Abstract: A method for preparing a supercapacitor with good cycling stability uses NiO@CoMoO4/NF, an activated carbon plate, a KOH solution (6 mol/L), and polypropylene as raw materials, and is implemented through preparation of an NiO@CoMoO4/NF electrode and assembly of the supercapacitor, wherein the NiO@CoMoO4/NF is the anode of the supercapacitor, the activated carbon plate is the cathode of the supercapacitor, the KOH solution is the electrolyte, and the polypropylene is an isolation plate. The NiO@CoMoO4/NF electrode in the supercapacitor of the present disclosure treated with the ductile material can better adapt to volume changes during the charging and discharging process. After 10,000 cycles of charging and discharging, the capacity of the present disclosure has not faded and still maintains 100% of the maximum capacity, with a high specific capacitance of 79.4 F/g, an energy density of 35.7 Wh/kg, and a functional density of 899.5 W/kg.