Patents by Inventor Philip De Smedt

Philip De Smedt has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 10544067
    Abstract: The present invention is a process for dehydrating an alcohol to prepare corresponding olefin(s), comprising: (a) providing a feed (A) comprising at least an alcohol having at least 2 carbon atoms, and preferably at most 5 carbon atoms, or a mixture thereof optionally water, optionally an inert component, in a dehydration unit, (b) placing the feed (A) into contact with an acidic catalyst in a reaction zone of said dehydration unit at conditions effective to dehydrate at least a portion of the alcohol to make an olefin or a mixture of olefins having the same number of carbon atoms as the alcohol, (c) recovering from said dehydration unit an effluent (B) comprising: an olefin or a mixture of olefins, water, undesired by-products including aldehydes and lighter products resulting from degradation of said aldehydes under the conditions of step (b), optionally unconverted alcohol(s) if any, optionally the inert component, wherein, said feed (A)-providing step (a) comprises adding an effective amount of one
    Type: Grant
    Filed: December 18, 2015
    Date of Patent: January 28, 2020
    Assignee: TOTAL RESEARCH & TECHNOLOGY FELUY
    Inventors: Delphine Minoux, Nikolai Nesterenko, Cindy Adam, Walter Vermeiren, Philip De Smedt, Jean-Pierre Dath, Vincent Coupard, Sylvie Maury, Nicolas Aribert
  • Patent number: 10472300
    Abstract: The present invention is a process for dehydrating an alcohol to prepare a corresponding olefin, comprising: (a) providing a composition (A) comprising at least an alcohol having at least 2 carbon atoms, optionally water, optionally an inert component, in a dehydration unit, (b) placing the composition (A) into contact with an acidic catalyst in a reaction zone of said dehydration unit at conditions effective to dehydrate at least a portion of the alcohol to make a corresponding olefin, (c) recovering from said dehydration unit an effluent (B) comprising: at least an olefin, water, undesired by-products including aldehydes and light products, optionally unconverted alcohol(s), optionally the inert component, wherein, said composition (A)—providing step (a) comprises adding an effective amount of one or more sulfur containing compound capable to reduce the undesired by-products by comparison with a non introduction of such sulfur containing compound.
    Type: Grant
    Filed: December 18, 2015
    Date of Patent: November 12, 2019
    Assignees: Total Research & Technology Feluy, IFP Energies Nouvelles
    Inventors: Delphine Minoux, Nikolai Nesterenko, Cindy Adam, Walter Vermeiren, Philip De Smedt, Jean-Pierre Dath, Vincent Coupard, Sylvie Maury, Nicolas Aribert
  • Publication number: 20190092706
    Abstract: The present invention is a process for dehydrating an alcohol to prepare corresponding olefin(s), comprising: (a) providing a feed (A) comprising at least an alcohol having at least 2 carbon atoms, and preferably at most 5 carbon atoms, or a mixture thereof optionally water, optionally an inert component, in a dehydration unit, (b) placing the feed (A) into contact with an acidic catalyst in a reaction zone of said dehydration unit at conditions effective to dehydrate at least a portion of the alcohol to make an olefin or a mixture of olefins having the same number of carbon atoms as the alcohol, (c) recovering from said dehydration unit an effluent (B) comprising : an olefin or a mixture of olefins, water, undesired by-products including aldehydes and lighter products resulting from degradation of said aldehydes under the conditions of step (b), optionally unconverted alcohol(s) if any, optionally the inert component, wherein, said feed (A)-providing step (a) comprises adding an effective amount
    Type: Application
    Filed: December 18, 2015
    Publication date: March 28, 2019
    Inventors: Delphine Minoux, Nikolai Nesterenko, Cindy Adam, Walter Vermeiren, Philip De Smedt, Jean-Pierre Dath, Vincent Coupard, Sylvie Maury, Nicolas Aribert
  • Publication number: 20170355650
    Abstract: The present invention is a process for dehydrating an alcohol to prepare a corresponding olefin, comprising: (a) providing a composition (A) comprising at least an alcohol having at least 2 carbon atoms, optionally water, optionally an inert component, in a dehydration unit, (b) placing the composition (A) into contact with an acidic catalyst in a reaction zone of said dehydration unit at conditions effective to dehydrate at least a portion of the alcohol to make a corresponding olefin, (c) recovering from said dehydration unit an effluent (B) comprising : at least an olefin, water, undesired by-products including aldehydes and light products, optionally unconverted alcohol(s), optionally the inert component, wherein, said composition (A)-providing step (a) comprises adding an effective amount of one or more sulfur containing compound capable to reduce the undesired by-products by comparison with a non introduction of such sulfur containing compound.
