Patents by Inventor Olivier Guillon

Olivier Guillon has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240139805
    Abstract: The disclosure relates to a device and a method for sintering. The device for sintering comprises an electrically conductive first component, an electrically conductive second component and at least one electrically conductive surface element for heating a green body to be sintered. The first component and the second component are movable relative to each other and/or relative to the surface element such that an electrical circuit comprising the first component, the surface element and the second component can be closed by the relative movement. In this way, a rapid sintering process is enabled on an industrial scale. The device can be integrated in a particularly simple manner into existing sintering plants, for example, a FAST/SPS sintering plant.
    Type: Application
    Filed: February 2, 2022
    Publication date: May 2, 2024
    Inventors: Tarini Prasad MISHRA, Martin BRAM, Olivier GUILLON, Ralf STEINERT
  • Publication number: 20230397306
    Abstract: A method and a device for generating light and to a use of a component for emitting light is disclosed. In a method for generating light, a component comprising a first material from the group of cuprates is subjected to an electric voltage and/or an electric field at a temperature T below 0° C. such that the component emits light. In this way, a light generation is provided which is accompanied by a substantial energy saving as well as a significantly reduced technical effort and which is also possible at cryogenic temperatures.
    Type: Application
    Filed: September 21, 2021
    Publication date: December 7, 2023
    Inventors: Apurv DASH, Robert MÜCKE, Olivier GUILLON
  • Publication number: 20230387455
    Abstract: A solid-state cell, a solid-state battery, and an associated method for producing a solid-state cell is disclosed. A solid-state cell has an electrolyte comprising NaSICON. The solid-state cell comprises a first electrode arranged at a first region of the electrolyte and a second electrode arranged at a second region of the electrolyte. A continuous material layer is arranged at least a third region of the electrolyte on an outer surface of the electrolyte. Alternatively, a chemical composition of the outer surface in the third region of the electrolyte is changed. In this way, the formation of filaments and/or dendrites can be effectively prevented and operation at significantly increased current densities is possible.
    Type: Application
    Filed: October 28, 2021
    Publication date: November 30, 2023
    Inventors: Qianli MA, Frank TIETZ, Dina FATTAKHOVA-ROHLFING, Olivier GUILLON
  • Publication number: 20230382807
    Abstract: A method for producing a densified component and an article comprising a densified component is disclosed. In a method for producing a densified component, a starting material is subjected to an electric field at a temperature (T) below 800° C. The starting material comprises a first material from the group consisting of cuprates. The method has a low technical effort, since densification is possible without heating the starting material.
    Type: Application
    Filed: September 13, 2021
    Publication date: November 30, 2023
    Inventors: Apurv DASH, Robert MÜCKE, Olivier GUILLON
  • Patent number: 11786870
    Abstract: Disclosed are a CMS membrane, characterized in that it is obtainable by pyrolysis of a polyimide composed of the monomers 1-(4-aminophenyl)-1,3,3-trimethyl-2H-inden-5-amine and 5-(1,3-dioxo-2-benzofuran-5-carbonyl-2-benzofuran-1,3-dione of the following formulae: preferably by pyrolysis of the polyimide having the CAS number 62929-02-6, and a supported CMS membrane comprising a CMS membrane obtainable from a polyimide by pyrolysis and a porous support, characterized in that a mesoporous intermediate layer is provided between the CMS membrane and the porous support. Further disclosed are a process for preparing the supported membrane, the use of the membranes for separating gas mixtures or liquid mixtures, an apparatus for gas separation or for liquid separation, and the use of the polyimide for preparing a CMS membrane by pyrolysis.
    Type: Grant
    Filed: September 16, 2019
    Date of Patent: October 17, 2023
    Assignee: Forschungszentrum Jülich GmbH
    Inventors: Patrick Tchoua Ngamou, Mariya E. Ivanova, Wilhelm Albert Meulenberg, Olivier Guillon
  • Publication number: 20230184132
    Abstract: The disclosure relates to a method for operating a gas turbine at a high temperature and to a gas turbine assembly. In the method, a gas turbine having a structural material and a thermal barrier layer disposed on the structural material is cooled down in a decelerated manner after operation at an operating temperature above 1000° C., so that damage to the structural material and/or the thermal barrier layer is minimized. In this way, the gas turbine can be operated permanently at temperatures above 1500° C.
