Patents by Inventor Samuel Mark DeBusk

Samuel Mark DeBusk has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20220409549
    Abstract: The disclosure provides products configured for oral use, and methods of making the products. The products include a plurality of granules, the granules including at least one filler; at least one sugar alcohol; a cellulose ether, polyvinylpyrrolidone, or a combination thereof; and at least one active ingredient, at least one flavorant, or a combination thereof. The products may be in a granular form, or in the form of a tablet or pellet.
    Type: Application
    Filed: June 21, 2022
    Publication date: December 29, 2022
    Inventors: Ronald K. HUTCHENS, Darrell Eugene HOLTON, JR., John Paul MUA, Luis MONSALUD, Frank Kelley ST. CHARLES, Steven Lee ALDERMAN, Jerry Wayne MARSHALL, Matthew LAMPE, Samuel Mark DEBUSK
  • Publication number: 20220287356
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Application
    Filed: June 2, 2022
    Publication date: September 15, 2022
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Patent number: 11375741
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Grant
    Filed: May 24, 2018
    Date of Patent: July 5, 2022
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Patent number: 11166485
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Grant
    Filed: March 14, 2016
    Date of Patent: November 9, 2021
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Patent number: 10774472
    Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.
    Type: Grant
    Filed: January 18, 2019
    Date of Patent: September 15, 2020
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
  • Patent number: 10334874
    Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.
    Type: Grant
    Filed: April 15, 2016
    Date of Patent: July 2, 2019
    Assignees: R. J. Reynolds Tobacco Company, North Carolina State University
    Inventors: Medwick Vaughan Byrd, Jr., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
  • Publication number: 20190153673
    Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.
    Type: Application
    Filed: January 18, 2019
    Publication date: May 23, 2019
    Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
  • Patent number: 10196778
    Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.
    Type: Grant
    Filed: March 20, 2017
    Date of Patent: February 5, 2019
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
  • Publication number: 20180263276
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Application
    Filed: May 24, 2018
    Publication date: September 20, 2018
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Publication number: 20180266053
    Abstract: The present disclosure relates to cellulose nanomaterials made or derived from tobacco and methods for the production thereof. The tobacco-derived cellulose nanomaterials can be employed in various industrial applications such as film forming applications and solution thickening technologies. In particular, the disclosure is directed to methods for preparing tobacco-derived cellulose nanomaterials using less fibrillation cycles than in the production of wood pulp. The invention includes a method for preparing tobacco derived nanocellulose material comprising receiving a tobacco pulp in a dilute form such that the tobacco pulp is a tobacco pulp suspension with a consistency of less than about 5%; and mechanically fibrillating the tobacco pulp suspension to generate a tobacco derived nanocellulose material having at least one average particle size dimension in the range of about 1 nm to about 100 nm.
    Type: Application
    Filed: March 20, 2017
    Publication date: September 20, 2018
    Inventors: Andries Don Sebastian, Samuel Mark DeBusk, David Neil McClanahan, Panu Lahtinen, Marjo Maeaettaenen, Airi Saerkilahti
  • Patent number: 9950858
    Abstract: A paper material is provided herein, wherein the paper material includes a fibrous material including at least 5 dry weight percent of fibers derived from a plant of the Nicotiana species; wherein the paper material has a basis weight ranging from about 5 g/m2 to about 450 g/m2; and wherein the paper material has a caliper ranging from about 0.01 mils to about 200 mils. The paper material can be suitable for use in a smoking article in the form of at least one of a tipping material, a plug wrap and a wrapping material. The paper material can be suitable for use in at least one of a soft carton container suitable to house smoking articles, a label, a paper substrate of a barrier layer, a hard carton suitable to house smoking articles and a container suitable to house smokeless tobacco products.
    Type: Grant
    Filed: January 16, 2015
    Date of Patent: April 24, 2018
    Assignees: R.J. Reynolds Tobacco Company, North Carolina State University
    Inventors: Medwick Vaughan Byrd, Jr., David Neil McClanahan, Samuel Mark Debusk
  • Patent number: 9661876
    Abstract: The present disclosure describes methods of obtaining and/or deriving a sugar-enriched extract from plants of the Nicotiana species and methods for incorporation of such extracts into various tobacco compositions. One exemplary method for preparing a sugar-enriched extract comprises contacting Nicotiana plant material with a solvent and extracting sugars into the solvent to form a liquid sugar-containing extract; separating a solid extracted plant material from the liquid sugar-containing extract; clarifying the liquid sugar-containing extract to form a clarified sugar-containing extract and a solids fraction; and isolating the liquid sugar-containing extract to provide a sugar-enriched extract comprising a combined weight of fructose and glucose of at least about 10% by dry weight. In certain embodiments, the sugars of the extract comprise at least about 50% by weight fructose.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: May 30, 2017
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: John-Paul Mua, Barry Bratcher, Kyle Ford, Leigh Hagan, Leigh Ann Blevins Joyce, Joshua D. Morton, Samuel Mark Debusk, Margarette Elisa Lovette
  • Publication number: 20160227834
    Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.
