Patents by Inventor Michael D. Irwin

Michael D. Irwin has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 12540228
    Abstract: A method for producing a perovskite material photovoltaic device, the method comprising: depositing a layer comprising a fullerene or fullerene derivative on a perovskite material; depositing a cross-linking agent on the perovskite material or the layer comprising the fullerene or fullerene derivative, wherein the cross-linking agent comprises a silane, wherein the silane is a halosilyalkane; and depositing one or more polymers on the perovskite material or the layer comprising the fullerene or fullerene derivative.
    Type: Grant
    Filed: December 6, 2023
    Date of Patent: February 3, 2026
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Kamil Mielczarek, Nicholas Charles Anderson
  • Publication number: 20260008930
    Abstract: A method for preparing photoactive perovskite materials. The method comprises the steps of: introducing a lead halide and a first solvent to a first vessel and contacting the lead halide with the first solvent to dissolve the lead halide to form a lead halide solution, introducing a Group 1 metal halide a second solvent into a second vessel and contacting the Group 1 metal halide with the second solvent to dissolve the Group 1 metal halide to form a Group 1 metal halide solution, and contacting the lead halide solution with the Group 1 metal halide solution to form a thin-film precursor ink. The method further comprises depositing the thin-film precursor ink onto a substrate, drying the thin-film precursor ink to form a thin film, annealing the thin film; and rinsing the thin film with a salt solution.
    Type: Application
    Filed: September 12, 2025
    Publication date: January 8, 2026
    Inventors: Michael D. Irwin, Kamil Mielczarek, Vivek V. Dhas
  • Publication number: 20250289998
    Abstract: A method including forming a lead halide precursor ink comprising a group 1 metal halide, a lead halide, an ionic liquid, and a solvent; depositing the lead halide precursor ink onto a substrate; drying the lead halide precursor ink to form a lead halide film; and annealing the lead halide film.
    Type: Application
    Filed: March 20, 2025
    Publication date: September 18, 2025
    Inventors: Michael D. Irwin, Xiao-Xin Gao, Zhaofu Fei, Paul J. Dyson, Mohammad Khaja Nazeeruddin
  • Publication number: 20250263848
    Abstract: Particular embodiments described herein provide for a synthetic fuel creation system. The synthetic fuel creation system includes a syngas creation station to create syngas, a crude creation station to create heavy syncrude, and a crude cracking station to convert the heavy syncrude into synthetic fuel. The synthetic fuel creation system can use an electrocatalysis system to create the syngas and the electrocatalysis system can include an anode, a cathode, oxygen evolution reaction catalysts, hydrogen/carbon monoxide evolution reaction catalysts, and an electrolyte, where the hydrogen/carbon monoxide evolution reaction catalysts include a graphitic carbon nitride.
    Type: Application
    Filed: August 26, 2024
    Publication date: August 21, 2025
    Inventors: Michael D. Irwin, Michael Graetzel, Jing Gao, Pablo Jiménez-Calvo, Senthilkumar Pachamuthu
  • Patent number: 12359122
    Abstract: A method including forming a lead halide precursor ink comprising a group 1 metal halide, a lead halide, an ionic liquid, and a solvent; depositing the lead halide precursor ink onto a substrate; drying the lead halide precursor ink to form a lead halide film; and annealing the lead halide film.
    Type: Grant
    Filed: May 5, 2023
    Date of Patent: July 15, 2025
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Xiao-Xin Gao, Zhaofu Fei, Paul J. Dyson, Mohammad Khaja Nazeeruddin
  • Patent number: 12302681
    Abstract: A method for preparing photoactive perovskite materials. The method comprises the steps of preparing a lead and tin halide precursor ink.
    Type: Grant
    Filed: September 18, 2023
    Date of Patent: May 13, 2025
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Jerred A. Chute, Vivek V. Dhas
  • Patent number: 12300485
    Abstract: A perovskite material that has a perovskite crystal lattice having a formula of CxMyXz, and alkyl polyammonium cations disposed within or at a surface of the perovskite crystal lattice; wherein x, y, and z, are real numbers; C comprises one or more cations selected from the group consisting of Group 1 metals, Group 2 metals, ammonium, formamidinium, guanidinium, and ethene tetramine; M comprises one or more metals each selected from the group consisting of Be, Mg, Ca, Sr, Ba, Fe, Cd, Co, Ni, Cu, Ag, Au, Hg, Sn, Ge, Ga, Pb, In, Tl, Sb, Bi, Ti, Zn, Cd, Hg, and Zr, and combinations thereof; and X comprises one or more anions each selected from the group consisting of halides, pseudohalides, chalcogenides, and combinations thereof.
    Type: Grant
    Filed: December 20, 2023
    Date of Patent: May 13, 2025
    Assignee: CubivPV Inc.
