Patents by Inventor Paul F. Becher

Paul F. Becher has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 7968484
    Abstract: A high-strength, fracture-resistant silicon nitride ceramic material that includes about 5 to about 75 wt-% of elongated reinforcing grains of beta-silicon nitride, about 20 to about 95 wt-% of fine grains of beta-silicon nitride, wherein the fine grains have a major axis of less than about 1 micron; and about 1 to about 15 wt-% of an amorphous intergranular phase comprising Si, N, O, a rare earth element and a secondary densification element. The elongated reinforcing grains have an aspect ratio of 2:1 or greater and a major axis measuring about 1 micron or greater. The elongated reinforcing grains are essentially isotropically oriented within the ceramic microstructure. The silicon nitride ceramic exhibits a room temperature flexure strength of 1,000 MPa or greater and a fracture toughness of 9 MPa-m(1/2) or greater. The silicon nitride ceramic exhibits a peak strength of 800 MPa or greater at 1200 degrees C.
    Type: Grant
    Filed: September 7, 2007
    Date of Patent: June 28, 2011
    Assignee: UT-Battelle, LLC
    Inventors: Paul F. Becher, Hua-Tay Lin
  • Publication number: 20100267543
    Abstract: A high-strength, fracture-resistant silicon nitride ceramic material that includes about 5 to about 75 wt-% of elongated reinforcing grains of beta-silicon nitride, about 20 to about 95 wt-% of fine grains of beta-silicon nitride, wherein the fine grains have a major axis of less than about 1 micron; and about 1 to about 15 wt-% of an amorphous intergranular phase comprising Si, N, O, a rare earth element and a secondary densification element. The elongated reinforcing grains have an aspect ratio of 2:1 or greater and a major axis measuring about 1 micron or greater. The elongated reinforcing grains are essentially isotropically oriented within the ceramic microstructure. The silicon nitride ceramic exhibits a room temperature flexure strength of 1,000 MPa or greater and a fracture toughness of 9 MPa-m(1/2) or greater. The silicon nitride ceramic exhibits a peak strength of 800 MPa or greater at 1200 degrees C.
    Type: Application
    Filed: September 7, 2007
    Publication date: October 21, 2010
    Inventors: PAUL F. BECHER, HUA-TAY LIN
  • Patent number: 5905937
    Abstract: A method of making an intermetallic-bonded ceramic composite involves combining a particulate brittle intermetallic precursor with a particulate reactant metal and a particulate ceramic to form a mixture and heating the mixture in a non-oxidizing atmosphere at a sufficient temperature and for a sufficient time to react the brittle intermetallic precursor and the reactant metal to form a ductile intermetallic and sinter the mixture to form a ductile intermetallic-bonded ceramic composite.
    Type: Grant
    Filed: January 6, 1998
    Date of Patent: May 18, 1999
    Assignee: Lockheed Martin Energy Research Corporation
    Inventors: Kevin Plucknett, Terry N. Tiegs, Paul F. Becher
  • Patent number: 5538533
    Abstract: An improved ceramic composite comprising oxide ceramic particulates, nonoxide ceramic particulates selected from the group consisting of carbides, borides, nitrides of silicon and transition metals and mixtures thereof, and a ductile binder selected from the group consisting of metallic, intermetallic alloys and mixtures thereof is described. The ceramic composite is made by blending powders of the ceramic particulates and the ductile to form a mixture and consolidating the mixture of under conditions of temperature and pressure sufficient to produce a densified ceramic composite.
    Type: Grant
    Filed: September 11, 1995
    Date of Patent: July 23, 1996
    Assignee: Martin Marietta Energy Systems, Inc.
    Inventors: Kathleen B. Alexander, Terry N. Tiegs, Paul F. Becher, Shirley B. Waters
  • Patent number: 5482673
    Abstract: A process for preparing ceramic composite comprising blending TiC particulates, Al.sub.2 O.sub.3 particulates and nickle aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m.sup.1/2, a hardness equal to or greater than 18 GPa.
    Type: Grant
    Filed: May 27, 1994
    Date of Patent: January 9, 1996
    Assignee: Martin Marietta Energy Systems, Inc.
    Inventors: Kathleen B. Alexander, Terry N. Tiegs, Paul F. Becher, Shirley B. Waters
  • Patent number: 4971933
    Abstract: A ternary ceramic alloy which produces toughening of zirconia and zirconia composites through the stress transformation from tetragonal phase to monoclinic phase. This alloy, having the general formula Ce.sub.x Hf.sub.y Zn.sub.1-x-y O.sub.2, is produced through the addition of appropriate amounts of ceria and hafnia to the zirconia. Typically, improved toughness is achieved with about 5 to about 15 mol % ceria and up to about 40 mol % hafnia. The preparation of alloys of these compositions are given together with data as to the densities, tetragonal phase content, hardness and fracture toughness. The alloys are useful in preparing zirconia bodies as well as reinforcing ceramic composites.
    Type: Grant
    Filed: March 14, 1989
    Date of Patent: November 20, 1990
    Assignee: Martin Marietta Energy Systems, Inc.
    Inventors: Paul F. Becher, Eric F. Funkenbusch
  • Patent number: 4812280
    Abstract: A process for manufacturing large, fully dense, high purity TiB.sub.2 articles by pressing powders with a sintering aid at relatively low temperatures to reduce grain growth. The process requires stringent temperature and pressure applications in the hot-pressing step to ensure maximum removal of sintering aid and to avoid damage to the fabricated article or the die.
    Type: Grant
    Filed: April 17, 1986
    Date of Patent: March 14, 1989
    Assignee: The United States of America as represented by the Department of Energy
    Inventors: Arthur J. Moorhead, E. S. Bomar, Paul F. Becher
  • Patent number: 4657877
    Abstract: The flexural strength and/or fracture toughness of SiC whisker-reinforced composites utilizing mullite or alumina as the matrix material for the composite are increased by the addition of zirconia in a monoclinic or tetragonal phase to the matrix. The zirconia addition also provides for a lower hot-pressing temperature and increases the flexural strength and/or fracture toughness of the SiC whisker-reinforced composites over SiC whisker-reinforced composites of the similar matrix materials reinforced with similar concentrations of SiC whiskers.
    Type: Grant
    Filed: May 21, 1986
    Date of Patent: April 14, 1987
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Paul F. Becher, Terry N. Tiegs