Abstract: In an apparatus for microwave-assisted preparation of specimens with a microwave generator (1), a microwave chamber for receiving specimens (5) to be processed, and a container arrangement (11) for a number of containers (9) for liquids, the microwave chamber is realized as a waveguide (2) that includes a first opening (7a) for introduction of a specimen (5) and a second opening (8a), preferably arranged at the bottom, through which a liquid container (9) is reversibly introduced into the microwave chamber while the specimen (5) is held stationary, until the liquid container thus introduced into the microwave chamber, and the liquid contained therein, surround the specimen (5).

Abstract: In an apparatus for microwave-assisted preparation of specimens with a microwave generator (1), a microwave chamber for receiving specimens (5) to be processed, and a container arrangement (11) for a number of containers (9) for liquids, the microwave chamber is realized as a waveguide (2) that comprises a first opening (7a) for introduction of a specimen (5) and a second opening (8a), preferably arranged at the bottom, through which a liquid container (9) is reversibly introduced into the microwave chamber while the specimen (5) is held stationary, until the liquid container thus introduced into the microwave chamber, and the liquid contained therein, surround the specimen (5).

Abstract: In an apparatus for microwave-assisted preparation of specimens, the microwave chamber for reception of specimens to be processed is embodied as a waveguide (3), in particular as a monomode waveguide, and is equipped with at least one opening (3a) for introduction of the at least one specimen (11) into the waveguide. A cooling circuit comprises a cooling means (8) adapted to cool the fluid (12), which fluid surrounds the at least one specimen and is separated from the cooling liquid of the cooling circuit, in the region of the at least one specimen (11) inside the waveguide. The opening (3a) can be sealed in microwave-tight fashion, by means of a closure means (7), during operation of the apparatus.

Abstract: The invention relates to a line element for handling fluids, in particular for digestion or for synthesis of substances in chemical process engineering, said line element comprising at least one temperature-resistant and pressure-resistant support element (15) that has a first interior in which an inner line (14) made of a plastic material resistant to chemicals is arranged, at least one free end of the line element being provided with a connector element (16) that has a second interior into which the inner line (14) extends, the line element according to the invention being characterized in that the support element (15) and/or the connector element (16) has at least one relief opening (25, 26) which ensures a communicating link between the first interior of the support element (15), or second interior of the connector element (16), and the environment.

Abstract: The present invention concerns a device for monitoring the pressure in at least two pressure-tight analysis vessels, that have been sealed by means of lids, whereby heat is supplied to the analysis vessels by means of a heating apparatus. The internal pressure of the analysis vessel acts on its lid. The lid is connected to a piston in a closed hydraulic system. The force, that is dependent on the internal pressure of the analysis vessel, is transferred by the lid to the piston in the hydraulic system. A lid and a piston are assigned to every analysis vessel. In addition, a stop device is assigned to each piston, whereby the stop device limits the outward movement of the piston in the event of excess pressure in the hydraulic system relative to the internal pressure of the analysis vessel. The pistons are connected to one another via the hydraulic system.

Abstract: The present invention concerns a device for measuring the pressure and temperature in at least one pressure-tight analysis vessel, that has been sealed by means of a lid, whereby heat is supplied to the analysis vessel by means of a microwave oven. The device comprises a measurement device that is connected to a unit for controlling the microwave oven. In this regard, the measurement device is arranged in a microwave-tight housing inside the microwave field that is produced by the microwave oven. The housing is constructed in such a way that it forms a shield that is impermeable for the microwave field. A microwave-free zone is produced inside the housing. Electronic, current-carrying components can be arranged in the microwave-tight housing without, as a result, generating interference in the microwave field.