    Inventors: Michael D. Irwin, Michael Holland, Nicholas Anderson
  • Patent number: 12243740
    Abstract: A perovskite material that has a perovskite crystal lattice having a formula of CxMyXz, where x, y, and z, are real numbers. Bulky organic cations reside near a surface or a grain boundary of the perovskite crystal lattice. C includes one or more cations selected from the group consisting of Group 1 metals, Group 2 metals, methylammonium, formamidinium, guanidinium, and ethene tetramine. M includes one or more metals each selected from the group consisting of Be, Mg, Ca, Sr, Ba, Fe, Cd, Co, Ni, Cu, Ag, Au, Hg, Sn, Ge, Ga, Pb, In, Tl, Sb, Bi, Ti, Zn, Cd, Hg, and Zr and combinations thereof. X includes one or more anions each selected from the group consisting of halides, sulfides, selenides, and combinations thereof.
    Type: Grant
    Filed: October 28, 2019
    Date of Patent: March 4, 2025
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Michael Holland, Nicholas Anderson
  • Publication number: 20240425968
    Abstract: A method for solvent-free perovskite deposition. The method comprises loading a lead target and one or more samples adhered to a substrate holder into a deposition chamber, pumping down to a high vacuum pressure, and backfilling the deposition chamber with the vapor of a salt precursor to form a perovskite material.
    Type: Application
    Filed: September 9, 2024
    Publication date: December 26, 2024
    Inventors: Michael D. Irwin, Marissa Higgins, David W. Miller
  • Publication number: 20240407247
    Abstract: Photovoltaic devices such as solar cells, hybrid solar cell-batteries, and other such devices may include an active layer disposed between two electrodes, the active layer having perovskite material and other material such as mesoporous material, interfacial layers, thin-coat interfacial layers, and combinations thereof. The perovskite material may be photoactive. The perovskite material may be disposed between two or more other materials in the photovoltaic device. Inclusion of these materials in various arrangements within an active layer of a photovoltaic device may improve device performance. Other materials may be included to further improve device performance, such as, for example: additional perovskites, and additional interfacial layers.
    Type: Application
    Filed: August 7, 2024
    Publication date: December 5, 2024
    Inventors: Michael D. Irwin, Vivek V. Dhas
  • Publication number: 20240401211
    Abstract: Particular embodiments described herein provide for a synthetic fuel creation system. The synthetic fuel creation system includes a syngas creation station to create syngas, a crude creation station to create heavy syncrude, and a crude cracking station to convert the heavy syncrude into synthetic fuel. The synthetic fuel creation system can use an electrocatalysis system to create the syngas and the electrocatalysis system can include an anode, a cathode, oxygen evolution reaction catalysts, hydrogen/carbon monoxide evolution reaction catalysts, and an electrolyte, where a pH of the electrolyte is acidic during at least a portion of creation of the syngas.
    Type: Application
    Filed: June 3, 2024
    Publication date: December 5, 2024
    Inventor: Michael D. Irwin
  • Publication number: 20240392135
    Abstract: A method for preparing a nickel oxide precursor ink comprising: preparing a solvent comprising diols and alcohol amines; adding nickel nitrate into the solvent to form a nickel nitrate containing solution; adding at least one metal acetate into the nickel nitrate containing solution to form a nickel nitrate and metal acetate containing solution; adding water to the nickel nitrate and metal acetate containing solution to form a nickel oxide precursor mixture; heating the nickel oxide precursor mixture to 60 to 75 Celsius; and cooling the nickel oxide precursor mixture to form the nickel oxide precursor ink.
    Type: Application
    Filed: July 31, 2024
    Publication date: November 28, 2024
    Inventors: Michael D. Irwin, Erin Sanehira
  • Patent number: 12116663
    Abstract: A method for solvent-free perovskite deposition. The method comprises loading a lead target and one or more samples adhered to a substrate holder into a deposition chamber, pumping down to a high vacuum pressure, and backfilling the deposition chamber with the vapor of a salt precursor to form a perovskite material.
    Type: Grant
    Filed: April 17, 2020
    Date of Patent: October 15, 2024
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Marissa Higgins, David W. Miller
  • Patent number: 12089485
    Abstract: Photovoltaic devices such as solar cells, hybrid solar cell-batteries, and other such devices may include an active layer disposed between two electrodes, the active layer having perovskite material and other material such as mesoporous material, interfacial layers, thin-coat interfacial layers, and combinations thereof. The perovskite material may be photoactive. The perovskite material may be disposed between two or more other materials in the photovoltaic device. Inclusion of these materials in various arrangements within an active layer of a photovoltaic device may improve device performance. Other materials may be included to further improve device performance, such as, for example: additional perovskites, and additional interfacial layers.
