Patents by Inventor Shaikh Asrof Ali

Shaikh Asrof Ali has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 9790296
    Abstract: Cross-linked tetrapolymers made up of different diallyl zwitterionic diallyl quaternary ammonium salt monomers, with one of them functioning as a cross-linking monomer. The cross-linked terpolymers include a repeating unit with multiple ligand centers that different metal ions can bind to. The cross-linked tetrapolymers are cationic, zwitterionic and anionic, and can be in either an acidic form or a basic form. A method of removing metal ions from an aqueous solution with these cross-linked tetrapolymers is also described.
    Type: Grant
    Filed: March 11, 2015
    Date of Patent: October 17, 2017
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Shamsuddeen Abdullahi Haladu, Shaikh Asrof Ali, Tawfik Abdo Saleh
  • Patent number: 9782768
    Abstract: Cross-linked cyclocopolymers made up of one or more quaternary ammonium salts and sulfur dioxide as monomers. One of the quaternary ammonium salts is also an aspartic acid derivative. The cross-linked copolymers include a repeating unit with multiple chelating centers that different metal ions can bind to. The cross-linked copolymers are zwitterionic or anionic, and can be in either an acidic form or a basic form. A method for removing metal ions from an aqueous sample with these cross-linked copolymers is also described.
    Type: Grant
    Filed: September 30, 2016
    Date of Patent: October 10, 2017
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Zakariyah Abdulkareem Jamiu, Tawfik Abdo Saleh, Shaikh Asrof Ali
  • Patent number: 9771657
    Abstract: Compounds and methods of inhibiting corrosion of mild steel. Compounds disclosed herein are cationic and contain multiple functional motifs such as propargyl, cinnamaldehyde, isoxazolidine and hydrophobe. These compounds are found to be effective in inhibiting mild steel corrosion in HCl, H2SO4, NaCl and CO2-saturated environments.
    Type: Grant
    Filed: April 14, 2017
    Date of Patent: September 26, 2017
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Shaikh Asrof Ali, Mohammad Abu Jafar Mazumder, Hasan Ali Al-Muallem
  • Patent number: 9758878
    Abstract: Compounds and methods of inhibiting corrosion of mild steel. Compounds disclosed herein are cationic and contain multiple functional motifs such as propargyl, cinnamaldehyde, isoxazolidine and hydrophobe. These compounds are found to be effective in inhibiting mild steel corrosion in HCl, H2SO4, NaCl and CO2-saturated environments.
    Type: Grant
    Filed: October 28, 2014
    Date of Patent: September 12, 2017
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Shaikh Asrof Ali, Mohammad Abu Jafar Mazumder, Hasan Ali Al-Muallem
  • Publication number: 20170218523
    Abstract: Compounds and methods of inhibiting corrosion of mild steel. Compounds disclosed herein are cationic and contain multiple functional motifs such as propargyl, cinnamaldehyde, isoxazolidine and hydrophobe. These compounds are found to be effective in inhibiting mild steel corrosion in HCl, H2SO4, NaCl and CO2-saturated environments.
    Type: Application
    Filed: April 14, 2017
    Publication date: August 3, 2017
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Shaikh Asrof ALI, Mohammad Abu Jafar Mazumder, Hasan Ali Al-Muallem
  • Publication number: 20170197847
    Abstract: Cross-linked cyclopolymeric resins from N,N-diallyl quaternary ammonium monomers and tetrallylpiperazinium cross-linking monomer or salts, solvates, tautomers or stereoisomers as adsorbent materials for the removal of heavy metals from aqueous solution. A process for producing the cross-linked cyclopolymeric resins by Butler cyclocopolymerization of the monomers with a free radical initiator. The cross linked cyclopolymeric resins are polyzwitterionic or polyzwitterionic and dianionic and feature repeating units with multiple chelating centers that heavy metal ions can bind to. In addition, a method for removing heavy metals from aqueous solution via contacting and treatment with the cross-linked cyclopolymeric resins.
