Abstract: System and methods are described for dynamically controlling operation of a rheometer. A program is created on a programming interface for executing a test upon a sample in a rheometer by receiving user selections of a plurality of nodes and connections of each node to another node according to directional connection indicators. Nodes indicate steps for performing a test upon a sample or configuring a rheometer for performing a test upon a sample. Scripts are created for generating a sequence of instructions to the rheometer. The scripts include instructions for performing steps indicated by each of the selected nodes and in accordance with the directional connection indicators. Low-level instructions are downloaded from the scripts for execution in the rheometer, and drivers in the rheometer are instructed for performing the downloaded instructions.

Abstract: A rheometer includes a holder assembly for coupling a test specimen to a motor assembly to effect rotational strain in the test specimen while enabling the determination of axial displacement effected by the test specimen normal to the direction of the rotational strain, the holder assembly having a first member coupled to the test specimen, a second member coupled to the motor assembly, and a suspension arrangement coupling the first member with the second member for simultaneous maximum resistance to relative rotational displacement between the first and second members and minimum resistance to relative axial displacement between the first and second members.

Abstract: A rheometer includes a holder assembly for coupling a test specimen to a motor assembly to effect rotational strain in the test specimen while enabling the determination of axial displacement effected by the test specimen normal to the direction of the rotational strain, the holder assembly having a first member coupled to the test specimen, a second member coupled to the motor assembly, and a suspension arrangement coupling the first member with the second member for simultaneous maximum resistance to relative rotational displacement between the first and second members and minimum resistance to relative axial displacement between the first and second members.

Abstract: System and methods are described for dynamically controlling operation of a rheometer. A program is created on a programming interface for executing a test upon a sample in a rheometer by receiving user selections of a plurality of nodes and connections of each node to another node according to directional connection indicators. Nodes indicate steps for performing a test upon a sample or configuring a rheometer for performing a test upon a sample. Scripts are created for generating a sequence of instructions to the rheometer. The scripts include instructions for performing steps indicated by each of the selected nodes and in accordance with the directional connection indicators. Low-level instructions are downloaded from the scripts for execution in the rheometer, and drivers in the rheometer are instructed for performing the downloaded instructions.

Abstract: On-line rheological measurements are made on a process flowing material, such as a polymer melt, utilizing a rheometer of the type in which an inlet pump delivers a relatively large volumetric flow of diverted process material from a process main stream to an inlet site located in very close proximity to the entrance of a capillary passage, and a metering pump draws a smaller portion of the volumetric flow of the diverted material from the inlet site through the capillary passage for return to the process main stream. The viscosity of the diverted material is measured as a function of the rate of flow of the material through the capillary passage and the pressure drop between spaced apart locations along the capillary passage.

Abstract: Apparatus and method for the simultaneous measurement of rheological and thermal characteristics of a test specimen subjects the test specimen to stress for rheological measurements, while at the same time subjecting the same test specimen to controlled temperature changes for the measurement of temperature differentials indicative of thermal characteristics of the test specimen while the test specimen is being stressed for the rheological measurements, and a measuring cell for measuring the thermal characteristics of a specimen.

Abstract: A magnetic resonance analyzing apparatus includes a sampling region; a first temperature stabilization assembly for maintaining the sampling region at a predetermined temperature; a magnet for applying a base magnetic field to the sampling region; a coil for applying a first 0.degree. phase excitation pulse to the sampling region at a first time, and a second 90.degree.

Abstract: Apparatus and method for measuring the shear viscosity of a fluid urges sample fluid through a gap between a sleeve having an axial passage and a pin extending axially into the passage in the sleeve to subject the sample fluid to shear while measuring the axial force tending to move the pin and the sleeve axially away from one another, the axial force being indicative of the shear viscosity of the sample fluid.

Abstract: On-line rheological measurements are made utilizing a rheometer of the type in which a first metering pump delivers diverted melt from a process main stream to a capillary passage and a second metering pump returns the diverted melt from the capillary passage to the process main stream and the viscosity of the diverted melt is measured by controlling the rate of flow of the melt to maintain constant the pressure drop between spaced apart locations along the capillary passage and measuring the temperature of the melt in the capillary passage. The measurements may be made while controlling the speed of the second metering pump independent of the speed of the first metering pump to maintain the pressure at the exit of the capillary passage essentially constant.

Abstract: Impact testing apparatus in which a weighted dart is dropped from a prescribed height to penetrate a test specimen when traveling at a desired velocity and level of kinetic energy, the acceleration of the dart being assisted by a spring force in the direction of travel so that the prescribed height is maintained at a minimum for a given desired velocity and the dart being guided to the test specimen by a generally tubular guide within which the dart is loosely fitted. A force transducer is located at the tip of the dart for providing impact force information as the tip penetrates the test specimen.

Abstract: Apparatus and method for measuring the viscous component and the elastic component of forces within a viscoelastic test specimen placed in shear, the test specimen being coupled to a platen having a rest position, the platen being displaceable from the rest position rotationally and axially relative to a fixed axis in response to rotational and axial forces exerted by the test specimen upon the platen as a result of the viscous component and the elastic component, the apparatus and method including an arrangement of component parts and a plurality of steps for establishing a rotational counterforce for balancing the rotational force on the platen and simultaneously establishing an axial counterforce for balancing the axial force on the platen to maintain the platen at the rest position, and indicating the magnitude of the counterforces necessary to maintain the platen at the rest position, whereby the viscous component and the elastic component of forces are measured at zero compliance.

Abstract: A rotational rheometer utilizes a rotor coupled to a test specimen and suspended in a stator by a low friction bearing suspension system, a compensation arrangement which compensates for bearing torque on the rotor throughout the full range of rotation of the rotor, and position transducers arranged for determining accurately both the angular position of the rotor throughout a full range of 360.degree. of rotation, and the longitudinal position of the rotor, relative to the stator.

Abstract: Disclosed herein is a torsion tube apparatus for making on-line measurements of the viscosity and elasticity of a fluid. The apparatus includes a housing member, an outer cylinder having one end rotatably mounted with respect to the housing member, and a motor for rotating this outer cylinder. An elongated torsion tube is mounted concentrically within and spaced from the outer cylinder and has one end fixed to the housing member, with its other end freely disposed within the cylinder for torsional movement with respect to the fixed end. Therefore, an annular void is defined between the tube and cylinder. Fluid may be introduced through a conduit into the interior of the cylinder for flow therethrough and discharge therefrom, such that rotating motion of the fluid caused by rotation of the cylinder exerts a torsional force directly on the outer surface of the tube. A torsion indicating shaft extends concentrically through the tube, having its one end fixed to the free end of the tube.