Abstract: Embodiments of methods for producing and testing aqueous gas streams within a self-pressurized flow cell are disclosed. The aqueous gas streams comprise mixtures of aqueous salt precursor and aqueous acid precursor that are mixed in-line and introduced to the self-pressurized flow cell to produce aqueous gases. Once in the self-pressurized flow cell, the precursor mixture formed from the mixed aqueous salt precursor and the aqueous acid precursor may react with the sample. Both the sample and the reacted aqueous solution may be subjected to a variety of real-time tests, such electrochemical tests and in line characterization techniques. These embodiments allow for the concentrations of the aqueous salt precursor and the aqueous acid precursor to be accurately and precisely maintained while allowing for increased safety when handling and testing the various toxic aqueous gas streams produced.

Abstract: The present application provides aerosol processes for selectively incorporating properties of solid precursor particles into processed materials is provided. In one aspect, a carrier gas and a precursor mixture are injected into an aerosol generator. The precursor mixture includes solid precursor particles and a liquid component. One or more ultrasonic transducers are applied to the precursor mixture in the aerosol generator to aerosolize a portion of the precursor mixture that comprises solid particles that are smaller than a predetermined size. The aerosolized portion of the precursor mixture is transferred, via the carrier gas, into a reactor. The aerosolized portion in the reactor is then dried and sometimes reacted to produce solid product particles, and the solid product particles are collected in a particle collector.

Abstract: The present application provides aerosol processes for selectively incorporating properties of solid precursor particles into processed materials is provided. In one aspect, a carrier gas and a precursor mixture are injected into an aerosol generator. The precursor mixture includes solid precursor particles and a liquid component. One or more ultrasonic transducers are applied to the to the precursor mixture in the aerosol generator to aerosolize a portion of the precursor mixture that comprises solid particles that are smaller than a predetermined size. The aerosolized portion of the precursor mixture is transferred, via the carrier gas, into a reactor. The aerosolized portion in the reactor is then dried and sometimes reacted to produce solid product particles, and the solid product particles are collected in a particle collector.

Abstract: Embodiments of methods for producing and testing aqueous gas streams within a self-pressurized flow cell are disclosed. The aqueous gas streams comprise mixtures of aqueous salt precursor and aqueous acid precursor that are mixed in-line and introduced to the self-pressurized flow cell to produce aqueous gases. Once in the self-pressurized flow cell, the precursor mixture formed from the mixed aqueous salt precursor and the aqueous acid precursor may react with the sample. Both the sample and the reacted aqueous solution may be subjected to a variety of real-time tests, such electrochemical tests and in line characterization techniques. These embodiments allow for the concentrations of the aqueous salt precursor and the aqueous acid precursor to be accurately and precisely maintained while allowing for increased safety when handling and testing the various toxic aqueous gas streams produced.

Abstract: Embodiments of a method of synthesizing a metathesis and isomerization catalyst or metathesis catalyst or isomerization catalyst comprises forming a catalyst precursor solution comprising a diluent and a catalyst precursor where the catalyst precursor comprises at least one of a silica precursor and an alumina precursor for the isomerization catalyst and additionally an oxometallate precursor or metal oxide precursor for the metathesis catalyst or the metathesis and isomerization catalyst, where the catalyst precursor solution is absent a surfactant; aerosolizing the catalyst precursor solution; drying the aerosolized catalyst precursor mixture to form a dried catalyst precursor; and reacting the dried catalyst precursor to yield the metathesis and isomerization catalyst or the metathesis catalyst or the isomerization catalyst, the metathesis and isomerization catalyst comprising a silica and alumina support with an oxometallate or a metal oxide distributed within the silica and alumina support.

Abstract: Embodiments of a method of synthesizing a metathesis and isomerization catalyst or metathesis catalyst or isomerization catalyst comprises forming a catalyst precursor solution comprising a diluent and a catalyst precursor where the catalyst precursor comprises at least one of a silica precursor and an alumina precursor for the isomerization catalyst and additionally an oxometallate precursor or metal oxide precursor for the metathesis catalyst or the metathesis and isomerization catalyst, where the catalyst precursor solution is absent a surfactant; aerosolizing the catalyst precursor solution; drying the aerosolized catalyst precursor mixture to form a dried catalyst precursor; and reacting the dried catalyst precursor to yield the metathesis and isomerization catalyst or the metathesis catalyst or the isomerization catalyst, the metathesis and isomerization catalyst comprising a silica and alumina support with an oxometallate or a metal oxide distributed within the silica and alumina support.