    Type: Application
    Filed: April 22, 2021
    Publication date: June 15, 2023
    Inventors: Robert VAßEN, Daniel Emil MACK, Martin TANDLER, Olivier GUILLON
  • Patent number: 11542204
    Abstract: The invention relates to a method for producing a non-oxide ceramic powder comprising a nitride, a carbide, a boride or at least one MAX phase with the general composition Mn+1AXn, where M=at least one element from the group of transition elements (Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta), A=at least one A group element from the group (Si, Al, Ga, Ge, As, Cd, In, Sn, Tl and Pb), X=carbon (C) and/or nitrogen (N) and/or boron (B), and n=1, 2 or 3. According to the invention, corresponding quantities of elementary starting materials or other precursors are mixed with at least one metal halide salt (NZ), compressed (pellet), and heated for synthesis with a metal halide salt (NZ). The compressed pellet is first enveloped with another metal halide salt, compressed again, arranged in a salt bath and heated therewith until the melting temperature of the salt is exceeded. Optionally, melted silicate can be added, which prevents the salt from evaporating at high temperatures.
    Type: Grant
    Filed: June 7, 2018
    Date of Patent: January 3, 2023
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Apurv Dash, Jesus Gonzalez, Robert Vassen, Olivier Guillon
  • Patent number: 11417870
    Abstract: Provided is a method for producing an electrode for a solid-state battery comprising providing a multilayer solid ceramic electrolyte that comprises at least one dense layer having a total ion conductivity of at least 1 mS/cm at 25° C. and at least one porous layer having continuous and open pores having an average pore diameter between 1 and 50 ?m; providing an aqueous infiltration fluid comprising at least one organic additive that can be at least partially converted into carbon; introducing the aqueous infiltration fluid into the at least one porous layer of the multilayer solid ceramic electrolyte; and subjecting the multilayer solid ceramic electrolyte to a thermal treatment in the form of sintering in a reducing atmosphere at temperatures between 400° C. and 900° C., whereby the electrode material is synthesized from the precursor of the electrode material on the surface of the pores in situ.
    Type: Grant
    Filed: January 15, 2020
    Date of Patent: August 16, 2022
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Tu Lan, Qianli Ma, Frank Tietz, Olivier Guillon
  • Publication number: 20220093910
    Abstract: Provided is a method for producing an electrode for a solid-state battery comprising providing a multilayer solid ceramic electrolyte that comprises at least one dense layer having a total ion conductivity of at least 1 mS/cm at 25° C. and at least one porous layer having continuous and open pores having an average pore diameter between 1 and 50 ?m; providing an aqueous infiltration fluid comprising at least one organic additive that can be at least partially converted into carbon; introducing the aqueous infiltration fluid into the at least one porous layer of the multilayer solid ceramic electrolyte; and subjecting the multilayer solid ceramic electrolyte to a thermal treatment in the form of sintering in a reducing atmosphere at temperatures between 400° C. and 900° C., whereby the electrode material is synthesized from the precursor of the electrode material on the surface of the pores in situ.
    Type: Application
    Filed: January 15, 2020
    Publication date: March 24, 2022
    Inventors: Tu Lan, Qianli Ma, Frank Tietz, Olivier Guillon
  • Publication number: 20220032237
    Abstract: Disclosed are a CMS membrane, characterized in that it is obtainable by pyrolysis of a polyimide composed of the monomers 1-(4-aminophenyl)-1,3,3-trimethyl-2H-inden-5-amine and 5-(1,3-dioxo-2-benzofuran-5-carbonyl-2-benzofuran-1,3-dione of the following formulae: preferably by pyrolysis of the polyimide having the CAS number 62929-02-6, and a supported CMS membrane comprising a CMS membrane obtainable from a polyimide by pyrolysis and a porous support, characterized in that a mesoporous intermediate layer is provided between the CMS membrane and the porous support. Further disclosed are a process for preparing the supported membrane, the use of the membranes for separating gas mixtures or liquid mixtures, an apparatus for gas separation or for liquid separation, and the use of the polyimide for preparing a CMS membrane by pyrolysis.
