Patents by Inventor M. Leslie Carman

M. Leslie Carman has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11725137
    Abstract: A plastic scintillator includes a polymer matrix, an aliphatic additive present in the polymer matrix in an effective amount to impart fog resistance to the plastic scintillator, and at least one fluorescent dye in the polymer matrix, the dye being effective to provide scintillation upon exposure to radiation. The effective amount of the aliphatic additive is in a range of greater than 0 weight percent up to 5 weight percent relative to the total weight of the plastic scintillator. Moreover, the aliphatic additive has a structure comprising up to 300 repeat units.
    Type: Grant
    Filed: April 29, 2021
    Date of Patent: August 15, 2023
    Assignees: Lawrence Livermore National Security, LLC, Ludlum Measurements, Inc., National Technology & Engineering Solutions of Sandia, LLC
    Inventors: Andrew Neil Mabe, M Leslie Carman, Stephen Anthony Payne, Natalia P. Zaitseva, Charles R. Hurlbut, Terence C. O'Brien, Kyle Ray Shipp, Nicholas Richard Myllenbeck
  • Publication number: 20210340437
    Abstract: A plastic scintillator includes a polymer matrix, an aliphatic additive present in the polymer matrix in an effective amount to impart fog resistance to the plastic scintillator, and at least one fluorescent dye in the polymer matrix, the dye being effective to provide scintillation upon exposure to radiation. The effective amount of the aliphatic additive is in a range of greater than 0 weight percent up to 5 weight percent relative to the total weight of the plastic scintillator. Moreover, the aliphatic additive has a structure comprising up to 300 repeat units.
    Type: Application
    Filed: April 29, 2021
    Publication date: November 4, 2021
    Applicants: Lawrence Livermore National Security, LLC, National Technology & Engineering Solutions of Sandia, LLC, Ludlum Measurements, Inc., National Technology & Engineering Solutions of Sandia, LLC
    Inventors: Andrew Neil Mabe, M Leslie Carman, Stephen Anthony Payne, Natalia P. Zaitseva, Charles R. Hurlbut, Terence C. O'Brien, Kyle Ray Shipp, Nicholas Richard Myllenbeck
  • Publication number: 20210317364
    Abstract: A scintillator material includes a polymer matrix, a primary dye in the polymer matrix, the primary dye being a fluorescent dye; a secondary dye, and a Li-containing compound in the polymer matrix, where the Li-containing compound is a Li salt of a short-chain aliphatic acid. In addition, the scintillator material exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons.
    Type: Application
    Filed: April 8, 2021
    Publication date: October 14, 2021
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Andrew M. Glenn, Andrew Neil Mabe
  • Publication number: 20200224087
    Abstract: Scintillating plastics resistant to crazing and fogging, methods of making and using the same are disclosed. The scintillating plastics include: one or more primary polymers present in an amount ranging from about 40 wt % to about 95 wt %; one or more secondary polymers present in an amount ranging from about 1 wt % to about 60 wt %; and one or more fluors present in an amount ranging from about 0.1 wt % to about 50 wt %. Methods of making such plastics include: creating a homogenous mixture of precursor materials including primary polymer, secondary polymer, and fluor in the amounts set forth above; and polymerizing the homogenous mixture. Methods of using such plastics include: exposing the scintillating plastic to one or more extreme environmental conditions for a predetermined amount of time without generating crazing or fogging within the scintillating plastic. Various additional features and specific embodiments of these inventive concepts are also disclosed.
    Type: Application
    Filed: March 20, 2020
    Publication date: July 16, 2020
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Andrew M. Glenn, Andrew Neil Mabe, Stephen A. Payne
  • Patent number: 10647914
    Abstract: Scintillating plastics resistant to crazing and fogging, methods of making and using the same are disclosed. The scintillating plastics include: one or more primary polymers present in an amount ranging from about 40 wt % to about 95 wt %; one or more secondary polymers present in an amount ranging from about 1 wt % to about 60 wt %; and one or more fluors present in an amount ranging from about 0.1 wt % to about 50 wt %. Methods of making such plastics include: creating a homogenous mixture of precursor materials including primary polymer, secondary polymer, and fluor in the amounts set forth above; and polymerizing the homogenous mixture. Methods of using such plastics include: exposing the scintillating plastic to one or more extreme environmental conditions for a predetermined amount of time without generating crazing or fogging within the scintillating plastic. Various additional features and specific embodiments of these inventive concepts are also disclosed.
    Type: Grant
    Filed: March 17, 2017
    Date of Patent: May 12, 2020
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Andrew M. Glenn, Andrew Neil Mabe, Stephen A. Payne
  • Patent number: 10266761
    Abstract: In one embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 5 wt % or more; wherein the scintillator material exhibits an optical response signature for neutrons that is different than an optical response signature for gamma rays. In another embodiment, a scintillator material includes a polymer matrix comprising at least one of: polyvinyl xylene (PVX); polyvinyl diphenyl; and polyvinyl tetrahydronaphthalene; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount greater than 10 wt %. A total loading of dye in the scintillator material is sufficient to cause the scintillator material to exhibit a pulse-shape discrimination (PSD) figure of merit (FOM) of about at least 2.0.
