Abstract: Disclosed is an apparatus for measuring the moisture content of a sample. The apparatus includes a first sealed chamber for accepting the sample and a first impulse furnace within the first chamber for dissociating water in the sample into the hydrogen and oxygen, a second sealed chamber in gaseous communication with the first chamber, a second impulse furnace within the second chamber for dissociating water and the hydrogen and the oxygen, and a hydrogen analyzer for determining the amount of hydrogen formed by the first and second impulse furnace. Also disclosed is a method of measuring the amount of water in the sample. The sample is heated in an enclosed chamber in the presence of a water dissociation catalyst, whereby water in the first chamber is dissociated into hydrogen and oxygen. Vapors are passed from the enclosed chamber to a second enclosed chamber which contains a water dissociation catalyst, whereby water in the vapors is dissociated into hydrogen and oxygen.

Abstract: Nuclear fuel rods are processed to remove moisture in an oven which is evacuated. Measurement of the moisture content in each of a plurality of nuclear fuel rods (typically 44) is carried out by condensing the vapor derived from one randomly-selected control rod in a nitrogen-liquid cooled trap, collecting the condensed vapor in magnesium perchlorate, and determining the weight of the collected moisture. Moisture from the one fuel rod is condensed, collected and has its weight determined repeatedly in increments until the difference between the weight of a last increment and of a just preceding increment is less than 1 mg. (The permissible content is 6 mg. or less.) The rods have small perforations through which the vapor can escape. The evacuating system includes a main evacuating channel connected directly to the oven and a branch channel connected to the one fuel rod through the cold trap.