Abstract: A centrifugal testing device for simulating ground subsidence induced by buried pipeline leakage and infiltration includes a model box provided with a transparent observation window at a front side, a chamber partitioning plate, a damaged pipeline model, permeable plates, and a water-soil separation device. A front part of the model box is divided into a test soil chamber for filling model soil and seepage chambers located at two sides of the test soil chamber. A rear part of the model box is divided into a soil filtration chamber and water circulation supply chambers located at two sides of the soil filtration chamber. The damaged pipeline model includes a front end provided with an electric push rod for controlling a crack of the damaged pipeline model to be opened and closed and a rear end provided with a ball valve device and connected to a water pump.

Abstract: A centrifugal testing device for simulating ground subsidence induced by buried pipeline leakage and infiltration includes a model box provided with a transparent observation window at a front side, a chamber partitioning plate, a damaged pipeline model, permeable plates, and a water-soil separation device. A front part of the model box is divided into a test soil chamber for filling model soil and seepage chambers located at two sides of the test soil chamber. A rear part of the model box is divided into a soil filtration chamber and water circulation supply chambers located at two sides of the soil filtration chamber. The damaged pipeline model includes a front end provided with an electric push rod for controlling a crack of the damaged pipeline model to be opened and closed and a rear end provided with a ball valve device and connected to a water pump.

Abstract: A method for synthesizing pitavastatin tert-butyl ester includes obtaining a substance B through reacting (4R-CIS)-6-chloromethyl-2,2-dimethyl-1,3-dioxolane-4-acetic acid tert-butyl ester with a substance A under the action of a first base catalyst, 5 oxidizing with an oxidizing agent to obtain a substance C, then reacting with 2-cyclopropyl-4-(4-fluorophenyl)-quinoline-3-formaldehyde under the action of a second base catalyst to obtain a substance D, and finally, carrying out an acid deprotection to obtain pitavastatin t-butyl ester. The reaction conditions of the present invention are mild and controllable, and the reaction conditions of the synthesis of the Julia olefination do 10 not require an ultra-low temperature reaction. The operation is convenient and simple, the stereoselectivity is good, the yield is high, and the synthesized pitavastatin t-butyl ester is a completely non-cis isomer, and its purity is high.

Abstract: The present disclosure provides methods, electrodes, and systems for electrochemical oxidation of polyfluoroalkyl and perfluroalkyl (PFAS) contaminants using Magnéli phase titanium suboxide ceramic electrodes/membranes. Magnéli phase titanium suboxide ceramic electrodes/membranes can be porous and can be included in reactive electrochemical membrane filtration systems for filtration, concentration, and oxidation of PFASs and other contaminants.

Abstract: The present disclosure provides methods, electrodes, and systems for electrochemical oxidation of polyfluoroalkyl and perfluroalkyl (PFAS) contaminants using Magnéli phase titanium suboxide ceramic electrodes/membranes. Magneli phase titanium suboxide ceramic electrodes/membranes can be porous and can be included in reactive electrochemical membrane filtration systems for filtration, concentration, and oxidation of PFASs and other contaminants.

Abstract: REM systems for disinfecting water, which includes a tank, a membrane anode, a cathode, and a conductive contactor, is disclosed. The conductive contactor is in direct contact with the membrane anode. The conductive contactor is in electrical communication with the cathode. The REM systems can further contain an inlet and an outlet for supplying water into the tank and removing water out of the tank respectively. The membrane anode includes a carbon-based material. In the most preferred embodiment, the membrane anode includes layers of activated carbon fiber cloth (ACFC). The membrane anode functions as both the anodic electrode that produces electrochemical reaction and the membrane filter. In one preferred embodiment, the membrane anode generates reactive oxygen species from water oxidation reaction that is effective in disinfecting pathogens in water. Methods of making and using the REM systems are also disclosed.

Abstract: Method for Synthesizing Pitavastatin t-Butyl Ester A method for synthesizing pitavastatin tert-butyl ester includes obtaining a substance B through reacting (4R-CIS)-6-chloromethyl-2,2-dimethyl-1,3-dioxolane-4-acetic acid tert-butyl ester with a substance A under the action of a first base catalyst, 5 oxidizing with an oxidizing agent to obtain a substance C, then reacting with 2-cyclopropyl-4-(4-fluorophenyl)-quinoline-3-formaldehyde under the action of a second base catalyst to obtain a substance D, and finally, carrying out an acid deprotection to obtain pitavastatin t-butyl ester. The reaction conditions of the present invention are mild and controllable, and the reaction conditions of the synthesis of the Julia olefination do 10 not require an ultra-low temperature reaction. The operation is convenient and simple, the stereoselectivity is good, the yield is high, and the synthesized pitavastatin t-butyl ester is a completely non-cis isomer, and its purity is high.

Abstract: The present disclosure provides methods, electrodes, and systems for electrochemical oxidation of polyfluoroalkyl and perfluroalkyl (PFAS) contaminants using Magnéli phase titanium suboxide ceramic electrodes/membranes. Magneli phase titanium suboxide ceramic electrodes/membranes can be porous and can be included in reactive electrochemical membrane filtration systems for filtration, concentration, and oxidation of PFASs and other contaminants.

Abstract: The present disclosure includes methods and compositions for reducing turf thatch and/or preventing turf thatch buildup. The compositions include isolated fungal laccase enzymes, such as laccase enzymes from white rot fungi. Methods of reducing and/or preventing turf thatch buildup include applying compositions including isolated fungal laccase enzymes to turfgrass.

