Patents by Inventor Samuel Mark DeBusk
Samuel Mark DeBusk has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Publication number: 20220409549Abstract: The disclosure provides products configured for oral use, and methods of making the products. The products include a plurality of granules, the granules including at least one filler; at least one sugar alcohol; a cellulose ether, polyvinylpyrrolidone, or a combination thereof; and at least one active ingredient, at least one flavorant, or a combination thereof. The products may be in a granular form, or in the form of a tablet or pellet.Type: ApplicationFiled: June 21, 2022Publication date: December 29, 2022Inventors: Ronald K. HUTCHENS, Darrell Eugene HOLTON, JR., John Paul MUA, Luis MONSALUD, Frank Kelley ST. CHARLES, Steven Lee ALDERMAN, Jerry Wayne MARSHALL, Matthew LAMPE, Samuel Mark DEBUSK
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Publication number: 20220287356Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: ApplicationFiled: June 2, 2022Publication date: September 15, 2022Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Patent number: 11375741Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: GrantFiled: May 24, 2018Date of Patent: July 5, 2022Assignee: R.J. Reynolds Tobacco CompanyInventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Patent number: 11166485Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: GrantFiled: March 14, 2016Date of Patent: November 9, 2021Assignee: R.J. Reynolds Tobacco CompanyInventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Patent number: 10774472Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.Type: GrantFiled: January 18, 2019Date of Patent: September 15, 2020Assignee: R.J. Reynolds Tobacco CompanyInventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
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Patent number: 10334874Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.Type: GrantFiled: April 15, 2016Date of Patent: July 2, 2019Assignees: R. J. Reynolds Tobacco Company, North Carolina State UniversityInventors: Medwick Vaughan Byrd, Jr., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
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Publication number: 20190153673Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.Type: ApplicationFiled: January 18, 2019Publication date: May 23, 2019Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
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Patent number: 10196778Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.Type: GrantFiled: March 20, 2017Date of Patent: February 5, 2019Assignee: R.J. Reynolds Tobacco CompanyInventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
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Publication number: 20180266053Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.Type: ApplicationFiled: March 20, 2017Publication date: September 20, 2018Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
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Publication number: 20180263276Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: ApplicationFiled: May 24, 2018Publication date: September 20, 2018Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Patent number: 9950858Abstract: A paper material is provided herein, wherein the paper material includes a fibrous material including at least 5 dry weight percent of fibers derived from a plant of the Nicotiana species; wherein the paper material has a basis weight ranging from about 5 g/m2 to about 450 g/m2; and wherein the paper material has a caliper ranging from about 0.01 mils to about 200 mils. The paper material can be suitable for use in a smoking article in the form of at least one of a tipping material, a plug wrap and a wrapping material. The paper material can be suitable for use in at least one of a soft carton container suitable to house smoking articles, a label, a paper substrate of a barrier layer, a hard carton suitable to house smoking articles and a container suitable to house smokeless tobacco products.Type: GrantFiled: January 16, 2015Date of Patent: April 24, 2018Assignees: R.J. Reynolds Tobacco Company, North Carolina State UniversityInventors: Medwick Vaughan Byrd, Jr., David Neil McClanahan, Samuel Mark Debusk
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Patent number: 9661876Abstract: The present disclosure describes methods of obtaining and/or deriving a sugar-enriched extract from plants of the Nicotiana species and methods for incorporation of such extracts into various tobacco compositions. One exemplary method for preparing a sugar-enriched extract comprises contacting Nicotiana plant material with a solvent and extracting sugars into the solvent to form a liquid sugar-containing extract; separating a solid extracted plant material from the liquid sugar-containing extract; clarifying the liquid sugar-containing extract to form a clarified sugar-containing extract and a solids fraction; and isolating the liquid sugar-containing extract to provide a sugar-enriched extract comprising a combined weight of fructose and glucose of at least about 10% by dry weight. In certain embodiments, the sugars of the extract comprise at least about 50% by weight fructose.Type: GrantFiled: March 14, 2013Date of Patent: May 30, 2017Assignee: R.J. Reynolds Tobacco CompanyInventors: John-Paul Mua, Barry Bratcher, Kyle Ford, Leigh Hagan, Leigh Ann Blevins Joyce, Joshua D. Morton, Samuel Mark Debusk, Margarette Elisa Lovette
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Publication number: 20160227834Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.Type: ApplicationFiled: April 15, 2016Publication date: August 11, 2016Inventors: Medwick Vaughan Byrd, JR., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
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Publication number: 20160208440Abstract: A paper material is provided herein, wherein the paper material includes a fibrous material including at least 5 dry weight percent of fibers derived from a plant of the Nicotiana species; wherein the paper material has a basis weight ranging from about 5 g/m2 to about 450 g/m2; and wherein the paper material has a caliper ranging from about 0.01 mils to about 200 mils. The paper material can be suitable for use in a smoking article in the form of at least one of a tipping material, a plug wrap and a wrapping material. The paper material can be suitable for use in at least one of a soft carton container suitable to house smoking articles, a label, a paper substrate of a barrier layer, a hard carton suitable to house smoking articles and a container suitable to house smokeless tobacco products.Type: ApplicationFiled: January 16, 2015Publication date: July 21, 2016Inventors: Medwick Vaughan Byrd, JR., David Neil McClanahan, Samuel Mark Debusk
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Publication number: 20160192697Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: ApplicationFiled: March 14, 2016Publication date: July 7, 2016Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Patent number: 9339058Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.Type: GrantFiled: April 19, 2012Date of Patent: May 17, 2016Assignee: R. J. Reynolds Tobacco CompanyInventors: Medwick Vaughan Byrd, Jr., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
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Patent number: 9301544Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: GrantFiled: March 14, 2013Date of Patent: April 5, 2016Assignee: R.J. Reynolds Tobacco CompanyInventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Publication number: 20140271952Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.Type: ApplicationFiled: March 14, 2013Publication date: September 18, 2014Applicant: R.J. REYNOLDS TOBACCO COMPANYInventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
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Publication number: 20140271951Abstract: The present disclosure describes methods of obtaining and/or deriving a sugar-enriched extract from plants of the Nicotiana species and methods for incorporation of such extracts into various tobacco compositions. One exemplary method for preparing a sugar-enriched extract comprises contacting Nicotiana plant material with a solvent and extracting sugars into the solvent to form a liquid sugar-containing extract; separating a solid extracted plant material from the liquid sugar-containing extract; clarifying the liquid sugar-containing extract to form a clarified sugar-containing extract and a solids fraction; and isolating the liquid sugar-containing extract to provide a sugar-enriched extract comprising a combined weight of fructose and glucose of at least about 10% by dry weight. In certain embodiments, the sugars of the extract comprise at least about 50% by weight fructose.Type: ApplicationFiled: March 14, 2013Publication date: September 18, 2014Applicant: R.J. REYNOLDS TOBACCO COMPANYInventors: John-Paul Mua, Barry Bratcher, Kyle Ford, Leigh Hagan, Leigh Ann Blevins Joyce, Joshua D. Morton, Samuel Mark Debusk, Margarette Elisa Lovette
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Publication number: 20130276801Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.Type: ApplicationFiled: April 19, 2012Publication date: October 24, 2013Inventors: Medwick Vaughan Byrd, JR., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, Daivd Neil McClanahan