Abstract: A system and method for collecting a selected phase of a representative sample from a multiphase fluid flowing through a flowline, preferably located subsea. The system includes a multiphase sampling apparatus attachable to the flowline for sampling the representative sample; a vehicle sampling apparatus (e.g., ROV) locatable proximate the flowline having a power supply and a fluid sample collector for storing at least one selected phase of the representative sample; an interface for connecting the multiphase sampling apparatus and the vehicle sampling apparatus; and a temperature control arrangement disposed between the multiphase sampling apparatus and the vehicle sampling apparatus configured to minimize the temperature difference between the representative sample and the multiphase fluid flowing through the flowline.

Abstract: A system and method for collecting a selected phase of a representative sample from a multiphase fluid flowing through a flowline, preferably located subsea. The system includes a multiphase sampling apparatus attachable to the flowline for sampling the representative sample; a vehicle sampling apparatus (e.g., ROV) locatable proximate the flowline having a power supply and a fluid sample collector for storing at least one selected phase of the representative sample; an interface for connecting the multiphase sampling apparatus and the vehicle sampling apparatus; and a temperature control arrangement disposed between the multiphase sampling apparatus and the vehicle sampling apparatus configured to minimize the temperature difference between the representative sample and the multiphase fluid flowing through the flowline.

Abstract: An injector (101) for injecting a sample into a chromatography column (161) comprises a sample inlet (105) for feeding the sample into the injector (101), an injection chamber (107) comprises a packing (119) for separating the sample into components thereof, and a first sample outlet (109) intended to be in fluid communication with the chromatography column (161). The injector (101) may be used in a chromatography system (159) for analyzing a sample.

Abstract: A system and method are provided for collecting fluid samples from a fluid flowline located subsea. The system includes a multiphase sampling apparatus attachable to the flowline, and a vehicle sampling apparatus that is connectable to the multiphase sampling apparatus to allow the transfer of the collected fluid sample thereto. The vehicle sampling apparatus is preferably a subsea remotely operated vehicle (ROV) locatable proximate the fluid flowline and having a fluid sample collector and a fluid pump for transferring the collected fluid sample from the multiphase sampling apparatus to the fluid sample collector. The vehicle sampling apparatus includes a fluid analysis sensor capable of extracting information about the collected fluid sample at a subsea location. Optionally, the vehicle sampling apparatus can transport the collected fluid sample to a location remote from the fluid flowline for analysis.

Abstract: A carbon nanostructured micro-fabricated gas chromatography column which is particularly well-suited to the surface well-site and/or the downhole analysis of natural gas in oilfield or gasfield applications (but which may also be used in non-oilfield or non-gasfield situations) is described. This micro-fabricated column integrates a micro-structured substrate such as a silicon substrate with carbon nanotubes as an active nanostructured material in a micro-channel. Benefits of the present invention include enhanced separation of alkanes and isomers, particularly below hexane (i.e., below C6), as well as the separation of carbon dioxide, hydrogen sulfide, and water and other substances present in natural gas. The chromatography column of the present invention is in one embodiment a part of an entire gas chromatograph system that in its simplest form also comprises an injector and a detector. Preferably the injector, separation column, and detector are all micro-fabricated on a substrate.

Abstract: To take a sample of liquid and/or gaseous hydrocarbon at the surface or down an oil well, use is made of a flexible bag suspended by a tube from a top region of a wall of a closed receptacle. The bag and the tube are made of a flexible material that is leakproof and inert relative to the sample to be taken, such as a cross-linked polymer. The volume of sample admitted into the bag is controlled so as to avoid stretching the wall of the bag.

Abstract: A sample of fluid such as a gaseous fluid leaving a liquid/gas separator in a surface installation of an oil well, is taken continuously via a sampling tube. The tube opens out on the axis of a gas outlet pipe, facing towards the separator receptacle and located at the junction between the pipe and the receptacle. Sampling is performed isokinetically by regulating the flow rate in the tube by means of a regulator valve controlled by a regulator as a function of flow rates measured in the tube and in the pipe. In the tube, liquid is separated from the gas by means of a filter.

Abstract: A liquid sample to be analyzed is subjected to a vaporizing step. The vaporized components are submitted to a first separation stage by introducing said components into a packed chromatography column and flowing carrier gas through said column. The effluent of the first stage is passed through a flow dividing chamber. A second separation stage is performed by passing the effluent of the flow dividing chamber to a capillary chromatography column and flowing carrier gas therethrough. After a predetermined period of time, flushing gas is introduced through the flow dividing chamber and flowed through the first-stage packed column in a direction opposite to the original direction of flow while the direction of flow remains unchanged in the capillary column.