Patents by Inventor Kirk L. Williams

Kirk L. Williams has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11788213
    Abstract: A method of making a multi-composition fiber is provided, which includes providing a precursor laden environment, and forming a fiber in the precursor laden environment using laser heating. The precursor laden environment includes a primary precursor material and an elemental precursor material. The formed fiber includes a primary fiber material and an elemental additive material, where the elemental additive material has too large an atom size to fit within a single crystalline domain within a crystalline structure of the fiber, and is deposited on grain boundaries between adjacent crystalline domains of the primary fiber material to present an energy barrier to atomic diffusion through the grain boundaries, and to increase creep resistance by slowing down growth between the adjacent crystalline domains of the primary fiber material.
    Type: Grant
    Filed: December 23, 2020
    Date of Patent: October 17, 2023
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Shay L. Harrison, Joseph Pegna, Erik G. Vaaler, Ram K. Goduguchinta, Kirk L. Williams, John L. Schneiter
  • Publication number: 20220411921
    Abstract: Methods of forming a ceramic matrix, as well as fiber preforms and methods of forming fiber preforms to facilitate formation of a ceramic matrix are provided. The method includes obtaining a fiber preform to facilitate forming the ceramic matrix. The fiber preform includes a fiber layer with a plurality of fibers and a heating element embedded within the fiber preform. The method also includes heating the fiber preform via the heating element embedded within the fiber preform, and depositing matrix material into the fiber preform by embedded wire chemical vapor deposition (EWCVD) of the matrix material during the heating of the fiber preform by the heating element. The chemical vapor deposition of the matrix material within the fiber preform facilitates formation of the ceramic matrix.
    Type: Application
    Filed: April 28, 2022
    Publication date: December 29, 2022
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Joseph PEGNA, Kirk L. WILLIAMS, Shay L. HARRISON
  • Patent number: 11518719
    Abstract: Nuclear fuel structures and methods for fabricating are disclosed herein. The nuclear fuel structure includes a plurality of fibers arranged in the structure and a multilayer fuel region within at least one fiber of the plurality of fibers. The multilayer fuel region includes an inner layer region made of a nuclear fuel material, and an outer layer region encasing the nuclear fuel material. A plurality of discrete multilayer fuel regions may be formed over a core region along the at least one fiber, the plurality of discrete multilayer fuel regions having a respective inner layer region of nuclear fuel material and a respective outer layer region encasing the nuclear fuel material. The plurality of fibers may be wrapped around an inner rod or tube structure or inside an outer tube structure of the nuclear fuel structure, providing both structural support and the nuclear fuel material of the nuclear fuel structure.
    Type: Grant
    Filed: January 27, 2020
    Date of Patent: December 6, 2022
    Assignee: Free Form Fibers, LLC
    Inventors: Joseph Pegna, Erik G. Vaaler, Shay L. Harrison, John L. Schneiter, Kirk L. Williams, Ram K. Goduguchinta
  • Patent number: 11362256
    Abstract: A method is provided for growing a fiber structure, where the method includes: obtaining a substrate, growing an array of pedestal fibers on the substrate, growing fibers on the pedestal fibers, and depositing a coating surrounding each of the fibers. In another aspect, a method of fabricating a fiber structure includes obtaining a substrate and growing a plurality of fibers on the substrate according to 1½D printing. In another aspect, a multilayer functional fiber is provided produced by, for instance, the above-noted methods.
    Type: Grant
    Filed: June 27, 2018
    Date of Patent: June 14, 2022
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Joseph Pegna, Ram K. Goduguchinta, Kirk L. Williams, John L. Schneiter, Shay L. Harrison, Erik G. Vaaler
  • Publication number: 20220144711
    Abstract: A method of forming a high purity ingot for wafer production, such as a silicon carbidewafer. Precursors are added to a reactor; at least part of a fiber is formed in the reactor from the precursors using chemical deposition interacting with the precursors; and granular material is then formed from the fiber. The method further includes forming the ingot from the granular material. In one aspect, the chemical deposition can include laser induced chemical vapor deposition. Further, the method can include separating one or more wafers from the ingot for use in semiconductor fabrication.
