Abstract: A sample analysis cup, sample cup assembly, and method is provided including a cell body with an open top end including an outer top wall and an inner top wall, each extending axially and positioned in concentric relationship; a bottom wall extending from the outer top wall to the inner top wall, the bottom wall and the inner and outer top walls defining an internal reservoir therebetween; a transverse wall extending a selected distance from the inner top wall, the transverse wall partially closing the open top end; an open bottom end including an outer bottom wall and an inner bottom wall, each extending axially and positioned in concentric relationship, the outer and inner bottom walls defining an internal channel therebetween; and a hollow chamber defined between the open top end and the open bottom end.

Abstract: An accessory, method, and system is provided for protecting the lower chamber of X-ray spectroscopic instrumentation during analysis, the instrumentation including an upper chamber, a lower chamber, and a dividing plate, the lower chamber including an X-ray detector and an excitation source, the accessory including: a frame with a centrally-located aperture extending from one side of the frame to an opposite side of the frame; an adhesive layer disposed on each side of the frame; a thin film of polymeric material disposed on one side of the frame; and a removably attached release sheet on the adhesive layer disposed on the opposite side of the frame, where the accessory is disposed on a surface of the dividing plate to protect the lower chamber of the instrumentation from damage.

Abstract: A cup assembly for holding a sample to be analyzed spectrochemically, includes a tubular longitudinal member which is disposed symmetrical about a central axis. The tubular member extends longitudinally between a first end and a second end. An indented peripheral flange is defined at the second end. The indented flange has an inverted L shaped cross-section. An annular collar extends longitudinally between a first end and a second end. An internal peripheral flange is defined at the first end. The internal flange has an inverted L shaped cross-section complementing the indented flange of the tubular member. When a substantially thin film is interposed between the second end of the tubular member and the first end of the annular collar, the film is retained between the sample cell body and the collar between the indented flange and the internal flange. The cup may have a funnel shaped sample retaining chamber.

Abstract: An accessory, method, and system is provided for protecting the lower chamber of X-ray spectroscopic instrumentation during analysis, the instrumentation including an upper chamber, a lower chamber, and a dividing plate, the lower chamber including an X-ray detector and an excitation source, the accessory including: a frame with a centrally-located aperture extending from one side of the frame to an opposite side of the frame; an adhesive layer disposed on each side of the frame; a thin film of polymeric material disposed on one side of the frame; and a removably attached release sheet on the adhesive layer disposed on the opposite side of the frame, where the accessory is disposed on a surface of the dividing plate to protect the lower chamber of the instrumentation from damage.

Abstract: Sample cup holding devices including a base member with a top side, a bottom side, and one or more apertures extending from the top side to the bottom side, each of the one or more apertures for receiving a sample cup and maintaining the sample cup in a substantially vertical position, and a method for using same are provided.

Abstract: A sample cup for retaining a sample material to be subjected to an x-ray spectrochemical analysis. The sample cup comprises a cell body of a cylindrical configuration having an open top end and an open bottom end and defining a hollow between the two open ends, the open top end having an outer wall and an inner wall encircling the open top end. The outer wall and the inner wall extend axially and are positioned in concentric relationship with one another and form an internal reservoir space therebetween.

Abstract: A cup assembly for holding a sample to be analyzed spectrochemically, including a sample cell having a generally cylindrical wall longitudinally extending between a first end and a second end thereof and a sleeve having a generally cylindrical wall longitudinally extending between a first end and a second end thereof, and a plurality of projections longitudinally extending from the first end of the sleeve wall. When a substantially planar film is interposed between the sample cell and the sleeve, and the first end of the sample cell is inserted into the first end of the sleeve, the film is retained between the sample cell and the annular sleeve; and the longitudinal projections are positioned to perforate the film when the film is pulled against the longitudinal projections.

Abstract: A method and apparatus for covering and identifying a container utilizing a thin film material and a frame. The thin film material covers a through hole in the frame and has a perforation that defines an outer detaching surface an inner covering surface commensurate with the container opening. The method comprises the steps of attaching the thin film material to a frame having the through hole; disposing the frame onto an open top surface of the container; depressing a portion of the frame to detach the thin-film from the frame along the perforation and further sliding the frame coaxially to circumscribe the base of the container where it identifies information about the container.

Abstract: A sample cup for retaining a sample material to be subjected to an x-ray spectrochemical analysis. The sample cup comprises a cell body of a cylindrical configuration having an open top end and an open bottom end and defining a hollow between the two open ends, the open top end having an outer wall and an inner wall encircling the open top end. The outer wall and the inner wall extend axially and are positioned in concentric relationship with one another and form an internal reservoir space therebetween.

Abstract: A sample cup for retaining a sample material to be subjected to an x-ray spectrochemical analysis. The sample cup comprises a cell body of a cylindrical configuration having an open top end and an open bottom end and defining a hollow between the two open ends, the open top end having an outer wall and an inner wall encircling the open top end. The outer wall and the inner wall extend axially and are positioned in concentric relationship with one another and form a reservoir space therebetween.

