Abstract: A process for the preparation of canagliflozin. The process may be effectively implemented on an industrial scale. Several compounds useful as intermediates for the synthesis of canagliflozin (Formula 4, Formula 4a, Formula 4b and Formula 5) are also disclosed. The process involves the reduction of the compound of formula 3 in the presence of a metal hydride and an organic solvent to obtain the compound of formula 4, converting this into a compound of formula 5 which in turn is converted into canagliflozin.

Abstract: Photograph organization based on facial recognition is described. In one or more embodiments, a photograph organization module obtains multiple photographs having images of faces and recognizes the faces in the multiple photographs. The module builds a population by attempting to distinguish individual persons among the faces in the multiple photographs, with each person of the population corresponding to a group of multiple groups. After a first pass through the faces, the population includes a number of duplicative persons. With a second pass, the photograph organization module reduces the number of duplicative persons in the population by merging two or more groups of the multiple groups to produce a reduced number of groups. The merging is performed based on comparisons of the faces corresponding to the two or more groups. The multiple photographs are organized based on the reduced number of groups. Organization can include tagging or displaying grouped photographs.

Abstract: A loop-free hybrid network can include receiving an advertisement from a non-software defined network (SDN) network device, determining a network topology that includes the non-SDN network device and a number of SDN network devices, and sending an aggregating instruction to the non-SDN network device, wherein the aggregating instruction aggregates all connections between the non-SDN network device and the number of SDN network devices.

Abstract: Methods and apparatus for precipitating dissolved materials from a solution involve reduction of fines. In an embodiment, the method comprises: introducing a solution into a reactor, causing the dissolved materials in the solution to precipitate into crystals under a first reaction condition, adjusting the reaction condition from the first reaction condition to a second reaction condition, maintaining the reaction condition in the second reaction condition to cause a sub-population of the crystals to dissolve, and adjusting the reaction condition from the second reaction condition to the first reaction condition. In an embodiment, the apparatus comprises a reaction tank, a recycling path and at least an acid injector which is configured for dosing an acid into solution flow in the recycling path.

Abstract: Methods and apparatus for precipitating dissolved materials from a solution involve reduction of fines. In an embodiment, the method comprises: introducing a solution into a reactor, causing the dissolved materials in the solution to precipitate into crystals under a first reaction condition, adjusting the reaction condition from the first reaction condition to a second reaction condition, maintaining the reaction condition in the second reaction condition to cause a sub-population of the crystals to dissolve, and adjusting the reaction condition from the second reaction condition to the first reaction condition. In an embodiment, the apparatus comprises a reaction tank, a recycling path and at least an acid injector which is configured for dosing an acid into solution flow in the recycling path.

Abstract: A system is configured to: receive a message from a gateway device; identify one or more sessions corresponding to an identifier included in the message; and clear the one or more corresponding sessions. The identifier may correspond to a part of the gateway device where a session is stored or maintained for a mobile device to connect to a server device.

Abstract: An electronic document is produced from scanning a physical document that is to be subjected to redaction. The electronic document is sent to at least one device associated with at least one reviewer. Data relating to redaction input by the at least one reviewer is received. One of plural different options for processing the physical document is selected based on which of plural completion statuses has been marked for the electronic document.

Abstract: A method for treating phosphate-containing wastewater, such as phosphogypsum pond water. The method includes the steps of: (a) adding a first cation to the wastewater to precipitate fluorosilicate from the wastewater; (b) adding a second cation to the wastewater to precipitate fluoride from the wastewater; (c) raising the pH of the wastewater to precipitate the second cation from the wastewater; (d) removing residual silica from the wastewater; and (e) precipitating phosphate from the wastewater. The precipitated fluorosilicate may be sodium fluorosilicate. The precipitated phosphate may be struvite.

Abstract: Provided is a method of securing confidential information in a document. A user input is received to identify confidential information in a document. The confidential information is encrypted wherein encryption results in greeking of the confidential information. A password is associated with the encrypted confidential information, wherein the password is required to decrypt and ungreek the confidential information.

Abstract: A method, system and non-transitory computer-readable medium for forwarding data packet traffic in a point multi-point link aggregation using a link selector data table. A data packet is received at a device having a point multi-point link aggregation comprising a plurality of physical links. It is determined whether data extracted from the received data packet can be matched to one of a plurality of records in a link selector data table, where each record comprises data to identify a communication flow and data to identify one of the physical links, each record being generated from a data packet sampled in a transmission coming to the device along ones of the physical links. The received data packet is forwarded on the physical link identified by the one record, where the extracted data is matched to one of the plurality of records.

