Patents by Inventor Mazen Khaled

Mazen Khaled has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20250249493
    Abstract: A method for removing polycyclic aromatic hydrocarbons from a sample includes contacting the sample with a bacterial strain for a time sufficient to degrade at least one polycyclic aromatic hydrocarbon. The sample includes coronene at a first concentration, and the bacterial strain is Halomonas caseinilytica. The method further includes degrading at least one polycyclic aromatic hydrocarbon and further collecting a product containing coronene at a second concentration that is lower than the first concentration.
    Type: Application
    Filed: February 2, 2024
    Publication date: August 7, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Alexis NZILA, Ajibola Hakeem OKEYODE, Assad AL-THUKAIR, Musa M. MUSA, Mazen Khaled Hamed NAZAL
  • Publication number: 20250208007
    Abstract: A sampler system for water contaminants. The sampler system includes an adsorptive sampler housed within a cylindrical enclosure, which has a top face, a bottom face and a cylindrical surface. The cylindrical surface of the sampler system is fluid-permeable. A cable connects the top face of the cylindrical enclosure to a flotation device. A spring connects the adsorptive sampler to the bottom face of the cylindrical enclosure. The adsorptive sampler incudes a housing having a cavity and an adsorptive material disposed inside the cavity. The housing is attached to the spring and includes a front face and a back face. The spring is a cantilever in the form of a rigid film, wherein the rigid film is connected to the bottom face of the cylindrical enclosure along a flat edge of the rigid film.
    Type: Application
    Filed: March 10, 2025
    Publication date: June 26, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Nabeel Saeed Fuad ABUZAID, Muhammad HAWWA, Mazen Khaled NAZAL
  • Patent number: 12276582
    Abstract: A sampler system for water contaminants. The sampler system includes an adsorptive sampler housed within a cylindrical enclosure, which has a top face, a bottom face and a cylindrical surface. The cylindrical surface of the sampler system is fluid-permeable. A cable connects the top face of the cylindrical enclosure to a flotation device. A spring connects the adsorptive sampler to the bottom face of the cylindrical enclosure. The adsorptive sampler includes a housing having a cavity and an adsorptive material disposed inside the cavity. The housing is attached to the spring and includes a front face and a back face. The spring is a cantilever in the form of a rigid film, wherein the rigid film is connected to the bottom face of the cylindrical enclosure along a flat edge of the rigid film.
    Type: Grant
    Filed: January 9, 2023
    Date of Patent: April 15, 2025
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Nabeel Saeed Fuad Abuzaid, Muhammad Hawwa, Mazen Khaled Nazal
  • Publication number: 20250114748
    Abstract: A membrane-based inverted liquid-liquid extraction method for extracting an analyte from an unsupported aqueous liquid sample includes sealing the unsupported aqueous liquid sample in a porous membrane bag, immersing the porous membrane bag in an organic solvent, and extracting the analyte from the unsupported aqueous liquid sample to produce an extract within the organic solvent. The unsupported aqueous liquid sample is immiscible with the organic solvent. The porous membrane bag does not contain a solid sorbent.
    Type: Application
    Filed: October 6, 2023
    Publication date: April 10, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Muhammad SAJID, Mazen Khaled NAZAL, Durga Rao GIJJAPU
  • Publication number: 20250110099
    Abstract: A membrane-biochar strip for water sampling includes two porous polymeric membrane sheets having the same dimension. The two porous polymeric membrane sheets have an average pore size of about 50 to 150 micrometers (?m). Seagrass biochar (SGBC) particles are disposed between two porous polymeric membrane sheets resulting in a sandwich structure. An edge of the sandwich structure is sealed, and the SGBC particles are encapsulated in the membrane-biochar strip. The SGBC particles have an average particle size of about 150 to 400 ?m. The seagrass biochar (SGBC) particles are prepared from Halodule Uninervis seagrass.
    Type: Application
    Filed: October 3, 2023
    Publication date: April 3, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled NAZAL, Nabeel Saeed Fuad ABUZAID, Durga Rao GIJJAPU
  • Publication number: 20250076161
    Abstract: A sampler system includes an enclosure having a top, a bottom and a sidewall that is fluid permeable. The sampler system further includes a sampler apparatus housed within the enclosure. The sampler apparatus includes a sampling component having a support structure and an adsorbent. The sampler apparatus further includes an oscillating component including a spring which connects the sampling component to the bottom of the enclosure. A retaining component includes a first magnet attached to the sampling component and a second magnet separated from the first magnet by a gap.
    Type: Application
    Filed: August 29, 2023
    Publication date: March 6, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Nabeel Saeed Fuad ABUZAID, Muhammad HAWWA, Mazen Khaled NAZAL
  • Patent number: 12187936
    Abstract: A method for synthesizing carbon quantum dots (CQDs) including reacting a mixture of macroalgae and ethanol hydrothermally in an autoclave at a reaction temperature between 150 degrees Celsius (° C.) and 250° C. to form a suspension. The method further includes separating the CQDs from the suspension. The CQDs have a size of 1 to 5 nanometers (nm). The CQDs have a Stokes shift of at least 80 nm at an excitation wavelength of 270-410 nm.
