Abstract: An apparatus and method for nondestructively measuring a sample of material to determine changes in dynamic Young's Modulus, density, static viscosity, compressive strength and expansion or contraction of a material over a period of time and at substantially constant temperature and pressure. Samples of particular interest are cements and completions gels whose characteristic dynamic Young's Modulus, density, viscosity, compressive strength and expansion or contraction at down-hole conditions are particularly important to the petroleum industry.

Abstract: A method for determining the relative HAZ toughness of steel. The method comprises determining at least two thermal cycles of the steel for at least one weld heat input value and then simulating the HAZ that would result if the steel were actually welded in accordance with those thermal cycles. The steel is then fractured to determine various fracture properties, each of which may be used to determine the midpoint transition temperature associated with the fracture property used. The midpoint transition temperature is compared to a previously determined standard maximum midpoint transition temperature and if it is greater than the standard, the steel may have low HAZ toughness, but if it is less than the standard, the steel may have a high HAZ toughness.

Abstract: The electron bombardment furnace (B) consists of two confinement grid sections (26,28) which may be moved and separated from each other. Inside the bombardment furnace, a tungsten element (14) is enclosed. The material specimen (18) is located within the tungsten element and grounded by means of grounded support wires (20,22) connected to the respective sections of the furnace. The material specimen (18) is supported on the ground wires and heated by electron bombardment until melt occurs. The furnace sections are separated in opposite directions causing the ground wires to pull from the surfaces of the specimen, leaving the specimen freely suspended in the process chamber without the action of external forces. The specimen remains in its melt condition in the processing chamber where it can be undercooled without external forces acting on the specimen, which would cause dynamic nucleation.

Abstract: A method and apparatus for preparing and studying samples of materials supercooled and solidified in a containerless, low-gravity environment in bulk form is disclosed which includes an enclosure 10 in which a containerless environment is provided in which a sample specimen 52 is positioned. Method contemplates heating the specimen 52 in the containerless environment, dropping the specimen melt through the tube 12 wherein it cools by radiation, and alternately backfilling the tube 12 with an inert gas whereby the specimen melt cools by both radiation and convection during its free fall. During the free fall, the sample is in a containerless, low-gravity environment which will enhance supercooling in the sample and prevent sedimentation and thermal convection influences. The sample will continue to supercool until nucleation occurs which is detected by silicon photovoltaic detectors. The sample will solidify after nucleation and be completely solid before entering the detachable catcher.

Abstract: Containerless high temperature calorimeter apparatus is disclosed for measuring high temperature thermophysical properties of materials which includes a unique containerless heating apparatus wherein the specimen is suspended and heated by electron bombardment.