Patents by Inventor Michael K. Jeffries

Michael K. Jeffries has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20210230365
    Abstract: A polyaspartate composition can include a reaction product of a diamine and an amine-reactive component. The amine reactive-component can include a diester and an acrylate combined at an equivalent ratio of diester equivalents to acrylate equivalents of from less than 0.9:greater than 0.1 to greater than 0.3:less than 0.7. The diamine and the amine-reactive component can be combined at an equivalent ratio of diamine equivalents to amine-reactive component equivalents of from 1:0.8 to 0.8:1.
    Type: Application
    Filed: January 22, 2021
    Publication date: July 29, 2021
    Inventors: Matthew Stewart, Joseph Pierce, Michael K. Jeffries, Wendy S. Gustavich, Charles A. Gambino, Andrew Bradburn, Robert A. Wade, Myron W. Shaffer
  • Patent number: 11028296
    Abstract: The present invention provides an aqueous polyurethane dispersion (PUD) comprising an amorphous polyester having a glass transition temperature (Tg) as determined by differential scanning calorimetry of less than ?30° C.; wherein the aqueous polyurethane dispersion (PUD) has a glass transition temperature (Tg) as determined by differential scanning calorimetry (DSC) of 0° C. to 20° C. and a hard block content of greater than 50%.
    Type: Grant
    Filed: April 9, 2018
    Date of Patent: June 8, 2021
    Assignees: Covestro LLC, Covestro Deutschland AG
    Inventors: Stephanie Goldfein, Makoto Nakao, Lyubov Gindin, Hans Georg Grablowitz, Ronald Konitsney, Derick Henderson, Tina Kasardo, Philip Jones, Michael K. Jeffries
  • Publication number: 20200190390
    Abstract: The present invention provides an oil and gas well treatment comprising (a) preparing a composition by mixing an epoxy-based resin, an alkylphenol-blocked isocyanate, and a polyamine, (b) introducing the composition into a wellbore, (c) reacting the composition to produce a solid product, wherein the solid product reduces or prevents ingress of formation water into the oil and gas well.
    Type: Application
    Filed: August 1, 2018
    Publication date: June 18, 2020
    Inventors: David P. Zielinski, Michael K. Jeffries, Amy Maxin
  • Patent number: 10640702
    Abstract: Disclosed are coated particles, such as proppants, processes for their preparation and methods for using such particles, such as in a hydraulic fracturing process. The coated particles include a coating that includes a crystalline or semicrystalline polyester/polyurethane having a decrystallization temperature of at least 35° C.
    Type: Grant
    Filed: August 1, 2013
    Date of Patent: May 5, 2020
    Assignee: Covestro LLC
    Inventors: Kevan Hudson, Jeffrey F. Dormish, Michael K. Jeffries
  • Publication number: 20190055454
    Abstract: The present invention provides an oil or gas wellbore polymeric cement comprising the reaction product of an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder, wherein the reaction occurs in the wellbore at a temperature of at least 250° F. (121° C.). Also provided is a method of reducing fluid loss from an oil or gas well, comprising producing a polyisocyanurate cement by combining an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder within a wellbore at a temperature of at least 250° F. (121° C.). The various embodiments of the invention meet the controllability and minimized toxicity needed for this application. Standard aliphatic polyisocyanates reduce handling concerns while providing the reactivity response that fits this temperature range.
    Type: Application
    Filed: October 25, 2016
    Publication date: February 21, 2019
    Inventors: David P. Zielinski, Michael K. Jeffries
  • Publication number: 20190040291
    Abstract: The present invention provides an aqueous polyurethane dispersion (PUD) comprising an amorphous polyester having a glass transition temperature (Tg) as determined by differential scanning calorimetry of less than ?30° C.; wherein the aqueous polyurethane dispersion (PUD) has a glass transition temperature (Tg) as determined by differential scanning calorimetry (DSC) of 0° C. to 20° C. and a hard block content of greater than 50%.
    Type: Application
    Filed: April 9, 2018
    Publication date: February 7, 2019
    Inventors: Stephanie Goldfein, Makoto Nakao, Lyubov Gindin, Hans Georg Grablowitz, Ronald Konitsney, Derick Henderson, Tina Kasardo, Philip Jones, Michael K. Jeffries
  • Publication number: 20180346786
    Abstract: Methods and materials for treating completed oil and gas wells that have been partially depleted as a prelude to refracturing are provided. These methods include: (a) preparing a polyurethane diverting agent by mixing a polyol-containing component and a polyisocyanate-containing component; and (b) introducing the polyurethane diverting agent into the well. The polyol-containing component includes a polymeric polyol having a viscosity at 25° C. of no more than 1000 mPa·s and the isocyanate-containing component includes an unblocked (cyclo)aliphatic polyisocyanate polymer, optionally including allophanate groups, and having a viscosity at 25° C. of no more than 1000 mPa·s and at least 99% solids content.