Abstract: A method and apparatus for covering and identifying a container utilizing a thin film material and a frame. The thin film material covers a through hole in the frame and has a perforation that defines an outer detaching surface an inner covering surface commensurate with the container opening. The method comprises the steps of attaching the thin film material to a frame having the through hole; disposing the frame onto an open top surface of the container; depressing a portion of the frame to detach the thin-film from the frame along the perforation and further sliding the frame coaxially to circumscribe the base of the container where it identifies information about the container.

Abstract: A sample cup for retaining a sample material to be subjected to an x-ray spectrochemical analysis. The sample cup comprises a cell body of a cylindrical configuration having an open top end and an open bottom end and defining a hollow between the two open ends, the open top end having an outer wall and an inner wall encircling the open top end. The outer wall and the inner wall extend axially and are positioned in concentric relationship with one another and form a reservoir space therebetween.

Abstract: A method and apparatus for covering and identifying a container utilizing a thin film material and a frame. The thin film material covers a through hole in the frame and has a perforation that defines an outer detaching surface an inner covering surface commensurate with the container opening. The method comprises the steps of attaching the thin film material to a frame having the through hole; disposing the frame onto an open top surface of the container; depressing a portion of the frame to detach the thin-film from the frame along the perforation and further sliding the frame coaxially to circumscribe the base of the container where it identifies information about the container.

Abstract: A cup assembly for holding a sample to be analyzed spectrochemically, includes a tubular longitudinal member which is disposed symmetrical about a central axis. The tubular member extends longitudinally between a first end and a second end. An indented peripheral flange is defined at the second end. The indented flange has an inverted L shaped cross-section. An annular collar extends longitudinally between a first end and a second end. An internal peripheral flange is defined at the first end. The internal flange has an inverted L shaped cross-section complementing the indented flange of the tubular member. When a substantially thin film is interposed between the second end of the tubular member and the first end of the annular collar, the film is retained between the sample cell body and the collar between the indented flange and the internal flange. The cup may have a funnel shaped sample retaining chamber.

Abstract: A sample cup assembly for use with an analytical instrument having a sample cup holder with an inner diameter which is greater than the outer diameter of the sample cup assembly. The sample cup assembly can include a main cell for retaining a specimen to be analyzed; a collar for locating a thin film over the open end of the main cell such that the film sealingly closes the open end of the main cell; and two or more projections extending outwardly from either the main cell or collar. The projections engage the interior surface of the sample cup holder when the sample cup assembly is installed therein, thereby centering the sample cup assembly within the sample cup holder.

Abstract: A method for covering a sample cup for retaining a sample to be analyzed spectrochemically, the method comprising the steps of attaching a thin-film material to a substrate having a through hole to form a planar frame member, the thin-film material covering the through hole and having a patterned perforation positioned within the through hole defining an inner covering surface with diameter d1 and an outer detaching surface; disposing the planar frame member onto an open top surface of the sample cup with diameter d2 less than d1 such that the inner covering surface of the thin-film material extends across the open top surface; and depressing a portion of the planar frame member to cause detachment of the thin-film material from the substrate along the patterned perforation, and thereby causing increased tautness of the inner covering surface which extends across the open top surface.

Abstract: A sample receptacle for retaining a sample that is to be subjected to spectrochemical analysis. The sample receptacle includes a tubular body having at least one open end and a tapered exterior wall. A sheet of thin film material having peripheral edges is disposed across the open end of the tubular body. A generally annular collar, having an interior wall tapered at an angle supplemental to the taper of the interior wall, is disposed around the tubular body. As the annular collar is placed around the tubular body, the tapered exterior wall of the tubular body creates an interference fit with the tapered interior wall of the annular collar. The tapered surfaces of the tubular body and the annular collar engage the sheet of thin film material and pull the sheet of thin film material taut over the open end of the tubular body. The annular collar is sized to engage the entire length of the exterior wall of the tubular body.

Abstract: A sample cup for holding a speciman to be analyzed by x-ray spectroscopy, comprises an enclosure having at least one wall and two open ends. The sample cup also includes sample support means removably attached to each of the two open ends and sample loading means located on the at least one wall for filling the sample cup with the speciman to be analyzed.

Abstract: A sample receptacle for retaining a sample that is to be subjected to spectrochemical analysis. The sample receptacle includes a tubular body having at least one open end and a tapered exterior wall. A sheet of thin film material having peripheral edges is disposed across the open end of the tubular body. A generally annular collar, having an interior wall tapered at an angle supplemental to the taper of the interior wall, is disposed around the tubular body. As the annular collar is placed around the tubular body, the tapered exterior wall of the tubular body creates an interference fit with the tapered interior wall of the annular collar. The tapered surfaces of the tubular body and the annular collar engage the sheet of thin film material and pull the sheet of thin film material taut over the open end of the tubular body. The annular collar is sized to engage the entire length of the exterior wall of the tubular body.

Abstract: A briquette press apparatus for compacting powdered materials having a programmable control monitoring the forces of the press. During compression, the programmable control measures the compression force being asserted against the powdered material and regulates the press so that the compression force equals a programmed reference value. During decompression, the programmable control monitors the pressure release rate of the press and regulates the press so that the measured pressure release rate matches a programmed reference rate.