    Type: Grant
    Filed: March 7, 2016
    Date of Patent: April 23, 2019
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Nerine Cherepy, Andrew M. Glenn, Sebastien Hamel, Stephen A. Payne, Benjamin L. Rupert
  • Publication number: 20180265775
    Abstract: Scintillating plastics resistant to crazing and fogging, methods of making and using the same are disclosed. The scintillating plastics include: one or more primary polymers present in an amount ranging from about 40 wt % to about 95 wt %; one or more secondary polymers present in an amount ranging from about 1 wt % to about 60 wt %; and one or more fluors present in an amount ranging from about 0.1 wt % to about 50 wt %. Methods of making such plastics include: creating a homogenous mixture of precursor materials including primary polymer, secondary polymer, and fluor in the amounts set forth above; and polymerizing the homogenous mixture. Methods of using such plastics include: exposing the scintillating plastic to one or more extreme environmental conditions for a predetermined amount of time without generating crazing or fogging within the scintillating plastic. Various additional features and specific embodiments of these inventive concepts are also disclosed.
    Type: Application
    Filed: March 17, 2017
    Publication date: September 20, 2018
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Andrew M. Glenn, Andrew Neil Mabe, Stephen A. Payne
  • Patent number: 9650564
    Abstract: A scintillator material according to one embodiment includes a polymer matrix; a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 3 wt % or more; and at least one component in the polymer matrix, the component being selected from a group consisting of B, Li, Gd, a B-containing compound, a Li-containing compound and a Gd-containing compound, wherein the scintillator material exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons and gamma rays. A system according to one embodiment includes a scintillator material as disclosed herein and a photodetector for detecting the response of the material to fast neutron, thermal neutron and gamma ray irradiation.
    Type: Grant
    Filed: May 14, 2012
    Date of Patent: May 16, 2017
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Michelle A. Faust, Andrew M. Glenn, H. Paul Martinez, Iwona A. Pawelczak, Stephen A. Payne, Keith E. Lewis
  • Patent number: 9429663
    Abstract: A composition of matter includes an organic molecule having a composition different than stilbene. The organic molecule is embodied as a crystal, and exhibits: an optical response signature for neutrons; an optical response signature for gamma rays, and performance comparable to or superior to stilbene in terms of distinguishing neutrons from gamma rays. The optical response signature for neutrons is different than the optical response signature for gamma rays.
    Type: Grant
    Filed: April 9, 2014
    Date of Patent: August 30, 2016
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Stephen A. Payne, Wolfgang Stoeffl, Natalia P. Zaitseva, Nerine J. Cherepy, M. Leslie Carman
  • Publication number: 20160186052
    Abstract: In one embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 5 wt % or more; wherein the scintillator material exhibits an optical response signature for neutrons that is different than an optical response signature for gamma rays. In another embodiment, a scintillator material includes a polymer matrix comprising at least one of: polyvinyl xylene (PVX); polyvinyl diphenyl; and polyvinyl tetrahydronaphthalene; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount greater than 10 wt %. A total loading of dye in the scintillator material is sufficient to cause the scintillator material to exhibit a pulse-shape discrimination (PSD) figure of merit (FOM) of about at least 2.0.
    Type: Application
    Filed: March 7, 2016
    Publication date: June 30, 2016
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Nerine Cherepy, Andrew M. Glenn, Sebastien Hamel, Stephen A. Payne, Benjamin L. Rupert
  • Patent number: 9309456
    Abstract: In one embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 5 wt % or more; wherein the scintillator material exhibits an optical response signature for neutrons that is different than an optical response signature for gamma rays. In another embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount greater than 10 wt %.
    Type: Grant
    Filed: April 2, 2012
    Date of Patent: April 12, 2016
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Nerine Cherepy, Andrew M. Glenn, Sebastien Hamel, Stephen A. Payne, Benjamin L. Rupert
  • Patent number: 9274237
    Abstract: In one embodiment, a scintillator includes a scintillator material; a primary fluor, and a Li-containing compound, where the Li-containing compound is soluble in the primary fluor, and where the scintillator exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons and gamma rays.
    Type: Grant
    Filed: April 15, 2014
    Date of Patent: March 1, 2016
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Michelle A. Faust, Andrew M. Glenn, H. Paul Martinez, Stephen A. Payne
  • Publication number: 20150028217
    Abstract: In one embodiment, a scintillator includes a scintillator material; a primary fluor, and a Li-containing compound, where the Li-containing compound is soluble in the primary fluor, and where the scintillator exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons and gamma rays.
