Abstract: An improved method for producing .sup.99m Tc compositions. .sup.100 Mo metal is irradiated with photons in a particle (electron) accelerator to produce .sup.99 Mo metal which is dissolved in a solvent. A solvated .sup.99 Mo product is then dried to generate a supply of .sup.99 MoO.sub.3 crystals. The crystals are thereafter heated at a temperature which will sublimate the crystals and form a gaseous mixture containing vaporized .sup.99m TcO.sub.3 and vaporized .sup.99m TcO.sub.2 but will not cause the production of vaporized .sup.99 MoO.sub.3. The mixture is then combined with an oxidizing gas to generate a gaseous stream containing vaporized .sup.99m Tc.sub.2 O.sub.7. Next, the gaseous stream is cooled to a temperature sufficient to convert the vaporized .sup.99m Tc.sub.2 O.sub.7 into a condensed .sup.99m Tc-containing product. The product has high purity levels resulting from the use of reduced temperature conditions and ultrafine crystalline .sup.99 MoO.sub.3 starting materials with segregated .sup.

Abstract: A boltless, reusable flange system for joining metal piping includes a circular, wedge-shaped tongue on an upper flange for mating with a groove containing a fusible alloy in a lower flange. The lower flange includes a heating element for melting the fusible alloy, and a thermocouple device to sense the alloy temperature. Heat can be controlled and supplied from a remote source and monitored by a remote temperature indicator. The upper flange is positioned above the lower flange, tongue and groove aligned, and the lower flange is heated until the fusible alloy melts to allow the upper tongue to settle down within the lower groove. Upon removal of the heat, the alloy hardens to further bring the two flanges together in a solid and sealed couple, compressing an optional gasket.