Abstract: A method for treating, and recovering phosphate compounds from, phosphate-containing wastewater. The method includes the steps of: (a) removing fluoride from the wastewater; (b) recovering a phosphate compound from the wastewater by maintaining super saturation conditions for the phosphate compound; and (c) polishing the wastewater. A silica removal step may be optionally performed after step (a) and before step (b).

Abstract: Methods, computer readable media, and apparatuses for managing initiative consolidation are presented. According to one or more aspects, information about at least two new projects may be received. Subsequently, the information may be analyzed to identify one or more commonalities between the at least two new projects. Thereafter, it may be determined, based on the identified commonalities, to bundle the at least two new projects for one or more testing phases. In one or more arrangements, receiving information about the at least two new projects may include extracting, from one or more project design documents, a job listing for each project, where each job listing identifies one or more jobs included in each project. In some arrangements, a cost-benefit analysis may be generated to calculate potential savings associated with bundling the at least two new projects for the one or more testing phases.

Abstract: The present invention provides novel crystalline forms of Nelfinavir mesylate, Form-A, Form-B, Form-C, Form-D and the process for their preparation without the use of any special equipment such as a spray drier, avoiding the use of highly flammable solvents such as ethers. The crystalline form can be tailored with the selection of the ante solvent and appropriate conditions for the process.

Abstract: Present invention relates to an improved process for the preparation of Zopiclone and its enantiomerically enriched isomer (Eszopiclone). 6-(5-Chloropyridin-2-yl)-5-hydroxy-7-oxo-5,6-dihydropyrrolo[3,4-b]pyrazine is reacted with 1-chloro-carbonyl-4-methylpiperazine in the presence of alkali earth metal carbonates, hydroxides or oxides in a solvent medium to give Zopiclone. It is reacted with optically active acid in a mixture of water and water miscible organic solvent followed by work up to give Eszopiclone. The present invention also relates to process for the conversion of (R) or (S) Zopiclone to 6-(5-chloropyrid-2-yl)-5-hydroxy-7-oxo-5,6-dihydro-pyrrolo-[3,4-b]-pyrazine of the intermediate which can be converted to racemic Zopiclone.

Abstract: A control arrangement for a vehicle includes an infotainment console having a user interface with a plurality of pushbuttons. A communication device is communicatively coupled to the infotainment console and relays signals between the infotainment console and a portable computing device. The infotainment console reconfigures the user interface to enable the user to control the portable computing device via the user interface. Each of the pushbuttons is actuatable to cause operation of the portable computing device to proceed to a respective application within the portable computing device.

Abstract: Formation of scale in a wastewater treatment system upstream of a struvite precipitation reactor is inhibited by injection of one or more of CO2 and H3PO4. The injection may be performed at multiple locations. Injection may be controlled based on one or more of pH, fluid flow and fluid pressure. Scale may be inhibited while maintaining production of precipitated struvite.

Abstract: A solid substrate coating capable of swelling by a factor of at least 2 on contact with an aqueous solution. The solid substrate coating may be prepared by activating the surface of a solid substrate by treatment with a plasma, depositing a first layer of siloxane onto the surface of the solid substrate using plasma, and depositing a second layer of at least on chemical functionality on top of the first layer using plasma.

Abstract: The formation of a barrier layer within individual channels or cavities of a microfluidic device is described. The barrier layer is effected through a gas phase deposition process, desirably implemented in a plasma environment using a gas plasma reactor. Judicious selection of a precursor compound used within the gas plasma reactor can provide for generation of a layer on the individual surfaces. Desirably the surface or barrier layer is generated through the chemical adsorption of a metalloid oxide such as a silicon oxide layer on the surface of the individual channels or cavities.

Abstract: A system is configured to: receive a message from a gateway device; identify one or more sessions corresponding to an identifier included in the message; and clear the one or more corresponding sessions. The identifier may correspond to a part of the gateway device where a session is stored or maintained for a mobile device to connect to a server device.

Abstract: Present invention relates to an improved process for the preparation of Zopiclone and its enantiomerically enriched isomer (Eszopiclone). 6-(5-Chloropyridin-2-yl)-5-hydroxy-7-oxo-5,6-dihydropyrrolo[3,4-b]pyrazine is reacted with 1-chloro-carbonyl-4-methylpiperazine in the presence of alkali earth metal carbonates, hydroxides or oxides in a solvent medium to give Zopiclone. It is reacted with optically active acid in a mixture of water and water miscible organic solvent followed by work up to give Eszopiclone. The present invention also relates to process for the conversion of (R) or (S) Zopiclone to 6-(5-chloropyrid-2-yl)-5-hydroxy-7-oxo-5,6-dihydro-pyrrolo-[3,4-b]-pyrazine of the intermediate which can be converted to racemic Zopiclone.