    Type: Application
    Filed: April 15, 2016
    Publication date: August 11, 2016
    Inventors: Medwick Vaughan Byrd, JR., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
  • Publication number: 20160208440
    Abstract: A paper material is provided herein, wherein the paper material includes a fibrous material including at least 5 dry weight percent of fibers derived from a plant of the Nicotiana species; wherein the paper material has a basis weight ranging from about 5 g/m2 to about 450 g/m2; and wherein the paper material has a caliper ranging from about 0.01 mils to about 200 mils. The paper material can be suitable for use in a smoking article in the form of at least one of a tipping material, a plug wrap and a wrapping material. The paper material can be suitable for use in at least one of a soft carton container suitable to house smoking articles, a label, a paper substrate of a barrier layer, a hard carton suitable to house smoking articles and a container suitable to house smokeless tobacco products.
    Type: Application
    Filed: January 16, 2015
    Publication date: July 21, 2016
    Inventors: Medwick Vaughan Byrd, JR., David Neil McClanahan, Samuel Mark Debusk
  • Publication number: 20160192697
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Application
    Filed: March 14, 2016
    Publication date: July 7, 2016
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Patent number: 9339058
    Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.
    Type: Grant
    Filed: April 19, 2012
    Date of Patent: May 17, 2016
    Assignee: R. J. Reynolds Tobacco Company
    Inventors: Medwick Vaughan Byrd, Jr., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, David Neil McClanahan
  • Patent number: 9301544
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: April 5, 2016
    Assignee: R.J. Reynolds Tobacco Company
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Publication number: 20140271952
    Abstract: The present disclosure describes methods of obtaining and/or deriving proteins from plants of the Nicotiana species and methods for incorporation of such proteins into various products. For example, a method for obtaining a protein-enriched material from a plant of the Nicotiana species or portion thereof is provided, comprising: extracting one or more proteins from the plant material into a solvent to form a liquid protein-containing extract; separating a solid extracted plant material from the liquid protein-containing extract; clarifying the liquid protein-containing extract to form a clarified protein-containing extract and a solids fraction; and treating the clarified protein-containing extract so as to provide a protein-enriched material comprising at least about 60% protein by weight.
    Type: Application
    Filed: March 14, 2013
    Publication date: September 18, 2014
    Applicant: R.J. REYNOLDS TOBACCO COMPANY
    Inventors: John-Paul Mua, Kyle Ford, Leigh Ann Blevins Joyce, Margarette Elisa Lovette, Joshua D. Morton, Leigh Hagan, Barry Bratcher, Samuel Mark Debusk
  • Publication number: 20140271951
    Abstract: The present disclosure describes methods of obtaining and/or deriving a sugar-enriched extract from plants of the Nicotiana species and methods for incorporation of such extracts into various tobacco compositions. One exemplary method for preparing a sugar-enriched extract comprises contacting Nicotiana plant material with a solvent and extracting sugars into the solvent to form a liquid sugar-containing extract; separating a solid extracted plant material from the liquid sugar-containing extract; clarifying the liquid sugar-containing extract to form a clarified sugar-containing extract and a solids fraction; and isolating the liquid sugar-containing extract to provide a sugar-enriched extract comprising a combined weight of fructose and glucose of at least about 10% by dry weight. In certain embodiments, the sugars of the extract comprise at least about 50% by weight fructose.
    Type: Application
    Filed: March 14, 2013
    Publication date: September 18, 2014
    Applicant: R.J. REYNOLDS TOBACCO COMPANY
    Inventors: John-Paul Mua, Barry Bratcher, Kyle Ford, Leigh Hagan, Leigh Ann Blevins Joyce, Joshua D. Morton, Samuel Mark Debusk, Margarette Elisa Lovette
  • Publication number: 20130276801
    Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.
    Type: Application
    Filed: April 19, 2012
    Publication date: October 24, 2013
    Inventors: Medwick Vaughan Byrd, JR., Paul Stuart Chapman, Samuel Mark Debusk, Grady Lance Dooly, Anthony Richard Gerardi, Daivd Neil McClanahan