Abstract: The present invention discloses a new method for synthesizing a high-quality inorganic film by microwave heating, which relates to the field of preparation of inorganic materials. The method for synthesizing a high-quality inorganic film by microwave heating in the present invention allows a fine design and control of the temperature increase process during microwave heating, wherein the matrix and the synthesis solution is put into the microwave reactor at first, the temperature interval between the initial temperature and the target temperature of the synthesis solution is then divided into multiple sections, each of which sets a temperature increase rate, and then when the temperature reaches the target temperature after the designed temperature increase process, the synthesis solution reacts for a period of time at the target temperature, finally the high-quality inorganic film can be obtained after the treatment of washing and drying.