Patents by Inventor Martin Koestner
Martin Koestner has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 10766847Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: GrantFiled: October 16, 2018Date of Patent: September 8, 2020Assignee: RÖHM GMBHInventors: Steffen Krill, Torsten Balduf, Martin Koestner, Matthias Groemping, Alexander Lygin, Rudolf Burghardt
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Patent number: 10457626Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: GrantFiled: October 16, 2018Date of Patent: October 29, 2019Assignee: EVONIK ROEHM GmbHInventors: Steffen Krill, Torsten Balduf, Martin Koestner, Matthias Groemping, Alexander Lygin, Rudolf Burghardt
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Patent number: 10273201Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: GrantFiled: October 27, 2017Date of Patent: April 30, 2019Assignee: EVONIK RÖHM GmbHInventors: Steffen Krill, Torsten Balduf, Martin Koestner, Matthias Groemping, Alexander Lygin, Rudolf Burghardt
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Publication number: 20190112255Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: ApplicationFiled: October 16, 2018Publication date: April 18, 2019Applicant: Evonik Roehm GmbHInventors: Steffen KRILL, Torsten BALDUF, Martin KOESTNER, Matthias GROEMPING, Alexander LYGIN, Rudolf BURGHARDT
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Publication number: 20190077742Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: ApplicationFiled: October 16, 2018Publication date: March 14, 2019Applicant: Evonik Roehm GmbHInventors: Steffen KRILL, Torsten BALDUF, Martin KOESTNER, Matthias GROEMPING, Alexander LYGIN, Rudolf BURGHARDT
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Patent number: 9994507Abstract: The present invention relates to an optimized process for the preparation of methacrolein. Methacrolein is used in chemical synthesis particularly as an intermediate for the preparation of methacrylic acid, methyl methacrylate or even active ingredients, fragrances or flavorings. In particular the present invention relates to the optimization of the process parameters by which, inter alia, a reduction of the content of harmful dimeric methacrolein in the end product may be achieved.Type: GrantFiled: September 16, 2015Date of Patent: June 12, 2018Assignee: Evonik Roehm GmbHInventors: Rudolf Burghardt, Steffen Krill, Torsten Balduf, Gerhard Koelbl, Martin Koestner, Eduard Rundal
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Publication number: 20180050977Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: ApplicationFiled: October 27, 2017Publication date: February 22, 2018Applicant: Evonik Roehm GmbHInventors: Steffen Krill, Torsten Balduf, Martin Koestner, Matthias Groemping, Alexander Lygin, Rudolf Burghardt
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Patent number: 9890105Abstract: The present invention relates to a process for producing methyl methacrylate, comprising the following steps: A) producing methacrolein and B) reacting the methacrolein obtained in step A) in an oxidative esterification reaction to give methyl methacrylate, characterized in that the two steps A) and B) take place in a liquid phase at a pressure of from 2 to 100 bar, and step B) is carried out in the presence of a heterogeneous noble-metal-containing catalyst comprising metals and/or comprising metal oxides.Type: GrantFiled: April 11, 2014Date of Patent: February 13, 2018Assignee: EVONIK ROEHM GmbHInventors: Steffen Krill, Torsten Balduf, Martin Koestner, Matthias Groemping, Alexander Lygin, Rudolf Burghardt
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Publication number: 20170275227Abstract: The present invention relates to an optimized process for the preparation of methacrolein. Methacrolein is used in chemical synthesis particularly as an intermediate for the preparation of methacrylic acid, methyl methacrylate or even active ingredients, fragrances or flavourings. In particular the present invention relates to the optimization of the process parameters by which, inter alia, a reduction of the content of harmful dimeric methacrolein in the end product may be achieved.Type: ApplicationFiled: September 16, 2015Publication date: September 28, 2017Applicant: Evonik Röhm GmbHInventors: Rudolf BURGHARDT, Steffen KRILL, Torsten BALDUF, Gerhard KOELBL, Martin KOESTNER, Eduard RUNDAL
