Abstract: A method for managing and controlling nitrogen emission from a cyclic liquor flow system in a pulp mill (1), the pulp mill (1) comprising a recovery system (20) for recovering heat and chemicals from a pulping process (30), the recovery system (20) comprising a recovery boiler (8) and a nitrogen oxide scrubber (15), the nitrogen oxide scrubber (15) being arranged to remove nitrogen oxide from flue gas (16) from the recovery boiler (8), the method comprising the steps of: —exposing flue gas (16) from the recovery oiler (8) to an oxidizing agent, thereby oxidising nitrogen oxide in the flue gas (16) to higher nitrogen oxides; —contacting the flue gas (16) with an alkaline aqueous scrubber liquid (17) in the nitrogen oxide scrubber (15), thereby absorbing the nitrogen oxides in the scrubber liquid (17) and producing a nitrogen containing scrubber liquid (17); —introducing all or a part of the nitrogen containing scrubber liquid (17) into the cyclic liquor flow system.

Abstract: The method is for separation of lignin from original black liquor (BLIN) having a first precipitation phase (PR1/PR2) for precipitation of lignin by a first acidification using acidifier, CO2, at alkaline conditions, then separating a lignin cake with subsequent suspension of the lignin cake in a strong acid to leach our metals from the lignin followed by dewatering and obtaining a clean lignin product LP. The acidic liquid phase (FL1) subjected to a sulphur removal process wherein a calcium containing compound is added to the acidic liquid phase, whereby sulphur in the acidic liquid phase is reacting with the calcium compound forming solid gypsum which could be separated and bled off from the process. The remaining acidic liquid could then be returned to the recovery process without negatively affecting the sulphur balance of the mill.

Abstract: The method is for separation of lignin from original black liquor (BLIN) having the following phases in sequence; a first precipitation phase (PR1) for precipitation of lignin by a first acidification of the original black liquor by adding a first acid or mixture of acids (G1a); followed by a second precipitation phase (PR2) for precipitation of lignin by a further acidification of the original black liquor by adding a second acid or mixture of acids (G1b). The first phase is implemented to lower the pH while avoiding any larger amount of precipitation, i.e. less than 2-5%, while the second phase is implemented in order to obtain the larger part of the precipitation. In total is 40-70% of the total lignin content of the original black liquor precipitated while the residual black liquor after precipitation is still strongly alkaline.

Abstract: The method is for separation of lignin from original black liquor (BLIN) and has the following phases in sequence. A first precipitation phase (PR1) for precipitation of lignin by a first acidification of the original black liquor by adding a first acid or mixture of acids (G1a) followed by a first storage phase wherein precipitated lignin particles are allowed to increase in size, followed by a second precipitation phase (PR2) for precipitation of lignin by a further acidification of the original black liquor by adding a second acid or mixture of acids (G1b). By retaining the acidified black liquor for at least 25 minutes in the storage phase are the precipitated lignin particles allowed to grow in size and the filterability is improved considerably.

Abstract: The method is for separation of lignin from original black liquor. Lignin is precipitated in a first acidification stage followed by dewatering a first lignin suspension while forming a first filter cake. The first lignin filter cake is suspended in a second acidification stage whereupon a second lignin suspension is obtained. The second lignin suspension is dewatered to form a second filter cake. The second filter cake is washed and the washed second lignin cake is dewatered to obtain a lignin product. Waste gases from the second acidification stage is recirculated back to the first acidification stage and mixed with the original black liquor.

Abstract: The method is for separation of lignin from original black liquor (BLIN) and has the following phases in sequence. A first precipitation phase (PR1) for precipitation of lignin by a first acidification of the original black liquor by adding a first acid or mixture of acids (G1a) followed by a first storage phase wherein precipitated lignin particles are allowed to increase in size, followed by a second precipitation phase (PR2) for precipitation of lignin by a further acidification of the original black liquor by adding a second acid or mixture of acids (G1b). By retaining the acidified black liquor for at least 25 minutes in the storage phase are the precipitated lignin particles allowed to grow in size and the filterability is improved considerably.