    Type: Application
    Filed: September 16, 2019
    Publication date: February 3, 2022
    Inventors: Patrick Tchoua Ngamou, Mariya E. Ivanova, Wilhelm Albert Meulenberg, Olivier Guillon
  • Patent number: 11065686
    Abstract: A method for sintering metallic and/or non-oxide components includes completely encapsulating, in a metal halide salt, a green body comprising at least one metallic and/or non-oxide powder, and compressing the encapsulated green body so as to be gastight. The method further includes heating, together with a metal halide salt in the presence of oxygen up to sintering temperatures, the compressed, encapsulated green body. The method additionally includes at least partially dissolving, after cooling, the metal halide salt in a liquid so that the sintered component can be removed.
    Type: Grant
    Filed: June 8, 2018
    Date of Patent: July 20, 2021
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Apurv Dash, Jesus Gonzalez, Robert Vassen, Olivier Guillon
  • Publication number: 20210147301
    Abstract: The invention relates to a method for producing a non-oxide ceramic powder comprising a nitride, a carbide, a boride or at least one MAX phase with the general composition Mn+1AXn, where M=at least one element from the group of transition elements (Sc, Ti, V, Cr, Zr, Nb, Mo, Hf and Ta), A=at least one A group element from the group (Si, Al, Ga, Ge, As, Cd, In, Sn, Tl and Pb), X=carbon (C) and/or nitrogen (N) and/or boron (B), and n=1, 2 or 3. According to the invention, corresponding quantities of elementary starting materials or other precursors are mixed with at least one metal halide salt (NZ), compressed (pellet), and heated for synthesis with a metal halide salt (NZ). The compressed pellet is first enveloped with another metal halide salt, compressed again, arranged in a salt bath and heated therewith until the melting temperature of the salt is exceeded. Optionally, melted silicate can be added, which prevents the salt from evaporating at high temperatures.
    Type: Application
    Filed: June 7, 2018
    Publication date: May 20, 2021
    Inventors: Apurv DASH, Jesus GONZALEZ, Robert VASSEN, Olivier GUILLON
  • Patent number: 10752555
    Abstract: A method for producing a transparent polycrystalline ceramic includes forming at least one planar transparent region near a surface within the ceramic, wherein the at least one planar transparent region has a lower thermal expansion coefficient than other regions of the ceramic. The method further includes generating compressive stresses in the at least one planar transparent region near the surface after a thermal treatment and cooling.
    Type: Grant
    Filed: June 29, 2017
    Date of Patent: August 25, 2020
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Olivier Guillon, Marc Rubat Du Merac, Martin Bram
  • Publication number: 20200216942
    Abstract: A method for coating, with a coating material, a monocrystalline substrate surface of a component comprising a monocrystalline alloy includes polishing the monocrystalline substrate surface, transferring the substrate to a vacuum chamber, and heating the entire substrate to a temperature of at least half a melting temperature of the substrate but less than a melting temperature of the substrate. The method further includes applying the coating material in powder form onto the polished monocrystalline substrate surface by vacuum plasma spraying. The powder has a mean particle size in a range of 10 to 200 ?m. A pressure in a range of 1 to 200 mbar is set for the vacuum plasma spraying, and an argon atmosphere having a hydrogen content in a range of 10 to 50 vol. % is used as a working gas for the vacuum plasma spraying.
    Type: Application
    Filed: October 4, 2018
    Publication date: July 9, 2020
    Inventors: Tobias Kalfhaus, Robert Vassen, Olivier Guillon
  • Publication number: 20200171575
    Abstract: A method for sintering metallic and/or non-oxide components includes completely encapsulating, in a metal halide salt, a green body comprising at least one metallic and/or non-oxide powder, and compressing the encapsulated green body so as to be gastight. The method further includes heating, together with a metal halide salt in the presence of oxygen up to sintering temperatures, the compressed, encapsulated green body. The method additionally includes at least partially dissolving, after cooling, the metal halide salt in a liquid so that the sintered component can be removed.