    Type: Application
    Filed: January 21, 2022
    Publication date: May 12, 2022
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, John L. SCHNEITER, Joseph PEGNA, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS, Erik G. VAALER
  • Publication number: 20210253434
    Abstract: A method and apparatus for forming a plurality of fibers from (e.g., CVD) precursors, including a reactor adapted to grow a plurality of individual fibers; and a plurality of independently controllable lasers, each laser of the plurality of lasers growing a respective fiber. A high performance fiber (HPF) structure, including a plurality of fibers arranged in the structure; a matrix disposed between the fibers; wherein a multilayer coating is provided along the surfaces of at least some of the fibers with an inner layer region having a sheet-like strength; and an outer layer region, having a particle-like strength, such that any cracks propagating toward the outer layer from the matrix propagate along the outer layer and back into the matrix, thereby preventing the cracks from approaching the fibers.
    Type: Application
    Filed: November 2, 2020
    Publication date: August 19, 2021
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Joseph PEGNA, John L. SCHNEITER, Kirk L. WILLIAMS, Ramkiran GODUGUCHINTA
  • Publication number: 20210230743
    Abstract: A method of forming a high purity granular material, such as silicon carbide powder. Precursors are added to a reactor; at least part of a fiber is formed in the reactor from the precursors using chemical deposition interacting with said precursors; and the granular material is then formed from the fiber. In one aspect, the chemical deposition may include laser induced chemical vapor deposition. The granular material may be formed by grinding or milling the fiber into the granular material, e.g., ball milling the fiber. In one example, silicon carbide powder having greater than 90% beta crystalline phase purity and less than 0.25% oxygen contamination can be obtained.
    Type: Application
    Filed: January 25, 2021
    Publication date: July 29, 2021
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, John L. SCHNEITER, Joseph PEGNA, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS, Erik G. VAALER
  • Publication number: 20210222332
    Abstract: A multi-composition fiber is provided including a primary fiber material and an elemental additive material deposited on grain boundaries between adjacent crystalline domains of the primary fiber material. A method of making a multi-composition fiber is also provided, which includes providing a precursor laden environment, and promoting fiber growth using laser heating. The precursor laden environment includes a primary precursor material and an elemental precursor material.
    Type: Application
    Filed: December 23, 2020
    Publication date: July 22, 2021
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, Joseph PEGNA, Erik G. VAALER, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS, John L. SCHNEITER
  • Patent number: 10882749
    Abstract: A method and apparatus for forming a plurality of fibers from (e.g., CVD) precursors, including a reactor adapted to grow a plurality of individual fibers; and a plurality of independently controllable lasers, each laser of the plurality of lasers growing a respective fiber. A high performance fiber (HPF) structure, including a plurality of fibers arranged in the structure; a matrix disposed between the fibers; wherein a multilayer coating is provided along the surfaces of at least some of the fibers with an inner layer region having a sheet-like strength; and an outer layer region, having a particle-like strength, such that any cracks propagating toward the outer layer from the matrix propagate along the outer layer and back into the matrix, thereby preventing the cracks from approaching the fibers.
    Type: Grant
    Filed: August 13, 2018
    Date of Patent: January 5, 2021
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Joseph Pegna, John L. Schneiter, Kirk L. Williams, Ramkiran Goduguchinta
  • Patent number: 10876227
    Abstract: A multi-composition fiber is provided including a primary fiber material and an elemental additive material deposited on grain boundaries between adjacent crystalline domains of the primary fiber material. A method of making a multi-composition fiber is also provided, which includes providing a precursor laden environment, and promoting fiber growth using laser heating. The precursor laden environment includes a primary precursor material and an elemental precursor material.