Abstract: Various embodiments provide methods for removing a PFC by concentration and separation. In an exemplary method, a PFC in an aqueous solution or in a mixed water-organic solvent solution can be adsorbed onto a surface of a floc generated by electroflocculation, to form sludge. The sludge containing the PFC can be centrifuged to separate the PFC from the sludge and to form a concentrated PFC solution. Eelectroflocculation provides a simple process that is easy to operate. Reaction conditions are mild. Energy consumption is low. Treatment effect is desirable, stable, and reliable. Industrial application can be easy to implement. Further, the centrifugal separation technology used for the harmless treatment of the generated PFC-containing sludge is novel and does not need to use chemicals. Further, dewatering of the sludge is achieved at the same time during the harmless treatment. The needed equipment is simple and can be automatically operated.

Abstract: The present disclosure describes methods and compositions for reducing and/or preventing soil water repellency. Embodiments of methods of reducing soil water repellency (SWR) of the present disclosure include applying to an area of groundcover a composition including an effective amount of at least one isolated enzyme capable of degrading or altering organic matter associated with SWR, where the SWR of the area of groundcover is reduced after treatment with the enzyme composition.

Abstract: The present invention relates to the field of medicine, and disclosed are an L-setastine hydrochloride and a preparation method therefor. The compound of the present invention has the advantages of stronger histamine Hi receptor antagonism and small side effect; the yield of the preparation method is more than 80%, and the product purity is high. The present invention also provides an application of the compound as an H1 histamine receptor antagonist.

Abstract: Various embodiments provide methods for removing a PFC by concentration and separation. In an exemplary method, a PFC in an aqueous solution or in a mixed water-organic solvent solution can be adsorbed onto a surface of a floc generated by electroflocculation, to form sludge. The sludge containing the PFC can be centrifuged to separate the PFC from the sludge and to form a concentrated PFC solution. Eelectroflocculation provides a simple process that is easy to operate. Reaction conditions are mild. Energy consumption is low. Treatment effect is desirable, stable, and reliable. Industrial application can be easy to implement. Further, the centrifugal separation technology used for the harmless treatment of the generated PFC-containing sludge is novel and does not need to use chemicals. Further, dewatering of the sludge is achieved at the same time during the harmless treatment. The needed equipment is simple and can be automatically operated.

Abstract: A method of preparing (S)-2-amino-5-methoxytetralin hydrochloride[(S)-2-amino-5-methoxyl-1,2,3,4-tetrahydronaphthalene hydrochloride], comprising the steps of: (1) producing a compound (I) by addition-elimination reaction of 5-methoxy-2-tetralone and R-(+)-a-phenylethylamine; (2) producing a compound (II) by reduction reaction of the compound (I) with a reducing agent; and (3) producing a compound (II) hydrochloride by reacting the compound (II) with a salt-forming agent, then carrying out reduction reaction with a palladium-carbon catalyst to produce (S)-2-amino-5-methoxytetralin hydrochloride. The method can significantly increase the yield of (S)-2-amino-5-methoxytetralin hydrochloride with short synthetic path, low preparation cost and less pollution, which is environmentally friendly and is suitable for medical industrialized production. The structural formulae of the compound (I) and the compound (II) are: respectively.

Abstract: The present disclosure describes methods and compositions for reducing and/or preventing soil water repellency. Embodiments of methods of reducing soil water repellency (SWR) of the present disclosure include applying to an area of groundcover a composition including an effective amount of at least one isolated enzyme capable of degrading or altering organic matter associated with SWR, where the SWR of the area of groundcover is reduced after treatment with the enzyme composition.

Abstract: The present disclosure includes methods and compositions for reducing turf thatch and/or preventing turf thatch buildup. The compositions include isolated fungal laccase enzymes, such as laccase enzymes from white rot fungi. Methods of reducing and/or preventing turf thatch buildup include applying compositions including isolated fungal laccase enzymes to turfgrass.

Abstract: The present disclosure describes methods and compositions for reducing turf thatch and/or preventing turf thatch buildup.

Abstract: Embodiments of the present disclosure include methods of treating a biomass, in particular lignocellulosic biomass (e.g., switch grass, sweet sorghum, miscanthus, pine wood, corn stover, and the like), under appropriate conditions to effectively reduce and/or reform the lignin contents in lignocellulosic biomass without significantly reducing its sugar contents.

Abstract: The present invention relates to the field of medicine, and disclosed are an L-setastine hydrochloride and a preparation method therefor. The compound of the present invention has the advantages of stronger histamine Hi receptor antagonism and small side effect; the yield of the preparation method is more than 80%, and the product purity is high. The present invention also provides an application of the compound as an H1 histamine receptor antagonist.

Abstract: A method of preparing (S)-2-amino-5-methoxytetralin hydrochloride[(S)-2-amino-5-methoxyl-1,2,3,4-tetrahydronaphthalene hydrochloride], comprising the steps of: (1) producing a compound (I) by addition-elimination reaction of 5-methoxy-2-tetralone and R-(+)-a-phenylethylamine; (2) producing a compound (II) by reduction reaction of the compound (I) with a reducing agent; and (3) producing a compound (II) hydrochloride by reacting the compound (II) with a salt-forming agent, then carrying out reduction reaction with a palladium-carbon catalyst to produce (S)-2-amino-5-methoxytetralin hydrochloride. The method can significantly increase the yield of (S)-2-amino-5-methoxytetralin hydrochloride with short synthetic path, low preparation cost and less pollution, which is environmentally friendly and is suitable for medical industrialized production. The structural formulae of the compound (I) and the compound (II) are: resepectively.