    Type: Application
    Filed: January 12, 2016
    Publication date: July 13, 2017
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh, Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu
  • Publication number: 20170113215
    Abstract: Cross-linked cyclocopolymers made up of one or more quaternary ammonium salts and sulfur dioxide as monomers. One of the quaternary ammonium salts is also an aspartic acid derivative. The cross-linked copolymers include a repeating unit with multiple chelating centers that different metal ions can bind to. The cross-linked copolymers are zwitterionic or anionic, and can be in either an acidic form or a basic form. A method for removing metal ions from an aqueous sample with these cross-linked copolymers is also described.
    Type: Application
    Filed: September 30, 2016
    Publication date: April 27, 2017
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Zakariyah Abdulkareem JAMIU, Tawfik Abdo SALEH, Shaikh Asrof ALI
  • Patent number: 9617388
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Grant
    Filed: September 30, 2016
    Date of Patent: April 11, 2017
    Assignees: King Fahd University of Petroleum and Minerals, King Abdulaziz City for Science and Technology
    Inventors: Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu
  • Patent number: 9580521
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Grant
    Filed: September 30, 2016
    Date of Patent: February 28, 2017
    Assignees: King Fahd University of Petroleum and Minerals, King Abdulaziz City for Science and Technology
    Inventors: Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu
  • Publication number: 20170044277
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Application
    Filed: September 30, 2016
    Publication date: February 16, 2017
    Applicants: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS, KING ABDULAZIZ CITY FOR SCIENCE AND TECHNOLOGY
    Inventors: SHAIKH ASROF ALI, SHAMSUDDEEN ABDULLAHI HALADU
  • Patent number: 9556301
    Abstract: Cyclopolymers and N,N-diallyl methionine-based monomers or salts, solvates, tautomers or stereoisomers as corrosion inhibitors. A process for producing the cyclopolymers by Butler cyclopolymerization of the monomers in the presence of sulfur dioxide. In addition, a method for determining a percent inhibition efficiency of metal corrosion for the cyclopolymers and monomers as well as applications and methods for the cyclopolymers as coatings, compositions, and formulations for preventing metal corrosion.
    Type: Grant
    Filed: December 2, 2015
    Date of Patent: January 31, 2017
    Assignee: King Fahd Universoty of Petroleum and Minerals
    Inventors: Mohammad Abu Jafar Mazumder, Hasan Ali Al-Muallem, Shaikh Asrof Ali, Mohamad Khalid Estaitie
  • Publication number: 20170015788
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Application
    Filed: September 30, 2016
    Publication date: January 19, 2017
    Applicants: King Fahd University of Petroleum and Minerals, King Abdulaziz City for Science and Technology
    Inventors: Shaikh Asrof ALI, Shamsuddeen Abdullahi HALADU
  • Publication number: 20160347988
    Abstract: An aminoalkyl imidazolines of the formula: having p-octyloxy-, p-dodecyloxy-, or p-octadecyloxy-phenyl pendants as hydrophobes, for use to mitigate mild steel corrosion. An electron-rich aromatic ring, in conjugation with an amidine motif, imparts increasing corrosion inhibition efficiencies with an increasing hydrophobe chain length. X-ray photoelectron spectroscopy confirms the formation of an aminoalkyl imidazoline film on a metal surface prior to reaching a critical molar concentration.
    Type: Application
    Filed: June 1, 2015
    Publication date: December 1, 2016
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Mohammad Abu JAFAR MAZUMDER, Shaikh Asrof ALI, Hasan Ali AL-MUALLEM
  • Patent number: 9481765
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) (i.e. poly(Z-alt-SO2). Phosophonate ester hydroloysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Grant
    Filed: December 30, 2013
    Date of Patent: November 1, 2016
    Assignees: King Fahd University of Petroleum and Minerals, KIng Abdulaziz City for Science and Technology
    Inventors: Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu
  • Patent number: 9480979
    Abstract: Cross-linked cyclocopolymers made up of one or more quaternary ammonium salts and sulfur dioxide as monomers. One of the quaternary ammonium salts is also an aspartic acid derivative. The cross-linked copolymers include a repeating unit with multiple chelating centers that different metal ions can bind to. The cross-linked copolymers are zwitterionic or anionic, and can be in either an acidic form or a basic form. A method for removing metal ions from an aqueous sample with these cross-linked copolymers is also described.
