Abstract: A process for separately recovering platinum group metal values, nickel values and copper from nickel-copper-iron sulphidic matte containing platinum group metals includes leaching ground matte at atmospheric pressure in acidic nickel-copper sulphate solution at a temperature in the range of from about 75.degree. to about 105.degree. C. and at a pH below about 4 initially under oxidizing conditions and subsequently under neutral or non-oxidizing conditions to cause dissolution of nickel and iron, precipitation of copper as a copper sulphide and precipitation of dissolved platinum group metals. The copper, nickel and platinum group metal containing solids are separated from the nickel and iron containing sulphate solution and are leached in acidic nickel-copper sulphate solution under pressurized oxidizing conditions at a temperature of from about 120.degree. to about 180.degree. C. to cause dissolution of nickel and copper with minor dissolution of platinum group metals.

Abstract: A process for separately recovering nickel and cobalt from solution includes adjusting the pH of the solution to a value between about 3 and about 6, and then contacting the solution with a chelating ion exchange resin having aminocarboxylic acid functional groups to selectively load nickel onto the resin to produce a nickel loaded resin and a nickel depleted cobalt containing solution. The process is also applicable to the separate recovery of copper and zinc from solution.