    Type: Application
    Filed: May 25, 2018
    Publication date: December 6, 2018
    Inventors: David P. Zielinski, Michael K. Jeffries
  • Patent number: 10000686
    Abstract: Methods of treating a well bore within an underground formation are disclosed. These methods include: (a) preparing a treatment composition by mixing a polyol-containing component and a polyisocyanate-containing component; and (b) introducing the treatment composition into the well bore. The polyol-containing component includes a polymeric polyol having a viscosity at 25° C. of no more than 1000 mPa·s and the isocyanate-containing component includes an unblocked (cyclo)aliphatic polyisocyanate polymer including allophanate groups and having a viscosity at 25° C. and at least 99% solids of no more than 1000 mPa·s.
    Type: Grant
    Filed: December 18, 2013
    Date of Patent: June 19, 2018
    Assignees: Covestro LLC, Ecolab USA Inc.
    Inventors: David P. Zielinski, Alan Ekin, Michael K. Jeffries, Mario Roberto Rojas
  • Patent number: 9896598
    Abstract: A process of directly coating a metal substrate and curing the coating using radiation sources such as UV radiation having a wavelength of 200 nm and above. Furthermore, compositions of the invention can be used as a tie-coat for coatings that do not bond well directly to various metal substrates.
    Type: Grant
    Filed: July 23, 2013
    Date of Patent: February 20, 2018
    Inventors: Ramesh Subramanian, Kurt E. Best, Charles A. Gambino, Christine A. Mebane, Michael K. Jeffries, Myron W. Shaffer, Michael J. Dvorchak
  • Patent number: 9815739
    Abstract: The present invention provides an oil or gas wellbore polymeric cement comprising the reaction product of an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder, wherein the reaction occurs in the wellbore at a temperature of at least 250° F. (121° C.). Also provided is a method of reducing fluid loss from an oil or gas well, comprising producing a polyisocyanurate cement by combining an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder within a wellbore at a temperature of at least 250° F. (121° C.). The various embodiments of the invention meet the controllability and minimized toxicity needed for this application. Standard aliphatic polyisocyanates reduce handling concerns while providing the reactivity response that fits this temperature range.
    Type: Grant
    Filed: October 30, 2015
    Date of Patent: November 14, 2017
    Assignee: Covestro LLC
    Inventors: David P Zielinski, Michael K. Jeffries
  • Publication number: 20170121225
    Abstract: The present invention provides an oil or gas wellbore polymeric cement comprising the reaction product of an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder, wherein the reaction occurs in the wellbore at a temperature of at least 250° F. (121° C.). Also provided is a method of reducing fluid loss from an oil or gas well, comprising producing a polyisocyanurate cement by combining an aliphatic isocyanate, a trimerization catalyst, and a catalyst retarder within a wellbore at a temperature of at least 250° F. (121° C.). The various embodiments of the invention meet the controllability and minimized toxicity needed for this application. Standard aliphatic polyisocyanates reduce handling concerns while providing the reactivity response that fits this temperature range.
    Type: Application
    Filed: October 30, 2015
    Publication date: May 4, 2017
    Inventors: David P. Zielinski, Michael K. Jeffries
  • Publication number: 20150166872
    Abstract: Methods of treating a well bore within an underground formation are disclosed. These methods include: (a) preparing a treatment composition by mixing a polyol-containing component and a polyisocyanate-containing component; and (b) introducing the treatment composition into the well bore. The polyol-containing component includes a polymeric polyol having a viscosity at 25° C. of no more than 1000 mPa·s and the isocyanate-containing component includes an unblocked (cyclo)aliphatic polyisocyanate polymer including allophanate groups and having a viscosity at 25° C. and at least 99% solids of no more than 1000 mPa·s.
    Type: Application
    Filed: December 18, 2013
    Publication date: June 18, 2015
    Applicant: Bayer MaterialScience LLC
    Inventors: David P. Zielinski, Abdullah Ekin, Michael K. Jeffries
  • Publication number: 20150034314
    Abstract: Disclosed are coated particles, such as proppants, processes for their preparation and methods for using such particles, such as in a hydraulic fracturing process. The coated particles include a coating that includes a crystalline or semicrystalline polyester/polyurethane having a decrystallization temperature of at least 35° C.