    Type: Grant
    Filed: October 21, 2015
    Date of Patent: November 1, 2016
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Zakariyah Abdulkareem Jamiu, Tawfik Abdo Saleh, Shaikh Asrof Ali
  • Patent number: 9481590
    Abstract: The poly(zwitterion-alt-sulfur dioxide) copolymer includes a structural unit having the structural formula: wherein “n” is the number of repeating units. The copolymer is made by cocyclopolymerizing 3-(N,N-diallyl,N-carboethoxymethylammonio)propanesulfonate with sulfur dioxide to obtain an intermediate polyzwitterion (PZ) copolymer, which is hydrolyzed to form the copolymer. The copolymer may be converted to a poly(electrolyte-zwitterion) by treatment with a base, such as sodium hydroxide.
    Type: Grant
    Filed: November 26, 2013
    Date of Patent: November 1, 2016
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu
  • Publication number: 20160264690
    Abstract: Cross-linked tetrapolymers made up of different diallyl zwitterionic diallyl quaternary ammonium salt monomers, with one of them functioning as a cross-linking monomer. The cross-linked terpolymers include a repeating unit with multiple ligand centers that different metal ions can bind to. The cross-linked tetrapolymers are cationic, zwitterionic and anionic, and can be in either an acidic form or a basic form. A method of removing metal ions from an aqueous solution with these cross-linked tetrapolymers is also described.
    Type: Application
    Filed: March 11, 2015
    Publication date: September 15, 2016
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Shamsuddeen Abdullahi Haladu, Shaikh Asrof Ali, Tawfik Abdo Saleh
  • Patent number: 9359458
    Abstract: The polyzwitterionic acid antiscalant is an antiscalant for use in desalination plants and the like for inhibiting CaSO4 and SO42? scale precipitation. The polyzwitterionic acid (PZA) antiscalant has the following structural formula: In order to make the PZA antiscalant, N-carboethoxymethyl-3-(N,N-diallylamino)propanesulfonate, a zwitterionic monomer, is cyclopolymerized in aqueous solution using tert-butyl hydroperoxide (TBHP) to make an intermediate polyzwitterion (PZ). Acidic hydrolysis of the ester groups of the PZ is performed to produce the PZA antiscalant. Evaluation of the antiscalant properties of the PZA antiscalant using concentrated brines revealed that the PZA antiscalant, at a concentration of 10 ppm, is very effective in inhibiting the formation of calcium sulfate scale, particularly in reverse osmosis plants.
    Type: Grant
    Filed: December 26, 2013
    Date of Patent: June 7, 2016
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Shamsuddeen Abdullahi Haladu, Shaikh Asrof Ali
  • Publication number: 20160115598
    Abstract: Compounds and methods of inhibiting corrosion of mild steel. Compounds disclosed herein are cationic and contain multiple functional motifs such as propargyl, cinnamaldehyde, isoxazolidine and hydrophobe. These compounds are found to be effective in inhibiting mild steel corrosion in HCl, H2SO4, NaCl and CO2-saturated environments.
    Type: Application
    Filed: October 28, 2014
    Publication date: April 28, 2016
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Shaikh Asrof ALI, Mohammad Abu Jafar Mazumder, Hasan Ali Al-Muallem
  • Patent number: 9309336
    Abstract: A zwitterionic monomer and corresponding cyclopolymerized polyzwitterion (±) (PZ) containing, on each repeating unit, both phosphonate and sulfonate functionalities. Phosphonate ester hydrolysis in PZ gave a pH-responsive polyzwitterionic acid (±) (PZA). The PZA under pH-induced transformation was converted into polyzwitterion/anion (±?) (PZAN) and polyzwitterion/dianion (±=) (PZDAN).
    Type: Grant
    Filed: November 27, 2013
    Date of Patent: April 12, 2016
    Assignees: King Fahd University Of Petroleum and Minerals, King Abdulaziz City for Science and Technology
    Inventors: Shaikh Asrof Ali, Shamsuddeen Abdullahi Haladu