Abstract: The invention provides a method and apparatus for sampling a frozen core of tar sand. The frozen core is first cut transversely along its length to form a pair of slabs of semi-circular cross-section. A longitudinal sample portion of substantially triangular cross-section is then cut from the central portion of the still frozen slab. The triangular sample portion is ground in a cryogenic grinder to produce a finely divided, substantially homogeneous material from which small representative sub-samples may be obtained. The triangular sample portion is cut from the slab by a pair of angularly disposed circular saws carried along the length of the slab. The slab is supported and held by cradle means which fix the flat face of the slab in a predetermined plane. The longitudinal sample portion thus formed has a triangular cross-section of substantially constant cross-sectional area.

Abstract: An oily mass of solids tailings is derived from flotation of bitumen during hot water extraction of bituminous sands, and subsequent separation of most of the bitumen from associated solids. This oily mass contains a high concentration of heavy minerals, in the order of 10% by weight titanium and 4% zirconium. The tailings are introduced into a hot reaction zone and contacted with oxygen while agitating the solids. The bitumen associated with the solids is burned, as is residual coke left from the combustion of the bitumen. The product particles are discrete, dry and clean. They can be slurried with water and passed through gravity concentrating means, such as a spiral, to produce a concentrate containing in the order of 18% titanium and 8% zirconium.

Abstract: An oily mass of solids tailings is derived from flotation of bitumen during hot water extraction of bituminous sands, and subsequent separation of most of the bitumen from associated solids. This oily mass contains a high concentration of heavy minerals, in the order of 10% by weight titanium and 4% zirconium. The tailings are introduced into a hot reaction zone and contacted with oxygen while agitating the solids. The bitumen associated with the solids is burned, as is residual coke left from the combustion of the bitumen. The product particles are discrete, dry and clean. They can be slurried with water and passed through gravity concentrating means, such as a spiral, to produce a concentrate containing in the order of 18% titanium and 8% zirconium.