Abstract: A method for solid-phase extraction is disclosed. The method includes fabricating a solid-phase extraction medium by incorporating a plurality of modified mesoporous silica particles within pores of a cotton fabric matrix, putting the solid-phase extraction medium in contact with a fluid containing metal ions including one of immersing the solid-phase extraction medium in the fluid containing metal ions or passing the fluid containing metal ions through the solid-phase extraction medium by continuously circulating the fluid through the solid-phase extraction medium, and extracting the metal ions from the fluid by adsorbing the metal ions onto the solid-phase extraction medium responsive to a contact between the solid-phase extraction medium and the fluid containing metal ions.

Abstract: A vacuum-assisted coated fiber located in a capillary tube system for sampling and delivering materials to an analytical device and a method for sampling analytes is disclosed. A sorbent comprising polypyrrole/graphene oxide is coated on a fiber inserted within an interior space of the capillary tube to entrap an analyte within a sample. The vacuum-assisted coated fiber located in a capillary tube device also includes a vacuum device configured to vacuum the extraction vial. This may improve the extraction of the analytes vapors from the sample, matrix to the sorbent bed.

Abstract: A method for solid-phase extraction is disclosed. The method includes fabricating a solid-phase extraction medium by incorporating a plurality of modified mesoporous silica particles within pores of a cotton fabric matrix, putting the solid-phase extraction medium in contact with a fluid containing metal ions including one of immersing the solid-phase extraction medium in the fluid containing metal ions or passing the fluid containing metal ions through the solid-phase extraction medium by continuously circulating the fluid through the solid-phase extraction medium, and extracting the metal ions from the fluid by adsorbing the metal ions onto the solid-phase extraction medium responsive to a contact between the solid-phase extraction medium and the fluid containing metal ions.

Abstract: A vacuum-assisted coated fiber located in a capillary tube system for sampling and delivering materials to an analytical device and a method for sampling analytes is disclosed. A sorbent comprising polypyrrole/graphene oxide is coated on a fiber inserted within an interior space of the capillary tube to entrap an analyte within a sample. The vacuum-assisted coated fiber located in a capillary tube device also includes a vacuum device configured to vacuum the extraction vial. This may improve the extraction of the analytes vapors from the sample, matrix to the sorbent bed.