    Type: Application
    Filed: December 18, 2015
    Publication date: December 14, 2017
    Inventors: Delphine Minoux, Nikolai Nesterenko, Cindy Adam, Walter Vermeiren, Philip De Smedt, Jean-Pierre Dath, Vincent Coupard, Sylvie Maury, Nicolas Aribert
  • Patent number: 9725376
    Abstract: The invention relates to a process for dehydration of an ethanol feedstock into ethylene comprising at least the stages: a) A stage for pretreatment of the ethanol feedstock on an acidic solid, b) A stage for evaporation of said pretreated ethanol feedstock in a heat exchanger, c) A stage for superheating said evaporated feedstock in such a way as to bring it to an inlet temperature that is compatible with the temperature of a dehydration reaction, d) A stage for dehydration of said feedstock that is obtained from stage c) in at least one adiabatic reactor that contains at least one dehydration catalyst.
    Type: Grant
    Filed: November 18, 2013
    Date of Patent: August 8, 2017
    Assignees: IFP Energies Nouvelles, Total Research & Technology Feluy
    Inventors: Vincent Coupard, Natacha Touchais, Thomas Plennevaux, Emilie Kobel, Stephanie Fleurier, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam, Nikolai Nesterenko
  • Patent number: 9663414
    Abstract: A process for dehydration of an ethanol feedstock to ethylene by: a) preheating ethanol feedstock by heat exchange with effluent from e), b) pretreating the ethanol feedstock to produce pretreated ethanol feedstock, c) vaporizing a vaporization feedstock containing pretreated ethanol feedstock and at least a portion of the flow of treated water recycled in an exchanger to produce a vaporized feedstock, d) compressing said vaporized feedstock to produce a compressed feedstock, e) dehydrating said compressed feedstock in at least one adiabatic reactor, f) separating the effluent from the last adiabatic reactor of e) into an effluent containing ethylene and an effluent containing water, g) purifying at least a portion of the effluent containing water from 0 and separating at least one flow of treated water and at least one flow of unconverted ethanol, h) recycling at least a portion of the flow of treated water from g) upstream of c).
    Type: Grant
    Filed: November 18, 2013
    Date of Patent: May 30, 2017
    Assignees: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent Coupard, Natacha Touchais, Thomas Plennevaux, Emilie Kobel, Stephanie Fleurier, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam, Nikolai Nesterenko
  • Patent number: 9650311
    Abstract: Process for the production of ethylene from an ethanol feedstock that comprises these stages: a) dehydration to produce at least ethylene and water effluents, b) partial condensation of said ethylene effluent, c) separating phases of said partially condensed ethylene effluent to produce gas and liquid effluents, d) compression of said gas effluent to produce compressed gas effluent, e) washing said compressed gas effluent by contact with the recycled washing water of stage h) to produce washed gas and waste water effluents, f) absorption of said washed gas effluent by contact with at least an absorbent solution to produce purified gas effluent, g) distilling said waste water effluent and, jointly, said water effluent from said dehydration stage to produce at least gas distillate, liquid distillate, purified water effluent, and distillation residue, h) recycling, as washing water, at least a portion of said purified water effluent upstream from the washing stage e).
    Type: Grant
    Filed: January 10, 2014
    Date of Patent: May 16, 2017
    Assignees: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent Coupard, Thomas Plennevaux, Stephanie Fleurier, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam, Nikolai Nesterenko
  • Publication number: 20150353443
    Abstract: Process for the production of ethylene from an ethanol feedstock that comprises these stages: a) dehydration to produce at least ethylene and water effluents, b) partial condensation of said ethylene effluent, c) separating phases of said partially condensed ethylene effluent to produce gas and liquid effluents, d) compression of said gas effluent to produce compressed gas effluent, e) washing said compressed gas effluent by contact with the recycled washing water of stage h) to produce washed gas and waste water effluents, f) absorption of said washed gas effluent by contact with at least an absorbent solution to produce purified gas effluent, g) distilling said waste water effluent and, jointly, said water effluent from said dehydration stage to produce at least gas distillate, liquid distillate, purified water effluent, and distillation residue, h) recycling, as washing water, at least a portion of said purified water effluent upstream from the washing stage e).
