Patents by Inventor Patrick J. Jefferies

Patrick J. Jefferies has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 4632783
    Abstract: A method for sanitizing flush toilets wherein a sanitizing agent and a triphenylmethane dyestuff are dispensed separately from a dual dispensing means into the toilet flush water. The dyestuff is resistant to attack by the sanitizing agent and therefore provides an aesthetically pleasing color to the water remaining in the bowl during the time period between flushes.
    Type: Grant
    Filed: May 13, 1985
    Date of Patent: December 30, 1986
    Assignee: The Hilton-Davis Chemical Co.
    Inventors: William M. Hung, Patrick J. Jefferies
  • Patent number: 4536367
    Abstract: A method for sanitizing flush toilets wherein a sanitizing agent and a triphenylmethane dyestuff are dispensed separately from a dual dispensing means into the toilet flush water. The dyestuff is resistant to attack by the sanitizing agent and therefore provides an aesthetically pleasing color to the water remaining in the bowl during the time period between flushes.
    Type: Grant
    Filed: December 9, 1983
    Date of Patent: August 20, 1985
    Assignee: The Hilton-Davis Chemical Co.
    Inventors: William M. Hung, Patrick J. Jefferies
  • Patent number: 4528136
    Abstract: Process comprises the combination of the two steps of condensing Y-benzaldehyde with N-R.sup.2 -N-R.sup.3 -aniline and 3-N-R-N-R.sup.1 -benzoic acid, under acidic conditions to produce 2-[(Y-phenyl) (4-N-R.sup.2 -N-R.sup.3 -aminophenyl)methyl]-5-N-R-N-R.sup.1 -aminobenzoic acid, and oxidizing said benzoic acid to produce 3-(Y-phenyl)-3-(4-N-R.sup.2 -N-R.sup.3 -aminophenyl)-6-N-R-N-R.sup.1 -aminophthalide.
    Type: Grant
    Filed: April 14, 1983
    Date of Patent: July 9, 1985
    Assignee: The Hilton-Davis Chemical Co.
    Inventors: Paul J. Schmidt, Patrick J. Jefferies
  • Patent number: 4399291
    Abstract: Process comprises the combination of the two steps of condensing Y-benzaldehyde with N--R.sup.2 --N--R.sup.3 -aniline and 3--N--R--N--R.sup.1 -benzoic acid, under acidic conditions to produce 2-[(Y-phenyl) (4--N--R.sup.2 --N--R.sup.3 -aminophenyl)methyl]-5--N--R--N--R.sup.1 -aminobenzoic acid, and oxidizing said benzoic acid to produce 3-(Y-phenyl)-3-(4--N--R.sup.2 --N--R.sup.3 -aminophenyl)-6--N--R--N--R.sup.1 -aminophthalide.
    Type: Grant
    Filed: December 9, 1981
    Date of Patent: August 16, 1983
    Assignee: Sterling Drug Inc.
    Inventors: Paul J. Schmidt, Patrick J. Jefferies
  • Patent number: 4206144
    Abstract: N,N-Dialkyl-N-aminoalkyl-N-aminophenylalkyl quaternary ammonium salts and N-methyl-N-(3-aminophenoxy-2-hydroxy-1-propyl)-N,N-bis(3-aminopropyl) quaternary ammonium salts and their N-nitrophenylalkyl and N-(3-nitrophenoxy) precussor quaternary ammonium salts, respectively are intermediates to water-soluble azo-dyestuffs useful for coloring natural fibers, synthetic fiber-forming materials and cellulosic materials. These dyes dye cotton and paper various shades of yellows, reds, and oranges with less prone to bleed and with a high degree of discharge when bleached with hypochlorite or chlorine bleaches.
    Type: Grant
    Filed: November 22, 1978
    Date of Patent: June 3, 1980
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse
  • Patent number: 4146558
    Abstract: Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.K is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.
    Type: Grant
    Filed: October 6, 1977
    Date of Patent: March 27, 1979
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse
  • Patent number: 4143034
    Abstract: Novel mixtures, which consist essentially of a monoazo compound selected from the group of 1-phenylazo-2-hydroxynaphthalenes or of a disazo compound selected from the group of various bis-phenyl and bridged bis-phenyl diamines diazotized and coupled to .beta.-naphthols, acetoacetanilides or 1-phenyl-3-methyl-5-pyrazolones and N,N'-bis(4-phenylazo-3-hydroxy-2-naphthocarbonyl)diaminoethanes multiply and randomly substituted with an average of one to eight aminomethyl groups per molecule or the acid-addition salts thereof, obtained by polyaminomethylating monoazo or disazo compounds, are useful for coloring natural fibers, synthetic fiber-forming material and cellulosic materials as well as in the manufacture of paper, varnishes, inks, coatings and plastics.
    Type: Grant
    Filed: March 9, 1977
    Date of Patent: March 6, 1979
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nicholas A. Ambrosiano
  • Patent number: 4103092
    Abstract: Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature or A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.
    Type: Grant
    Filed: July 14, 1975
    Date of Patent: July 25, 1978
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse
  • Patent number: 4065500
    Abstract: Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.degree. is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.degree.Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.
    Type: Grant
    Filed: March 31, 1976
    Date of Patent: December 27, 1977
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse
  • Patent number: 3996282
    Abstract: Water-soluble cationic dyestuffs of the formulae ##STR1## WHEREIN R.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NR.sup.0 Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##STR2## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.K is a small integer whose value is dependent on the nature of A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.
    Type: Grant
    Filed: July 5, 1974
    Date of Patent: December 7, 1976
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse
  • Patent number: 3935182
    Abstract: Water-soluble cationic dyestuffs of the formulae ##SPC1##WhereinR.sup.0 is hydrogen, lower-alkyl or hydroxy-lower-alkyl;R.sup.1 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.2 is lower-alkyl, lower-alkenyl, hydroxy-lower-alkyl or -(lower-alkylene)-NRO Y or R.sup.1 and R.sup.2 together with the nitrogen atom, are pyrrolidino, piperidino or 4-lower-alkanoyl piperazino;Y is hydrogen or ##EQU1## wherein R is hydrogen, lower-alkyl, lower-alkenyl, phenyl or phenyl-lower-alkyl;A is a member selected from the group consisting of an aromatic azo dyestuff residue attached to the quaternary ammonium nitrogen atom through a lower-alkylene bridge.k is a small integer whose value is dependent on the nature or A such that it has a range from one to two;R.sup.8 is lower-alkyl, lower-alkenyl or hydroxy-lower-alkyl;R.sup.9 is lower-alkyl, hydroxy-lower-alkyl or NH.sub.2 ;R.sup.10 is lower-alkyl or lower-alkenyl;A.sup.
    Type: Grant
    Filed: February 14, 1973
    Date of Patent: January 27, 1976
    Assignee: Sterling Drug Inc.
    Inventors: Patrick J. Jefferies, Nathan N. Crounse