Patents by Inventor Luca RUGNONE

Luca RUGNONE has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11236043
    Abstract: A process for the production of ammonia and urea in an ammonia-urea integrated plant comprising an ammonia section and a tied-in urea section, wherein a hydrocarbon is reformed to produce ammonia make-up synthesis gas; said make-up gas is purified by shift conversion and removal of carbon dioxide; carbon dioxide is removed from the make-up gas by a first and a second CO2 removal sections; the first section removes CO2 by absorption with a suitable medium, and the second section removes CO2 by washing with a carbamate solution taken from the urea section; the make-up gas is reacted to produce ammonia; the CO2 removed from the make-up gas and at least part of the ammonia are used to produce urea.
    Type: Grant
    Filed: February 1, 2018
    Date of Patent: February 1, 2022
    Assignee: Casale SA
    Inventors: Francesco Nettuno, Luca Rugnone, Raffaele Ostuni
  • Publication number: 20210172785
    Abstract: A method and system for measuring a liquid level in a pressure vessel, the method comprising: transmitting an electromagnetic signal through a wave guide in the form of an elongate solid rod (5) with bottom end immersed in the liquid and detecting a signal generated by the reflection on the surface of the liquid.
    Type: Application
    Filed: November 6, 2018
    Publication date: June 10, 2021
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10927012
    Abstract: A process and system for removing ammonia from ammonia-containing purge gas of a urea plant, the process comprising: contacting said ammonia-containing purge gas with carbon dioxide at a low temperature, reaction of ammonia to form crystals of ammonium salts in a multiphase stream, and removal of the solid ammonium salts from the multiphase stream.
    Type: Grant
    Filed: February 1, 2018
    Date of Patent: February 23, 2021
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10781167
    Abstract: A shell-and-tube stripper for carbamate decomposition and ammonia recovery from a urea solution comprising a bundle of heated tubes, said tubes being fed with said urea solution and carbon dioxide as stripping medium, the urea solutions forming a liquid falling film on the internal surface of the tubes and the carbon dioxide forming a counter-current gaseous flow; said tubes comprise an external layer made of super austenitic or super duplex stainless steel and an internal layer made of zirconium, said internal layer reaching temperatures higher than 220° C.
    Type: Grant
    Filed: December 9, 2016
    Date of Patent: September 22, 2020
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10703686
    Abstract: A process for making a combined fertilizer comprising a first nitrogen-based fertilizer, such as urea or ammonium nitrate, and one or more further components chosen among: nitrogen-based fertilizers, being different from the first nitrogen-based fertilizer and nutrients, wherein the combined fertilizer is made by a process of granulation in a fluid bed, the fluid bed being preferably in a vortex condition.
    Type: Grant
    Filed: April 13, 2016
    Date of Patent: July 7, 2020
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10550075
    Abstract: Integrated process for the production of urea and urea-ammonium nitrate, comprising: reacting ammonia and carbon dioxide to form a reaction mixture (4) containing urea and unconverted materials, and also comprising the recovery of unconverted materials in a first recovery stage at a first pressure and in a second recovery stage at a second pressure, wherein ammonia-containing offgas (19) released by said second recovery stage are condensed at said second pressure, and said condensed offgas (20) are recycled to said first recovery stage.
    Type: Grant
    Filed: September 4, 2017
    Date of Patent: February 4, 2020
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20200002273
    Abstract: A process for the production of ammonia and urea in an ammonia-urea integrated plant comprising an ammonia section and a tied-in urea section, wherein a hydrocarbon is reformed to produce ammonia make-up synthesis gas; said make-up gas is purified by shift conversion and removal of carbon dioxide; carbon dioxide is removed from the make-up gas by a first and a second CO2 removal sections;the first section removes CO2 by absorption with a suitable medium, and the second section removes CO2 by washing with a carbamate solution taken from the urea section; the make-up gas is reacted to produce ammonia; the CO2 removed from the make-up gas and at least part of the ammonia are used to produce urea.
    Type: Application
    Filed: February 1, 2018
    Publication date: January 2, 2020
    Applicant: Casale SA
    Inventors: Francesco Nettuno, Luca Rugnone, Raffaele Ostuni
  • Publication number: 20190375649
    Abstract: A process and system for removing ammonia from ammonia-containing purge gas of a urea plant, the process comprising: contacting said ammonia-containing purge gas with carbon dioxide at a low temperature, reaction of ammonia to form crystals of ammonium salts in a multiphase stream, and removal of the solid ammonium salts from the multiphase stream.