    Type: Grant
    Filed: November 29, 2017
    Date of Patent: December 29, 2020
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Shay L. Harrison, Joseph Pegna, Erik G. Vaaler, Ram K. Goduguchinta, Kirk L. Williams, John L. Schneiter
  • Patent number: 10822240
    Abstract: A method and apparatus for forming a plurality of fibers from (e.g., CVD) precursors, including a reactor adapted to grow a plurality of individual fibers; and a plurality of independently controllable lasers, each laser of the plurality of lasers growing a respective fiber. A high performance fiber (HPF) structure, including a plurality of fibers arranged in the structure; a matrix disposed between the fibers; wherein a multilayer coating is provided along the surfaces of at least some of the fibers with an inner layer region having a sheet-like strength; and an outer layer region, having a particle-like strength, such that any cracks propagating toward the outer layer from the matrix propagate along the outer layer and back into the matrix, thereby preventing the cracks from approaching the fibers.
    Type: Grant
    Filed: August 13, 2018
    Date of Patent: November 3, 2020
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Joseph Pegna, John L. Schneiter, Kirk L. Williams, Ramkiran Goduguchinta
  • Publication number: 20200203028
    Abstract: Nuclear fuel structures and methods for fabricating are disclosed herein. The nuclear fuel structure includes a plurality of fibers arranged in the structure and a multilayer fuel region within at least one fiber of the plurality of fibers. The multilayer fuel region includes an inner layer region made of a nuclear fuel material, and an outer layer region encasing the nuclear fuel material. A plurality of discrete multilayer fuel regions may be formed over a core region along the at least one fiber, the plurality of discrete multilayer fuel regions having a respective inner layer region of nuclear fuel material and a respective outer layer region encasing the nuclear fuel material. The plurality of fibers may be wrapped around an inner rod or tube structure or inside an outer tube structure of the nuclear fuel structure, providing both structural support and the nuclear fuel material of the nuclear fuel structure.
    Type: Application
    Filed: January 27, 2020
    Publication date: June 25, 2020
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Joseph PEGNA, Erik G. VAALER, Shay L. HARRISON, John L. SCHNEITER, Kirk L. WILLIAMS, Ram K. GODUGUCHINTA
  • Patent number: 10546661
    Abstract: Nuclear fuel structures and methods for fabricating are disclosed herein. The nuclear fuel structure includes a plurality of fibers arranged in the structure and a multilayer fuel region within at least one fiber of the plurality of fibers. The multilayer fuel region includes an inner layer region made of a nuclear fuel material, and an outer layer region encasing the nuclear fuel material. A plurality of discrete multilayer fuel regions may be formed over a core region along the at least one fiber, the plurality of discrete multilayer fuel regions having a respective inner layer region of nuclear fuel material and a respective outer layer region encasing the nuclear fuel material. The plurality of fibers may be wrapped around an inner rod or tube structure or inside an outer tube structure of the nuclear fuel structure, providing both structural support and the nuclear fuel material of the nuclear fuel structure.
    Type: Grant
    Filed: June 23, 2015
    Date of Patent: January 28, 2020
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Joseph Pegna, Erik G. Vaaler, Shay L. Harrison, John L. Schneiter, Kirk L. Williams, Ram K. Goduguchinta
  • Publication number: 20190062222
    Abstract: A method and apparatus for forming a plurality of fibers from (e.g., CVD) precursors, including a reactor adapted to grow a plurality of individual fibers; and a plurality of independently controllable lasers, each laser of the plurality of lasers growing a respective fiber. A high performance fiber (HPF) structure, including a plurality of fibers arranged in the structure; a matrix disposed between the fibers; wherein a multilayer coating is provided along the surfaces of at least some of the fibers with an inner layer region having a sheet-like strength; and an outer layer region, having a particle-like strength, such that any cracks propagating toward the outer layer from the matrix propagate along the outer layer and back into the matrix, thereby preventing the cracks from approaching the fibers.
    Type: Application
    Filed: August 13, 2018
    Publication date: February 28, 2019
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Joseph PEGNA, John L. SCHNEITER, Kirk L. WILLIAMS, Ramkiran GODUGUCHINTA
  • Publication number: 20180370860
    Abstract: A method is provided for growing a fiber structure, where the method includes: obtaining a substrate, growing an array of pedestal fibers on the substrate, growing fibers on the pedestal fibers, and depositing a coating surrounding each of the fibers. In another aspect, a method of fabricating a fiber structure includes obtaining a substrate and growing a plurality of fibers on the substrate according to 1½D printing. In another aspect, a multilayer functional fiber is provided produced by, for instance, the above-noted methods.