    Type: Application
    Filed: June 8, 2018
    Publication date: June 4, 2020
    Inventors: Apurv DASH, Jesus GONZALEZ, Robert VASSEN, Olivier GUILLON
  • Patent number: 10566654
    Abstract: A method for preparing electrolyte material having a NASICON structure, based on a Na3+xScxZr2?x(SiO4)2(PO4) compound where 0?x<2. The method includes providing an acidic, aqueous solution which, according to a desired stoichiometry, comprises sodium, scandium and zirconium in the form of water-soluble nitrates, acetates or carbonates, and soluble silicates or orthosilicic acids or organic silicon compounds in dissolved form; subsequently adding phosphoric acid or ammonium dihydrogenphosphate or other soluble phosphates, according to the desired stoichiometry, complex zirconium dioxide phosphates forming as colloidal precipitations; and subsequently drying and calcining the mixture.
    Type: Grant
    Filed: August 27, 2016
    Date of Patent: February 18, 2020
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Qianli Ma, Frank Tietz, Sahir Naqash, Olivier Guillon
  • Patent number: 10403881
    Abstract: A method for producing a ceramic cathode layer on an electrically conductive substrate includes applying a coating to the electrically conductive substrate, the coating being in a form of a suspension including at least one suspending agent and at least one ceramic material. The method further includes heating the coating in a reducing atmosphere such that the ceramic material is completely or in part reduced to a fusible reaction product, heating the coating in a reducing atmosphere to temperatures above the melting point of the reaction product so as to form a melt, densifying or sintering the coating in a reducing atmosphere at temperatures that are 100° C. greater than a melting temperature of the reaction product, and reoxidizing the densified or sintered coating in an oxidizing atmosphere in a temperature range of between 400° C. and 1,200° C.
    Type: Grant
    Filed: December 9, 2016
    Date of Patent: September 3, 2019
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Juergen Dornseiffer, Hans-Gregor Gehrke, Manuel Krott, Olivier Guillon, Sven Uhlenbruck
  • Publication number: 20190127285
    Abstract: A method for producing a transparent polycrystalline ceramic includes forming at least one planar transparent region near a surface within the ceramic, wherein the at least one planar transparent region has a lower thermal expansion coefficient than other regions of the ceramic. The method further includes generating compressive stresses in the at least one planar transparent region near the surface after a thermal treatment and cooling.
    Type: Application
    Filed: June 29, 2017
    Publication date: May 2, 2019
    Inventors: Olivier GUILLON, Marc RUBAT DU MERAC, Martin BRAM
  • Patent number: 10270126
    Abstract: A method for preparing a lithium titanium phosphate, wherein a sol-gel process is used to prepare the phosphate, includes producing a sol from source materials; converting the sol to a gel; and drying the gel to obtain a corresponding powder comprising the lithium titanium phosphate. In a substep, the method further includes adding titanium(IV) isopropoxide to water to produce precipitates of titanium hydroxide oxide, cooling a system down to a temperature of less than 10° C., and redissolving the precipitates by adding nitric acid to form an aqueous TiO2+ nitrate solution. The lithium titanium phosphate has a general composition Li1+x+yMxTi2?x(PO4)3?y(SiO4)y, wherein M=Al, Ga, In, Sc, V, Cr, Mn, Co, Fe, Y, La—Lu, wherein 0?x?0.5, and wherein 0?y?0.5.
    Type: Grant
    Filed: August 19, 2015
    Date of Patent: April 23, 2019
    Assignee: FORSCHUNGSZENTRUM JUELICH GMBH
    Inventors: Qianli Ma, Frank Tietz, Olivier Guillon
  • Publication number: 20190013512
    Abstract: A method for producing a ceramic cathode layer on an electrically conductive substrate includes applying a coating to the electrically conductive substrate, the coating being in a form of a suspension including at least one suspending agent and at least one ceramic material. The method further includes heating the coating in a reducing atmosphere such that the ceramic material is completely or in part reduced to a fusible reaction product, heating the coating in a reducing atmosphere to temperatures above the melting point of the reaction product so as to form a melt, densifying or sintering the coating in a reducing atmosphere at temperatures that are 100° C. greater than a melting temperature of the reaction product, and reoxidizing the densified or sintered coating in an oxidizing atmosphere in a temperature range of between 400° C. and 1,200° C.
    Type: Application
    Filed: December 9, 2016
    Publication date: January 10, 2019
    Applicant: Forschungszentrum Juelich GmbH
    Inventors: Juergen Dornseiffer, Hans-Gregor Gehrke, Manuel Krott, Olivier Guillon, Sven Uhlenbruck