstract: A dye-sensitized solar panel includes a titanium nanoparticle layer and a plant-derived photo-sensitizer supported on the titanium nanoparticle layer. The photo-sensitizer can be extracted from chard (the cicla cultivar group of B. vulgaris subsp. cicla), and the titanium nanoparticle layer includes titanium nanoparticles synthesized using henna (Lawsonia inermis). The titanium nanoparticle layer can, in addition to titanium nanoparticles, include zinc oxide nanoparticles.
    Type: Application
    Filed: May 4, 2017
    Publication date: October 12, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, NAWAL AHMAD ABDU MADKHALI
  • Publication number: 20170294271
    Abstract: The dye-sensitized solar panel includes a metal oxide layer and an organic photosensitizing dye on the metal oxide layer. The organic photosensitizing dye is extracted from chard (B. vulgaris subsp. cicla), and the metal oxide layer is composed of zinc oxide nanoparticles synthesized using B. vulgaris subsp. cicla dye as a reducing agent. A working electrode is mounted on a first transparent substrate. The working electrode includes a metal electrode and the metal oxide layer formed thereon. A counter electrode is mounted on a second transparent substrate. An electrolyte is sandwiched between the working electrode and the counter electrode.
    Type: Application
    Filed: April 12, 2016
    Publication date: October 12, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, NAWAL AHMAD ABDU MADKHALI, AISHA SALAH BADWELAN
  • Publication number: 20170294270
    Abstract: A dye-sensitized solar panel includes a titanium nanoparticle layer and a plant-derived photo-sensitizer supported on the titanium nanoparticle layer. The photo-sensitizer can be extracted from chard (B. vulgaris subsp. cicla), and the titanium nanoparticle layer includes titanium nanoparticles synthesized using henna (Lawsonia inermis). The titanium nanoparticle layer can, in addition to titanium nanoparticles, include zinc oxide nanoparticles.
    Type: Application
    Filed: April 12, 2016
    Publication date: October 12, 2017
    Inventors: MANAL AHMED GASMELSEED AWAD, AWATIF AHMED HENDI, KHALID MUSTAFA OSMAN ORTASHI, NAWAL AHMAD ABDU MADKHALI
  • Patent number: 9701552
    Abstract: A method of preparing metal nanoparticles from fungi includes preparing a biomass of fungal cells; providing an aqueous solution including a metal salt; mixing the biomass of fungal cells with the aqueous solution of metal salt; and incubating the resulting mixture at a temperature range of 35° C. to 60° C. to produce the metal nanoparticles.
    Type: Grant
    Filed: October 28, 2016
    Date of Patent: July 11, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Khalid Mustafa Osman Ortashi, Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Abeer Ramadan Mohamed Abdelaziz, Ahmed Sameer Ahmed Hendi, Abdulhakeem Abdulmuhseen Alahmed
  • Patent number: 9688539
    Abstract: The green synthesis of reduced graphene oxide nanoparticles using Nigella sativa seed extract comprises the steps of mixing a quantity of soot or other carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a suspension; stirring the suspension while maintaining the temperature of the suspension at about 35° C.; adding Nigella sativa seed extract to the suspension while raising the temperature of the suspension to about 60° C.; adding hydrogen peroxide to the suspension; and isolating the reduced graphene oxide nanoparticles by centrifugation.
    Type: Grant
    Filed: May 10, 2016
    Date of Patent: June 27, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Awatif Ahmed Hendi, Khalid Mustafa Osman Ortashi, Amel Laref
  • Patent number: 9623067
    Abstract: A method of preparing nanoparticles of date palm seeds comprises providing date seed powder; mixing the date seed powder with an acid solution to produce date palm seed nanoparticles; and isolating the date palm seed nanoparticles. A method of controlling the growth or proliferation of bacteria can include administering an effective amount of the date palm seed nanoparticles synthesized according to the present method to a site of bacterial activity.
    Type: Grant
    Filed: October 24, 2016
    Date of Patent: April 18, 2017
    Assignee: KING SAUD UNIVERSITY
    Inventors: Manal Ahmed Gasmelseed Awad, Ebtesam Mohammed Al Olayan, Hany Mohamed Yehia, Khalid Mustafa Osman Ortashi, Hatem Salama Mohamed Ali, Manal Fawzy Elkhadragy