    Type: Grant
    Filed: August 22, 2024
    Date of Patent: January 7, 2025
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Firoz Khan, Masoud Al-Rasheidi, Mazen Khaled Nazal
  • Patent number: 12187937
    Abstract: A method for synthesizing carbon quantum dots (CQDs) including reacting a mixture of macroalgae and ethanol hydrothermally in an autoclave at a reaction temperature between 150 degrees Celsius (° C.) and 250° C. to form a suspension. The method further includes separating the CQDs from the suspension. The CQDs have a size of 1 to 5 nanometers (nm). The CQDs have a Stokes shift of at least 80 nm at an excitation wavelength of 270-410 nm.
    Type: Grant
    Filed: August 22, 2024
    Date of Patent: January 7, 2025
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Firoz Khan, Masoud Al-Rasheidi, Mazen Khaled Nazal
  • Patent number: 12187938
    Abstract: A method for synthesizing carbon quantum dots (CQDs) including reacting a mixture of macroalgae and ethanol hydrothermally in an autoclave at a reaction temperature between 150 degrees Celsius (° C.) and 250° C. to form a suspension. The method further includes separating the CQDs from the suspension. The CQDs have a size of 1 to 5 nanometers (nm). The CQDs have a Stokes shift of at least 80 nm at an excitation wavelength of 270-410 nm.
    Type: Grant
    Filed: August 22, 2024
    Date of Patent: January 7, 2025
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Firoz Khan, Masoud Al-Rasheidi, Mazen Khaled Nazal
  • Patent number: 12116515
    Abstract: A method for synthesizing carbon quantum dots (CQDs) including reacting a mixture of macroalgae and ethanol hydrothermally in an autoclave at a reaction temperature between 150 degrees Celsius (° C.) and 250° C. to form a suspension. The method further includes separating the CQDs from the suspension. The CQDs have a size of 1 to 5 nanometers (nm). The CQDs have a Stokes shift of at least 80 nm at an excitation wavelength of 270-410 nm.
    Type: Grant
    Filed: June 18, 2024
    Date of Patent: October 15, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Firoz Khan, Masoud Al-Rasheidi, Mazen Khaled Nazal
  • Publication number: 20240230478
    Abstract: A sampler system for water contaminants. The sampler system includes an adsorptive sampler housed within a cylindrical enclosure, which has a top face, a bottom face and a cylindrical surface. The cylindrical surface of the sampler system is fluid-permeable. A cable connects the top face of the cylindrical enclosure to a flotation device. A spring connects the adsorptive sampler to the bottom face of the cylindrical enclosure. The adsorptive sampler includes a housing having a cavity and an adsorptive material disposed inside the cavity. The housing is attached to the spring and includes a front face and a back face. The spring is a cantilever in the form of a rigid film, wherein the rigid film is connected to the bottom face of the cylindrical enclosure along a flat edge of the rigid film.
    Type: Application
    Filed: January 9, 2023
    Publication date: July 11, 2024
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Nabeel Saeed Fuad ABUZAID, Muhammad HAWWA, Mazen Khaled NAZAL
  • Patent number: 11851598
    Abstract: Methods for preventing, inhibiting, or reducing metal (e.g. mild steel) corrosion in aqueous media utilizing a water-soluble formulation having a polyurea pre-dissolved in a polar aprotic solvent are described. The polyurea contains reacted units of a diisocyanate and a diaminoalkane. The effectiveness of the methods is demonstrated by corrosion inhibition efficiency and corrosion rate of metallic substrates in aqueous acidic environments using the water-soluble formulation.
    Type: Grant
    Filed: May 27, 2022
    Date of Patent: December 26, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Ismail Abdulazeez, Othman Al-Hamouz, Abdulaziz Al-Saadi, Mazen Khaled
  • Patent number: 11753590
    Abstract: Methods for preventing, inhibiting, or reducing metal (e.g. mild steel) corrosion in aqueous media utilizing a water-soluble formulation having a polyurea pre-dissolved in a polar aprotic solvent are described. The polyurea contains reacted units of a diisocyanate and a diaminoalkane. The effectiveness of the methods is demonstrated by corrosion inhibition efficiency and corrosion rate of metallic substrates in aqueous acidic environments using the water-soluble formulation.