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Publication number: 20170101322Abstract: The present invention describes a method of removing ammonia from alcoholic solution in the presence of carbonic acid compounds while avoiding fouling by supplying the solution to be separated to the upper part of a distillation column and adjusting the temperature at the introduction point such that the ammonium salts of the carbonic acid compound in question are soluble in the in question at the top of the distillation column under the operating conditions.Type: ApplicationFiled: March 13, 2015Publication date: April 13, 2017Applicant: Evonik Roehm GmbHInventors: Alexander MAY, Willi PLOESSER, Markus Rolf ROSSMEISSL, Steffen KRILL, Martin KOESTNER
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Patent number: 9428437Abstract: The present invention describes a process for preparing alpha-beta-unsaturated carboxylic acids by dehydration of hydroxycarboxylic or alkoxycarboxylic acids which are substituted in the alpha position, in particular 2-hydroxyisobutyric acid, while avoiding accumulation of by-products and additives.Type: GrantFiled: April 28, 2014Date of Patent: August 30, 2016Assignee: EVONIK ROEHM GmbHInventors: Alexander May, Steffen Krill, Joerg Becker, Willi Ploesser, Marcel Treskow, Martin Koestner
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Publication number: 20160137583Abstract: The present invention relates to a process for the production of alpha-hydroxycarboxylic esters by means of alcoholysis of the corresponding alpha-hydroxycarboxamide under heterogeneous catalysis.Type: ApplicationFiled: July 3, 2014Publication date: May 19, 2016Applicant: EVONIK ROHM GMBHInventors: Steffen KRILL, Alexander MAY, Joerg BECKER, Martin KOESTNER
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Publication number: 20160090344Abstract: The present invention describes a process for preparing alpha-beta-unsaturated carboxylic acids by dehydration of hydroxycarboxylic or alkoxycarboxylic acids which are substituted in the alpha position, in particular 2-hydroxyisobutyric acid, while avoiding accumulation of by-products and additives.Type: ApplicationFiled: April 28, 2014Publication date: March 31, 2016Applicant: EVONIK ROEHM GmbHInventors: Alexander MAY, Steffen KRILL, Joerg BECKER, Willi PLOESSER, Marcel TRESKOW, Martin KOESTNER
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Patent number: 8975440Abstract: The invention relates to a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid, comprising the steps of A) reacting a carbonyl compound with hydrocyanic acid to produce a hydroxycarboxylic acid nitrile, B) hydrolysis of the hydroxycarboxylic acid nitrile obtained in step A) in the presence of a catalyst comprising manganese dioxide, wherein a molar excess of carbonyl compound is used in relation to the hydrocyanic acid to react the carbonyl compound with hydrocyanic acid according to step A), and the reaction mixture obtained in step A) is not purified by distillation before the hydrolysis according to step B) is carried out. The invention furthermore relates to a method for producing alkyl(meth)acrylates from polymers, moulding compounds and moulded bodies, wherein a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid is carried out in accordance with the method described above.Type: GrantFiled: October 29, 2009Date of Patent: March 10, 2015Assignee: Evonik Roehm GmbHInventors: Alexander May, Martin Koestner, Joerg Becker, Joerg Schallenberg, Hermann Siegert, Bernd Vogel
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Publication number: 20140187817Abstract: The invention relates to a process for preparation of methacrylic acid, comprising process steps a) providing a crude methacrylic acid-comprising aqueous solution comprising at least one impurity at least partially dissolved therein; b) precipitation of at least a part of the at least one impurity from the crude methacrylic acid-comprising aqueous solution to form at least one solid impurity and a mother liquor; c) separation of at least a part of the at least one solid impurity from the mother liquor to obtain a purified methacrylic acid-comprising aqueous solution and a solid impurity; d) separation of methacrylic acid from the purified methacrylic acid-comprising aqueous solution.Type: ApplicationFiled: September 16, 2011Publication date: July 3, 2014Applicant: Evonik Roehm GmbHInventors: Torsten Balduf, Martin Koestner, Wenxing Zhang, Heidi Groen, Axel Hengstermann, Maya Krapfl