Abstract: The method is for separation of lignin from original black liquor (BLIN) having a first precipitation phase (PR1/PR2) for precipitation of lignin by a first acidification using acidifier, CO2, at alkaline conditions, then separating a lignin cake with subsequent suspension of the lignin cake in a strong acid to leach our metals from the lignin followed by dewatering and obtaining a clean lignin product LP. The acidic liquid phase (FL1) subjected to a sulphur removal process wherein a calcium containing compound is added to the acidic liquid phase, whereby sulphur in the acidic liquid phase is reacting with the calcium compound forming solid gypsum which could be separated and bled off from the process. The remaining acidic liquid could then be returned to the recovery process without negatively affecting the sulphur balance of the mill.

Abstract: The method is for separation of lignin from original black liquor (BLIN) having the following phases in sequence; a first precipitation phase (PR1) for precipitation of lignin by a first acidification of the original black liquor by adding a first acid or mixture of acids (G1a); followed by a second precipitation phase (PR2) for precipitation of lignin by a further acidification of the original black liquor by adding a second acid or mixture of acids (G1b). The first phase is implemented to lower the pH while avoiding any larger amount of precipitation, i.e. less than 2-5%, while the second phase is implemented in order to obtain the larger part of the precipitation. In total is 40-70% of the total lignin content of the original black liquor precipitated while the residual black liquor after precipitation is still strongly alkaline.

Abstract: The method is for separation of lignin from original black liquor. Lignin is precipitated in a first acidification stage followed by dewatering a first lignin suspension while forming a first filter cake. The first lignin filter cake is suspended in a second acidification stage whereupon a second lignin suspension is obtained. The second lignin suspension is dewatered to form a second filter cake. The second filter cake is washed and the washed second lignin cake is dewatered to obtain a lignin product. Waste gases from the second acidification stage is recirculated back to the first acidification stage and mixed with the original black liquor.

Abstract: Ash from a recovery boiler is purified by leaching or evaporation-crystallizing contaminants such as, chlorides and potassium salts in water. The leaching or evaporation-crystallizing takes place in an aqueous solution at a temperature that is in the vicinity of the boiling point of the aqueous solution. The leached or evaporation-crystallized ash is returned to the black liquor or to the recovery boiler while the leaching water or the evaporation-crystallization water is then cooled to less than 32.degree. C., preferably 10-15.degree. C. Sodium sulphate containing crystallization water, such as sodium sulphate heptahyfdrate or sodium sulphate decahydrate, is crystallized out and then separated to be reintroduced into the black liquor, directly into the recovery boiler or into the leaching solution or evaporation-crystallization solution.

Abstract: The invention relates to a process for producing polysulphide by means of oxidizing sulphide in spent liquors from kraft cellulose cooking. The process is characterized in that green liquor is firstly enriched in sulphide and then oxidized.

Abstract: A filtering apparatus comprises: a pressure vessel; a plurality of filter elements arranged within the pressure vessel, the filter elements each having an upper end, a lower end and a side wall; filling bodies positioned within the filter elements; a first conduit for introducing compressed gas into the pressure vessel; a second conduit for transporting unfiltered liquid to and from the pressure vessel; and a third conduit for removing filtrate from the pressure vessel and transporting back-flushing liquid to and from the filter elements, the third conduit positioned proximate to a bottom portion of the pressure vessel and attached to the lower ends of the filter elements, such that the third conduit provides a support structure for the filter elements and the back-flushing liquid introduced via the third conduit fills the filter elements in a direction from the lower ends toward the upper ends, the volume of back-flushing liquid introduced into the filter elements limited by the filling bodies.

Abstract: The invention relates to a method for lime sludge reburning in a fluidizing bed. The method is characterized in that a cooling medium (10) is injected immediately above the fluidizing bed (3). The invention also comprises means for performing the method. The arrangement which is known per se is provided with an injection device (10) for a cooling medium above the fluidizing bed (3).