    Type: Application
    Filed: February 1, 2018
    Publication date: December 12, 2019
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10493421
    Abstract: A combined reactor and condenser for the synthesis of urea from ammonia and carbon dioxide, including a condenser section coupled to a reaction section, comprising inputs directed to said condenser section for a gaseous stream comprising ammonia and carbon dioxide and for a solution containing ammonium carbamate and liquid ammonia, and wherein the effluent of the condenser section is sent to the reaction section; the reaction section comprises a plurality of compartments and a plurality of mixers, at least one inside each of said compartments.
    Type: Grant
    Filed: July 20, 2016
    Date of Patent: December 3, 2019
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20190359558
    Abstract: Integrated process for the production of urea and urea-ammonium nitrate, comprising: reacting ammonia and carbon dioxide to form a reaction mixture (4) containing urea and unconverted materials, and also comprising the recovery of unconverted materials in a first recovery stage at a first pressure and in a second recovery stage at a second pressure, wherein ammonia-containing offgas (19) released by said second recovery stage are condensed at said second pressure, and said condensed offgas (20) are recycled to said first recovery stage.
    Type: Application
    Filed: September 4, 2017
    Publication date: November 28, 2019
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Patent number: 10209191
    Abstract: The invention discloses the use of Raman spectroscopy to analyze one or more process streams (5) of a urea synthesis production plant, where urea is synthesised from ammonia and carbon dioxide at high pressure (100-300 bar) and high temperature (50-250° C.). The radiation generated by the Raman scattering is analyzed to determine the concentration of components such as urea, ammonia and carbon dioxide in the process streams (5). A logic system implemented in a plant control unit (1) generates signals to target plant actuators to optimize the operation.
    Type: Grant
    Filed: June 2, 2015
    Date of Patent: February 19, 2019
    Assignee: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20180362452
    Abstract: A shell-and-tube stripper for carbamate decomposition and ammonia recovery from a urea solution comprising a bundle of heated tubes, said tubes being fed with said urea solution and carbon dioxide as stripping medium, the urea solutions forming a liquid falling film on the internal surface of the tubes and the carbon dioxide forming a counter-current gaseous flow; said tubes comprise an external layer made of super austenitic or super duplex stainless steel and an internal layer made of zirconium, said internal layer reaching temperatures higher than 220° C.
    Type: Application
    Filed: December 9, 2016
    Publication date: December 20, 2018
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20180243723
    Abstract: A combined reactor and condenser for the synthesis of urea from ammonia and carbon dioxide, including a condenser section coupled to a reaction section, comprising inputs directed to said condenser section for a gaseous stream comprising ammonia and carbon dioxide and for a solution containing ammonium carbamate and liquid ammonia, and wherein the effluent of the condenser section is sent to the reaction section; the reaction section comprises a plurality of compartments and a plurality of mixers, at least one inside each of said compartments.
    Type: Application
    Filed: July 20, 2016
    Publication date: August 30, 2018
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20180141879
    Abstract: A process for making a combined fertilizer comprising a first nitrogen-based fertilizer, such as urea or ammonium nitrate, and one or more further components chosen among: nitrogen-based fertilizers, being different from the first nitrogen-based fertilizer and nutrients, wherein the combined fertilizer is made by a process of granulation in a fluid bed, the fluid bed being preferably in a vortex condition.
    Type: Application
    Filed: April 13, 2016
    Publication date: May 24, 2018
    Applicant: Casale SA
    Inventor: Luca Rugnone
  • Publication number: 20170102333
    Abstract: The invention discloses the use of Raman spectroscopy to analyze one or more process streams (5) of a urea synthesis production plant, where urea is synthesised from ammonia and carbon dioxide at high pressure (100-300 bar) and high temperature (50-250° C.). The radiation generated by the Raman scattering is analyzed to determine the concentration of components such as urea, ammonia and carbon dioxide in the process streams (5). A logic system implemented in a plant control unit (1) generates signals to target plant actuators to optimize the operation.
    Type: Application
    Filed: June 2, 2015
    Publication date: April 13, 2017
    Applicant: Casale SA
    Inventor: Luca RUGNONE