    Type: Application
    Filed: June 27, 2018
    Publication date: December 27, 2018
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Joseph PEGNA, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS, John L. SCHNEITER, Shay L. HARRISON, Erik G. VAALER
  • Patent number: 10047015
    Abstract: A method and apparatus for forming a plurality of fibers from (e.g., CVD) precursors, including a reactor adapted to grow a plurality of individual fibers; and a plurality of independently controllable lasers, each laser of the plurality of lasers growing a respective fiber. A high performance fiber (HPF) structure, including a plurality of fibers arranged in the structure; a matrix disposed between the fibers; wherein a multilayer coating is provided along the surfaces of at least some of the fibers with an inner layer region having a sheet-like strength; and an outer layer region, having a particle-like strength, such that any cracks propagating toward the outer layer from the matrix propagate along the outer layer and back into the matrix, thereby preventing the cracks from approaching the fibers.
    Type: Grant
    Filed: January 18, 2013
    Date of Patent: August 14, 2018
    Assignee: FREE FORM FIBERS, LLC
    Inventors: Joseph Pegna, John L. Schneiter, Kirk L. Williams, Ramkiran Goduguchinta
  • Publication number: 20180148864
    Abstract: A multi-composition fiber is provided including a primary fiber material and an elemental additive material deposited on grain boundaries between adjacent crystalline domains of the primary fiber material. A method of making a multi-composition fiber is also provided, which includes providing a precursor laden environment, and promoting fiber growth using laser heating. The precursor laden environment includes a primary precursor material and an elemental precursor material.
    Type: Application
    Filed: November 29, 2017
    Publication date: May 31, 2018
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, Joseph PEGNA, Erik G. VAALER, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS, John L. SCHNEITER
  • Patent number: 9938393
    Abstract: A fully dense ceramic and/or other inorganic fiber containing elongated crystal grains in and around the fiber center and oriented along the fiber axis, with a smooth transition to more equiaxed grains towards the radial periphery of the fiber, and method for producing such.
    Type: Grant
    Filed: January 22, 2016
    Date of Patent: April 10, 2018
    Assignee: FREE FORM FIBERS, LLC
    Inventors: John L. Schneiter, Joseph Pegna, Ramkiran Goduguchinta, Kirk L. Williams, Shay Llewellyn Harrison
  • Publication number: 20180087157
    Abstract: Multi-composition fibers with one or more refractory additives, and methods of making the fibers, are provided. The method(s) includes providing a precursor-laden environment, and promoting fiber growth using laser heating. The precursor-laden environment includes a primary precursor material and a refractory precursor material. The multi-composition fiber may include a primary fiber material, and a refractory material substantially homogeneously intermixed with the primary fiber material.
    Type: Application
    Filed: September 28, 2017
    Publication date: March 29, 2018
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, Joseph PEGNA, Erik G. VAALER, John L. SCHNEITER, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS
  • Publication number: 20180087214
    Abstract: A refractory oxide coated fiber is provided including a primary fiber material and a refractory oxide coating over the primary fiber material. Further, a method of making a refractory oxide coated fiber is provided, which includes: providing a first precursor-laden environment, the first precursor-laden environment including a primary precursor; promoting fiber growth within the first precursor-laden environment using laser heating; and providing a second precursor-laden environment to promote coating of the fiber, the second precursor-laden environment comprising a refractory oxide precursor, and the coating producing a refractory oxide coating over the fiber with a hexagonal microstructure.
    Type: Application
    Filed: September 28, 2017
    Publication date: March 29, 2018
    Applicant: FREE FORM FIBERS, LLC
    Inventors: Shay L. HARRISON, Marvin KESHNER, Joseph PEGNA, Erik G. VAALER, John L. SCHNEITER, Ram K. GODUGUCHINTA, Kirk L. WILLIAMS