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Publication number: 20140135521Abstract: The present invention relates to a continuous process for preparing alpha-hydroxycarboxylic esters by reacting at least one alpha-hydroxycarboxamide present in the liquid phase with an alcohol in the presence of a catalyst, which is characterized in that the resulting alpha-hydroxycarboxylic ester is at least partly separated from the reaction mixture via the gas phase.Type: ApplicationFiled: July 3, 2012Publication date: May 15, 2014Applicant: Evonik Roehm GmbHInventors: Martin Koestner, Willi Ploesser, Alexander May
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Patent number: 8426637Abstract: The present invention relates to a process for preparation of pure methacrylic acid, at least comprising the process steps: a) gas phase oxidation of a C4 compound to obtain a methacrylic acid-comprising gas phase, b) condensation of the methacrylic acid-comprising gas phase to obtain an aqueous methacrylic acid solution, c) separation of at least a part of the methacrylic acid from the aqueous methacrylic acid solution to obtain at least one crude methacrylic acid-comprising product; d) separation of at least a part of the methacrylic acid from the at least one crude methacrylic acid-comprising product by means of a thermal separation process to obtain a pure methacrylic acid.Type: GrantFiled: November 17, 2008Date of Patent: April 23, 2013Assignee: Evonik Röhm GmbHInventors: Martin Koestner, Gerhard Koelbl, Ralf Meier
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Publication number: 20120232305Abstract: The invention relates to a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid, comprising the steps of A) reacting a carbonyl compound with hydrocyanic acid to produce a hydroxycarboxylic acid nitrile, B) hydrolysis of the hydroxycarboxylic acid nitrile obtained in step A) in the presence of a catalyst comprising manganese dioxide, wherein a molar excess of carbonyl compound is used in relation to the hydrocyanic acid to react the carbonyl compound with hydrocyanic acid according to step A), and the reaction mixture obtained in step A) is not purified by distillation before the hydrolysis according to step B) is carried out. The invention furthermore relates to a method for producing alkyl(meth)acrylates from polymers, moulding compounds and moulded bodies, wherein a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid is carried out in accordance with the method described above.Type: ApplicationFiled: October 29, 2009Publication date: September 13, 2012Applicant: EVONIK ROEHM GmbHInventors: Alexander MAY, Martin KOESTNER, Joerg BECKER, Joerg SCHALLENBERG, Hermann SIEGERT, Bernd VOGEL
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Publication number: 20110306784Abstract: The invention relates to a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid, comprising the steps of A) reacting a carbonyl compound with hydrocyanic acid to produce a hydroxycarboxylic acid nitrile, B) hydrolysis of the hydroxycarboxylic acid nitrile obtained in step A) in the presence of a catalyst comprising manganese dioxide, wherein a molar excess of carbonyl compound is used in relation to the hydrocyanic acid to react the carbonyl compound with hydrocyanic acid according to step A), and the reaction mixture obtained in step A) is not purified by distillation before the hydrolysis according to step B) is carried out. The invention furthermore relates to a method for producing alkyl(meth)acrylates from polymers, moulding compounds and moulded bodies, wherein a method for producing a carboxylic acid amide from a carbonyl compound and hydrocyanic acid is carried out in accordance with the method described above.Type: ApplicationFiled: October 29, 2009Publication date: December 15, 2011Applicant: EVONIK ROEHM GMBHInventors: Alexander May, Martin Koestner, Joerg Becker, Joerg Schallenberg, Hermann Siegert, Bernd Vogel
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Publication number: 20100273970Abstract: The present invention relates to a process for preparation of pure methacrylic acid, at least comprising the process steps: a) gas phase oxidation of a C4 compound to obtain a methacrylic acid-comprising gas phase, b) condensation of the methacrylic acid-comprising gas phase to obtain an aqueous methacrylic acid solution, c) separation of at least a part of the methacrylic acid from the aqueous methacrylic acid solution to obtain at least one crude methacrylic acid-comprising product; d) separation of at least a part of the methacrylic acid from the at least one crude methacrylic acid-comprising product by means of a thermal separation process to obtain a pure methacrylic acid.Type: ApplicationFiled: November 17, 2008Publication date: October 28, 2010Applicant: EVONIK ROEHM GMBHInventors: Martin Koestner, Gerhard Koelbl, Ralf Meier