Abstract: A method for determining the source of a surface bitumen sheen in an end pit lake formed by water capping of oil sand tailings is provided comprising quantifying bitumen flux using ice core samples of the end pit lake. The high areas of bitumen flux indicate the areas of the end pit lake that should be dredged for reclamation of the end pit lake to prevent the formation of hydrocarbon sheen on the surface of the end pit lake. A method for evaluating reclamation of an end pit lake is also provided.

Abstract: A method of quantifying at least one property of interest of an oil sands ore sample is provided using a laser-induced breakdown spectroscopy (LIBS) method. The property of interest may include bitumen content, water content, particle size information, cation exchange capacity, methylene blue index, mineralogical content (e.g., quartz, total clay, and clay components), amorphous material content, total ash content, and connate water parameter (e.g., conductivity, chloride content, or alkalinity).

Abstract: A method of quantifying at least one property of interest of an oil sands ore sample is provided using a laser-induced breakdown spectroscopy (LIBS) method. The property of interest may include bitumen content, water content, particle size information, cation exchange capacity, methylene blue index, mineralogical content (e.g., quartz, total clay, and clay components), amorphous material content, total ash content, and connate water parameter (e.g., conductivity, chloride content, or alkalinity).

Abstract: A method for determining the solids content, fines content and/or particle size distribution of the solids in an oil sands process stream test sample comprising bitumen, solids and water using low-field time-domain NMR is provided which involves building a non-solids partial least squares calibration model using oil sands process streams calibration samples having a known bitumen content, solids content, water content, fines content and/or particle size distribution by subjecting the calibration samples to a first T1-weighted T2 measurement NMR pulse sequence that maximizes very fast relaxing signals and a second T1-weighted T2 measurement NMR pulse sequence that maximizes slow relaxing signals. The measurement of other sample properties strongly correlated with surface area, such as methylene blue index, can also be measured using a partial least squares calibration model.

Abstract: A method for predicting a solids content, boiling point information, and micro carbon residue content of an extra heavy oil test sample involves subjecting extra heavy oil calibration samples to T1-weighted T2 low-field NMR pulse sequences, and recording T1 and T2 relaxation information to generate a NMR calibration data set. A chemometric partial least squares calibration model is determined to relate the NMR calibration data set to reference values of properties of the calibration samples. Similarly, the extra heavy oil test sample is subjected to the NMR T1-weighted T2 low-field NMR pulse sequences, the resulting relaxation information is recorded to generate NMR test data. The properties of the test sample are predicted based on the PLS calibration model and the NMR test data. The test sample may be derived from a process stream for upgrading bitumen, and may contain significant amounts of solids and high boiling point hydrocarbons (e.g., >524° C.).

Abstract: A method for determining the solids content, fines content and/or particle size distribution of the solids in an oil sands process stream test sample comprising bitumen, solids and water using low-field time-domain NMR is provided which involves building a non-solids partial least squares calibration model using oil sands process streams calibration samples having a known bitumen content, solids content, water content, fines content and/or particle size distribution by subjecting the calibration samples to a first T1-weighted T2 measurement NMR pulse sequence that maximizes very fast relaxing signals and a second T1-weighted T2 measurement NMR pulse sequence that maximizes slow relaxing signals. The measurement of other sample properties strongly correlated with surface area, such as methylene blue index, can also be measured using a partial least squares calibration model.

Abstract: A method of quantifying at least one property of interest of an oil sands ore sample is provided using a laser-induced breakdown spectroscopy (LIBS) method. The LIBS method may be applied to oil sands ore being conveyed prior to a slurry process to measure oil sand composition and provide information which may predict extraction characteristics. The LIBS method may be applied to oil sands core samples in a laboratory setting to reduce the cost and analysis time associated with conventional laboratory measurement techniques.