    Type: Application
    Filed: April 15, 2014
    Publication date: January 29, 2015
    Applicant: Lawrence Livermore National Sercurity, LLC
    Inventors: Natalia P. Zaitseva, M. Leslie Carman, Michelle A. Faust, Andrew M. Glenn, H. Paul Martinez, Stephen A. Payne
  • Patent number: 8872125
    Abstract: An organic crystal according to one embodiment includes an organic crystal comprising diphenylacetylene and stilbene or a stilbene derivative, the crystal having physical characteristics of formation from solution, the organic crystal exhibiting a signal response signature for neutrons from a radioactive source. A system according to one embodiment includes an organic crystal comprising diphenylacetylene and stilbene or a stilbene derivative, the crystal having physical characteristics of formation from solution, the organic crystal exhibiting a signal response signature for neutrons from a radioactive source; and a photodetector for detecting the signal response of the organic crystal. Methods of making such crystals are also provided.
    Type: Grant
    Filed: May 22, 2012
    Date of Patent: October 28, 2014
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Natalia Zaitseva, M. Leslie Carman, Steve Payne
  • Publication number: 20140291532
    Abstract: A composition of matter includes an organic molecule having a composition different than stilbene. The organic molecule is embodied as a crystal, and exhibits: an optical response signature for neutrons; an optical response signature for gamma rays, and performance comparable to or superior to stilbene in terms of distinguishing neutrons from gamma rays. The optical response signature for neutrons is different than the optical response signature for gamma rays.
    Type: Application
    Filed: April 9, 2014
    Publication date: October 2, 2014
    Applicant: Lawrence Livermore National Security, LLC
    Inventors: Stephen A. Payne, Wolfgang Stoeffl, Natalia P. Zaitseva, Nerine J. Cherepy, M. Leslie Carman
  • Patent number: 8835865
    Abstract: A mixed organic crystal according to one embodiment includes a single mixed crystal having two compounds with different bandgap energies, the organic crystal having a physical property of exhibiting a signal response signature for neutrons from a radioactive source, wherein the signal response signature does not include a significantly-delayed luminescence characteristic of neutrons interacting with the organic crystal relative to a luminescence characteristic of gamma rays interacting with the organic crystal. According to one embodiment, an organic crystal includes bibenzyl and stilbene or a stilbene derivative, the organic crystal having a physical property of exhibiting a signal response signature for neutrons from a radioactive source.
    Type: Grant
    Filed: November 7, 2012
    Date of Patent: September 16, 2014
    Assignee: Lawrence Livermore National Security, LLC.
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Andrew M. Glenn, Sebastien Hamel, Robert Hatarik, Stephen A. Payne, Wolfgang Stoeffl
  • Patent number: 8815606
    Abstract: A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
    Type: Grant
    Filed: April 21, 2008
    Date of Patent: August 26, 2014
    Assignee: Lawrence Livermore National Security, LLC.
    Inventors: Philip F. Pagoria, Alexander R. Mitchell, Richard E. Whipple, M. Leslie Carman
  • Patent number: 8735843
    Abstract: A material according to one embodiment exhibits an optical response signature for neutrons that is different than an optical response signature for gamma rays, said material exhibiting performance comparable to or superior to stilbene in terms of distinguishing neutrons from gamma rays, wherein the material is not stilbene, the material comprising a molecule selected from a group consisting of: two or more benzene rings, one or more benzene rings with a carboxylic acid group, one or more benzene rings with at least one double bound adjacent to said benzene ring, and one or more benzene rings for which at least one atom in the benzene ring is not carbon.
    Type: Grant
    Filed: January 8, 2013
    Date of Patent: May 27, 2014
    Assignee: Lawrence Livermore National Security, LLC.
    Inventors: Stephen A. Payne, Wolfgang Stoeffl, Natalia P. Zaitseva, Nerine J. Cherepy, M. Leslie Carman
  • Publication number: 20140027646
    Abstract: In one embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 5 wt % or more; wherein the scintillator material exhibits an optical response signature for neutrons that is different than an optical response signature for gamma rays. In another embodiment, a scintillator material includes a polymer matrix; and a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount greater than 10 wt %.
    Type: Application
    Filed: April 2, 2012
    Publication date: January 30, 2014
    Applicant: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Nerine Cherepy, Andrew M. Glenn, Sebastien Hamel, Stephen A. Payne, Benjamin L. Rupert
  • Publication number: 20130299702
    Abstract: A scintillator material according to one embodiment includes a polymer matrix; a primary dye in the polymer matrix, the primary dye being a fluorescent dye, the primary dye being present in an amount of 3 wt % or more; and at least one component in the polymer matrix, the component being selected from a group consisting of B, Li, Gd, a B-containing compound, a Li-containing compound and a Gd-containing compound, wherein the scintillator material exhibits an optical response signature for thermal neutrons that is different than an optical response signature for fast neutrons and gamma rays. A system according to one embodiment includes a scintillator material as disclosed herein and a photodetector for detecting the response of the material to fast neutron, thermal neutron and gamma ray irradiation.
    Type: Application
    Filed: May 14, 2012
    Publication date: November 14, 2013
    Applicant: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
    Inventors: Natalia P. Zaitseva, M Leslie Carman, Michelle A. Faust, Andrew M. Glenn, H. Paul Martinez, Iwona A. Pawelczak, Stephen A. Payne, Keith E. Lewis