    Type: Application
    Filed: August 1, 2013
    Publication date: February 5, 2015
    Inventors: Kevan Hudson, Jeffrey F. Dormish, Michael K. Jeffries
  • Patent number: 8765900
    Abstract: The present disclosure is directed to an aliphatic isocyanate-based moisture-curable resin. The disclosed resin may include an aliphatic isocyanate functional material and an cycloaliphatic isocyanate functional material. The resin may be used to formulate a coating composition that may exhibit no substantial sag when applied at a wet film thickness of at least 6 mils, and no substantial blistering when cured to a dry film thickness of at least 6 mils.
    Type: Grant
    Filed: August 27, 2009
    Date of Patent: July 1, 2014
    Assignee: Bayer MaterialScience LLC
    Inventors: Kurt E. Best, Michael K. Jeffries, Ahren Olson, Carl Angeloff
  • Publication number: 20130302530
    Abstract: A process of directly coating a metal substrate and curing the coating using radiation sources such as UV radiation having a wavelength of 200 nm and above. Furthermore, compositions of the invention can be used as a tie-coat for coatings that do not bond well directly to various metal substrates.
    Type: Application
    Filed: July 23, 2013
    Publication date: November 14, 2013
    Inventors: Ramesh Subramanian, Kurt E. Best, Charles A. Gambino, Christine A. Mebane, Michael K. Jeffries, Myron W. Shaffer, Michael J. Dvorchak
  • Publication number: 20130203934
    Abstract: A polyurea coating composition comprising the reaction product of: an isocyanate-functional component (A) comprising: a) an aliphatic isocyanate functional material; and b) a cycloaliphatic isocyanate functional material; and an isocyanate-reactive component (B) comprising at least one polyaspartic acid ester component.
    Type: Application
    Filed: April 5, 2011
    Publication date: August 8, 2013
    Applicant: Bayer MaterialScience LLC
    Inventors: Kurt E. Best, John P. Forsythe, Joseph R. Kleer, Michael K. Jeffries
  • Patent number: 8476396
    Abstract: A composition that includes isocyanate group containing compounds that include on average i) a NCO functionality less than or equal to 3.5; and ii) from 1.5 to 8 percent by weight, based on the isocyanate containing compound, of allophanate groups; and which is substantially free of uretdione groups. The composition can be used in two component elastomeric coating compositions that include a component A the above-described composition and a component B that includes a compound containing one or more functional groups that are reactive with isocyanate groups. The elastomeric coating compositions can be used to coat substrates.
    Type: Grant
    Filed: May 25, 2007
    Date of Patent: July 2, 2013
    Assignee: Bayer MaterialScience LLC
    Inventors: David P. Zielinski, Myron Shaffer, Michael K. Jeffries
  • Patent number: 8415471
    Abstract: This invention relates to flexible cycloaliphatic diisocyanate trimers and a process for the preparation of these. These flexible products are allophanate-modified, partially trimerized cycloaliphatic diisocyanates and are characterized by a low Tg. More specifically, the Tg of the resultant product ranges from about ?30° C. to about 40° C., after the excess monomer has been removed from the product.
    Type: Grant
    Filed: November 29, 2007
    Date of Patent: April 9, 2013
    Assignee: Baver MaterialScience LLC
    Inventors: Myron W. Shaffer, Michael K. Jeffries, David P. Zielinski
  • Publication number: 20110054141
    Abstract: The present disclosure is directed to an aliphatic isocyanate-based moisture-curable resin. The disclosed resin may include an aliphatic isocyanate functional material and an cycloaliphatic isocyanate functional material. The resin may be used to formulate a coating composition that may exhibit no substantial sag when applied at a wet film thickness of at least 6 mils, and no substantial blistering when cured to a dry film thickness of at least 6 mils.
    Type: Application
    Filed: August 27, 2009
    Publication date: March 3, 2011
    Applicant: Bayer MaterialScience LLC
    Inventors: Kurt E. Best, Michael K. Jeffries, Ahren Olson, Carl Angeloff
  • Publication number: 20090176907
    Abstract: A process of directly coating a metal substrate and curing the coating using radiation sources such as UV radiation having a wavelength of 200 nm and above. Furthermore, compositions of the invention can be used as a tie-coat for coatings that do not bond well directly to various metal substrates.
    Type: Application
    Filed: January 8, 2008
    Publication date: July 9, 2009
    Inventors: Ramesh Subramanian, Kurt E. Best, Charles A. Gambino, Christine M. Mebane, Michael K. Jeffries, Myron W. Shaffer, Michael K. Dvorchak