    Type: Grant
    Filed: May 27, 2022
    Date of Patent: September 12, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Ismail Abdulazeez, Othman Al-Hamouz, Abdulaziz Al-Saadi, Mazen Khaled
  • Patent number: 11684905
    Abstract: A biochar-derived adsorbent preferably from Sargassum boveanum, macroalgae can be used for removing phenolic compounds, such as 2,4,6-trichlorophenol and 2,4-dimethylphenol, from aqueous solutions. The carbonization can improve the removal capability of the macroalgae adsorbent for such phenolic compounds with removal efficiencies of 60% or more from high salinity seawater and 100% from distilled water. The adsorption may occur through a mixed mechanism dominated by physisorption following pseudo second-order kinetics. The adsorption of the phenolic molecules may be spontaneous, endothermic and thermodynamically favorable.
    Type: Grant
    Filed: April 12, 2022
    Date of Patent: June 27, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled Nazal, Nabeel Saeed Abuzaid
  • Patent number: 11517876
    Abstract: A method of forming an activated carbon sorbent from a seagrass. The method involves treating a seagrass with a base solution to form an intermediate solid, drying the intermediate solid to form a precursor, and pyrolyzing the precursor at 600 to 1000° C. to form the activated carbon sorbent. Preferably the seagrass is Halodule uninervis. The activated carbon sorbent is used in a method of removing an organic pollutant from a contaminated water. Preferred organic pollutants removed are phenols, specifically 2,4-dimethylphenol and 2,4-dichlorophenol.
    Type: Grant
    Filed: May 11, 2022
    Date of Patent: December 6, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled Nazal, Nabeel Saeed Abuzaid
  • Patent number: 11512400
    Abstract: A method and an electrocatalytic electrode for electrochemically reducing carbon dioxide to methanol are provided. An exemplary electrocatalytic electrode includes copper (I) oxide crystals electrodeposited over an atomically smooth copper electrode.
    Type: Grant
    Filed: December 10, 2020
    Date of Patent: November 29, 2022
    Assignees: Saudi Arabian Oil Company, King Fahd University of Petroleum & Minerals
    Inventors: Fayez Nasir Al-Rowaili, Mazen Khaled, Aqil Jamal, Sagheer A. Onaizi, Umer Zahid
  • Patent number: 11504694
    Abstract: A biochar-derived adsorbent preferably from Sargassum boveanum, macroalgae can be used for removing phenolic compounds, such as 2,4,6-trichlorophenol and 2,4-dimethylphenol, from aqueous solutions. The carbonization can improve the removal capability of the macroalgae adsorbent for such phenolic compounds with removal efficiencies of 60% or more from high salinity seawater and 100% from distilled water. The adsorption may occur through a mixed mechanism dominated by physisorption following pseudo second-order kinetics. The adsorption of the phenolic molecules may be spontaneous, endothermic and thermodynamically favorable.
    Type: Grant
    Filed: January 23, 2020
    Date of Patent: November 22, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled Nazal, Nabeel Saeed Abuzaid
  • Patent number: 11447887
    Abstract: A method for forming an atomically smooth surface on a copper electrode through electropolishing and the atomically smooth surface are provided. An exemplary method for forming an atomically smooth surface by electropolishing includes placing a copper foil in an electrolyte solution including ethylene glycol and phosphoric acid. The copper foil is coupled to a current source. Current is applied to the copper foil to electropolish the copper foil. The electropolishing is stopped when the electropolishing is completed.
    Type: Grant
    Filed: December 10, 2020
    Date of Patent: September 20, 2022
    Assignees: Saudi Arabian Oil Company, King Fahd University of Petroleum & Minerals
    Inventors: Fayez Nasir Al-Rowaili, Mazen Khaled, Aqil Jamal, Sagheer A. Onaizi, Umer Zahid
  • Patent number: 11414764
    Abstract: A method of inhibiting corrosion of metal in contact with a corrosive medium in an oil or gas field environment, whereby a formulation containing a polyurea is introduced into the corrosive medium in contact with the metal, wherein the polyurea is formed from a polymerization reaction between a piperazine having at least two reactive amine groups and a diisocyanate. The polyurea is introduced into the corrosive medium at a concentration of 1 to 250 ppm.
    Type: Grant
    Filed: October 16, 2019
    Date of Patent: August 16, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled, Abdulaziz A. Al-Saadi, Ismail Abdulazeez, Othman Al-Hamouz
  • Publication number: 20220250030
    Abstract: A biochar-derived adsorbent preferably from Sargassum boveanum, macroalgae can be used for removing phenolic compounds, such as 2,4,6-trichlorophenol and 2,4-dimethylphenol, from aqueous solutions. The carbonization can improve the removal capability of the macroalgae adsorbent for such phenolic compounds with removal efficiencies of 60% or more from high salinity seawater and 100% from distilled water. The adsorption may occur through a mixed mechanism dominated by physisorption following pseudo second-order kinetics. The adsorption of the phenolic molecules may be spontaneous, endothermic and thermodynamically favorable.
    Type: Application
    Filed: April 12, 2022
    Publication date: August 11, 2022
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mazen Khaled NAZAL, Nabeel Saeed ABUZAID