    Type: Grant
    Filed: May 20, 2021
    Date of Patent: September 10, 2024
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Vivek V. Dhas
  • Patent number: 12046425
    Abstract: A photovoltaic device comprising a first electrode, a second electrode, an active layer disposed at least partially between the first and second electrodes, an interfacial layer disposed at least partially between the first and second electrodes, and a non-stoichiometric oxide layer disposed at least partially between and in contact with one of the first or second electrodes and an encapsulant layer. The active layer of the photovoltaic device comprises a photoactive material.
    Type: Grant
    Filed: April 14, 2017
    Date of Patent: July 23, 2024
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Kamil Mielczarek
  • Publication number: 20240128076
    Abstract: A perovskite material that has a perovskite crystal lattice having a formula of CxMyXz, and alkyl polyammonium cations disposed within or at a surface of the perovskite crystal lattice; wherein x, y, and z, are real numbers; C comprises one or more cations selected from the group consisting of Group 1 metals, Group 2 metals, ammonium, formamidinium, guanidinium, and ethene tetramine; M comprises one or more metals each selected from the group consisting of Be, Mg, Ca, Sr, Ba, Fe, Cd, Co, Ni, Cu, Ag, Au, Hg, Sn, Ge, Ga, Pb, In, Tl, Sb, Bi, Ti, Zn, Cd, Hg, and Zr, and combinations thereof; and X comprises one or more anions each selected from the group consisting of halides, pseudohalides, chalcogenides, and combinations thereof.
    Type: Application
    Filed: December 20, 2023
    Publication date: April 18, 2024
    Inventors: Michael D. Irwin, Michael Holland, Nicholas Anderson
  • Publication number: 20240118602
    Abstract: A method for preparing photoactive perovskite materials. The method comprises the steps of: introducing a lead halide and a first solvent to a first vessel and contacting the lead halide with the first solvent to dissolve the lead halide to form a lead halide solution, introducing a Group 1 metal halide a second solvent into a second vessel and contacting the Group 1 metal halide with the second solvent to dissolve the Group 1 metal halide to form a Group 1 metal halide solution, and contacting the lead halide solution with the Group 1 metal halide solution to form a thin-film precursor ink. The method further comprises depositing the thin-film precursor ink onto a substrate, drying the thin-film precursor ink to form a thin film, annealing the thin film; and rinsing the thin film with a salt solution.
    Type: Application
    Filed: December 20, 2023
    Publication date: April 11, 2024
    Inventors: Michael D. Irwin, Kamil Mielczarek, Vivek V. Dhas
  • Patent number: 11953821
    Abstract: A method for preparing photoactive perovskite materials. The method comprises the steps of: introducing a lead halide and a first solvent to a first vessel and contacting the lead halide with the first solvent to dissolve the lead halide to form a lead halide solution, introducing a Group 1 metal halide a second solvent into a second vessel and contacting the Group 1 metal halide with the second solvent to dissolve the Group 1 metal halide to form a Group 1 metal halide solution, and contacting the lead halide solution with the Group 1 metal halide solution to form a thin-film precursor ink. The method further comprises depositing the thin-film precursor ink onto a substrate, drying the thin-film precursor ink to form a thin film, annealing the thin film; and rinsing the thin film with a salt solution.
    Type: Grant
    Filed: March 7, 2022
    Date of Patent: April 9, 2024
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Kamil Mielczarek, Vivek V. Dhas
  • Publication number: 20240114766
    Abstract: A method for producing a perovskite material photovoltaic device, the method comprising: depositing a layer comprising a fullerene or fullerene derivative on a perovskite material; depositing a cross-linking agent on the perovskite material or the layer comprising the fullerene or fullerene derivative, wherein the cross-linking agent comprises a silane, wherein the silane is a halosilyalkane; and depositing one or more polymers on the perovskite material or the layer comprising the fullerene or fullerene derivative.
    Type: Application
    Filed: December 6, 2023
    Publication date: April 4, 2024
    Inventors: Michael D. Irwin, Kamil Mielczarek, Nicholas Charles Anderson
  • Patent number: 11901177
    Abstract: A perovskite material that has a perovskite crystal lattice having a formula of CxMyXz, and alkyl polyammonium cations disposed within or at a surface of the perovskite crystal lattice; wherein x, y, and z, are real numbers; C comprises one or more cations selected from the group consisting of Group 1 metals, Group 2 metals, ammonium, formamidinium, guanidinium, and ethene tetramine; M comprises one or more metals each selected from the group consisting of Be, Mg, Ca, Sr, Ba, Fe, Cd, Co, Ni, Cu, Ag, Au, Hg, Sn, Ge, Ga, Pb, In, Tl, Sb, Bi, Ti, Zn, Cd, Hg, and Zr, and combinations thereof and X comprises one or more anions each selected from the group consisting of halides, pseudohalides, chalcogenides, and combinations thereof.
    Type: Grant
    Filed: January 23, 2023
    Date of Patent: February 13, 2024
    Assignee: CubicPV Inc.
    Inventors: Michael D. Irwin, Michael Holland, Nicholas Anderson