Abstract: The present disclosure provides sensing systems and methods that are useful for monitoring materials (e.g., cement) via light diffusion to identify characteristics thereof and changes therein. The systems can utilize a light source, a light sensor, and light transmitting members combined with the material to be monitored. In use, light from the light source can be allowed to scatter through the material via the light transmitting members for detection by the light sensor. The data regarding the light transfer can be transmitted utilizing a communication interface and can be analyzed using data processing equipment. The systems and methods may particularly be utilized in monitoring the reinforcing cement positioned between the casing and the formation in an oil well.

Abstract: The invention relates to a corrosion resistant reactor tube, method for providing a passivating or corrosion resistant coating to the inside of the reactor tube, and a method of making high bismuth glass powders using the corrosion resistant reactor tube.

Abstract: The invention relates to a corrosion resistant reactor tube, method for providing a passivating or corrosion resistant coating to the inside of the reactor tube, and a method of making high bismuth glass powders using the corrosion resistant reactor tube.

Abstract: The present disclosure relates to a dielectric composition having a resin and a filler. The filler is used to raise the dielectric and has a passivating surface coating thereon.

Abstract: A process for forming an aerosol of semiconductor nanoparticles includes pyrolyzing a semiconductor material-containing gas then quenching the gas being pyrolyzed to control particle size and prevent uncontrolled coagulation. The aerosol is heated to densify the particles and form crystalline nanoparticles. In an exemplary embodiment, the crystalline particles are advantageously classified by size using a differential mobility analyzer and particles having diameters outside of a pre-selected range of sizes, are removed from the aerosol. In an exemplary embodiment, the crystalline, classified and densified nanoparticles are oxidized to form a continuous oxide shell over the semiconductor core of the particles. The cores include a density which approaches the bulk density of the pure material of which the cores are composed and the majority of the particle cores are single crystalline. The oxidized particles are deposited on a substrate using thermophoretic, electrophoretic, or other deposition means.

Abstract: A stratum or discontinuous monolayer of dielectric-coated semiconductor particles includes a high density of semiconductor nanoparticles with a tightly controlled range of particle sizes in the nanometer range. In an exemplary embodiment, the nanoparticles of the stratum are substantially the same size and include cores which are crystalline, preferably single crystalline, and include a density which is approximately the same as the bulk density of the semiconductor material of which the particle cores are formed. In an exemplary embodiment, the cores and particles are preferably spherical in shape. The stratum is characterized by a uniform particle density on the order of 1012 to 1013 particles/cm2. A plurality of adjacent particles contact each other, but the dielectric shells provide electrical isolation and prevent lateral conduction between the particles of the stratum. The stratum includes a density of foreign atom contamination of less than 1011 atoms/cm2.

Abstract: A process for forming an aerosol of semiconductor nanoparticles includes pyrolyzing a semiconductor material-containing gas then quenching the gas being pyrolyzed to control particle size and prevent uncontrolled coagulation. The aerosol is heated to densify the particles and form crystalline nanoparticles. In an exemplary embodiment, the crystalline particles are advantageously classified by size using a differential mobility analyzer and particles having diameters outside of a pre-selected range of sizes, are removed from the aerosol. In an exemplary embodiment, the crystalline, classified and densified nanoparticles are oxidized to form a continuous oxide shell over the semiconductor core of the particles. The cores include a density which approaches the bulk density of the pure material of which the cores are composed and the majority of the particle cores are single crystalline. The oxidized particles are deposited on a substrate using thermophoretic, electrophoretic, or other deposition means.

Abstract: A stratum or discontinuous monolayer of dielectric-coated semiconductor particles includes a high density of semiconductor nanoparticles with a tightly controlled range of particle sizes in the nanometer range. In an exemplary embodiment, the nanoparticles of the stratum are substantially the same size and include cores which are crystalline, preferably single crystalline, and include a density which is approximately the same as the bulk density of the semiconductor material of which the particle cores are formed. In an exemplary embodiment, the cores and particles are preferably spherical in shape. The stratum is characterized by a uniform particle density on the order of 1012 to 1013 particles/cm2. A plurality of adjacent particles contact each other, but the dielectric shells provide electrical isolation and prevent lateral conduction between the particles of the stratum. The stratum includes a density of foreign atom contamination of less than 1011 atoms/cm2.