    Type: Application
    Filed: January 10, 2014
    Publication date: December 10, 2015
    Applicants: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent COUPARD, Thomas PLENNEVAUX, Stephanie FLEURIER, Walter VERMEIREN, Delphine MINOUX, Philip DE SMEDT, Cindy ADAM, Nikolai NESTERENKO
  • Publication number: 20150299068
    Abstract: A process for dehydration of an ethanol feedstock to ethylene by: a) preheating ethanol feedstock by heat exchange with effluent from e), b) pretreating the ethanol feedstock to produce pretreated ethanol feedstock, c) vaporizing a vaporization feedstock containing pretreated ethanol feedstock and at least a portion of the flow of treated water recycled in an exchanger to produce a vaporized feedstock, d) compressing said vaporized feedstock to produce a compressed feedstock, e) dehydrating said compressed feedstock in at least one adiabatic reactor, f) separating the effluent from the last adiabatic reactor of e) into an effluent containing ethylene and an effluent containing water, g) purifying at least a portion of the effluent containing water from 0 and separating at least one flow of treated water and at least one flow of unconverted ethanol, h) recycling at least a portion of the flow of treated water from g) upstream of c).
    Type: Application
    Filed: November 18, 2013
    Publication date: October 22, 2015
    Applicants: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent COUPARD, Natacha TOUCHAIS, Thomas PLENNEVAUX, Emilie KOBEL, Stephanie FLEURIER, Walter VERMEIREN, Delphine MINOUX, Philip DE SMEDT, Cindy ADAM, Nikolai NESTERENKO
  • Publication number: 20150291485
    Abstract: The invention relates to a process for dehydration of an ethanol feedstock into ethylene comprising at least the stages: a) A stage for pretreatment of the ethanol feedstock on an acidic solid, b) A stage for evaporation of said pretreated ethanol feedstock in a heat exchanger, c) A stage for superheating said evaporated feedstock in such a way as to bring it to an inlet temperature that is compatible with the temperature of a dehydration reaction, d) A stage for dehydration of said feedstock that is obtained from stage c) in at least one adiabatic reactor that contains at least one dehydration catalyst.
    Type: Application
    Filed: November 18, 2013
    Publication date: October 15, 2015
    Applicants: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent Coupard, Natacha Touchais, Thomas Plennevaux, Emilie Kobel, Stephanie Fleurier, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam, Nikolai Nesterenko
  • Patent number: 9085502
    Abstract: A process for dehydration of an ethanol feedstock into ethylene, comprising the vaporization of said ethanol feedstock in a mixture with at least a portion of the recycled purified water stream from heat exchange with the effluent that is obtained from the last reactor.
    Type: Grant
    Filed: July 20, 2012
    Date of Patent: July 21, 2015
    Assignees: TOTAL PETROCHEMICALS RESEARCH FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent Coupard, Natacha Touchais, Stephanie Fleurier, Helena Gonzalez Penas, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam
  • Patent number: 9079812
    Abstract: A process for dehydration of an ethanol feedstock into ethylene, comprising the vaporization of said dilute hydrated ethanol feedstock in an exchanger, with heat exchange with the effluent that is obtained from a last reactor, with said mixture being introduced into said vaporization stage at a pressure that is lower than the pressure of the effluent that is obtained from the last reactor, the compression of the mixture that is vaporized in a compressor, the introduction of the vaporized and compressed mixture, into at least one adiabatic reactor that contains at least one dehydration catalyst.
    Type: Grant
    Filed: October 5, 2012
    Date of Patent: July 14, 2015
    Assignees: TOTAL RESEARCH & TECHNOLOGY FELUY, IFP ENERGIES NOUVELLES
    Inventors: Vincent Coupard, Natacha Touchais, Stephanie Fleurier, Helena Gonzalez Penas, Philip De Smedt, Walter Vermeiren, Cindy Adam, Delphine Minoux
  • Publication number: 20130190547
    Abstract: A process for dehydration of an ethanol feedstock into ethylene, comprising the vaporization of said ethanol feedstock in a mixture with at least a portion of the recycled purified water stream from heat exchange with the effluent that is obtained from the last reactor.
    Type: Application
    Filed: July 20, 2012
    Publication date: July 25, 2013
    Applicants: IFP Energies nouvelles, TOTAL PETROCHEMICALS RESEARCH FELUY
    Inventors: Vincent COUPARD, Natacha Touchais, Stephanie Fleurier, Helena Gonzalez Penas, Walter Vermeiren, Delphine Minoux, Philip De Smedt, Cindy Adam