Abstract: The invention discloses an improved process for producing an intermediate to produce large quantity of 2-(Phenyl methyl thio)-3-pyridine carboxylic acid. The process comprises reacting 2-chloro-3-cyanopyridine with benzyl mercaptan in presence of a base and an aprotic solvent. The resulting intermediate 2-(phenyl methyl thio)-3-cyanopyridine is hydrolyzed in presence of a base in an autoclave and isolated under acidic condition to get the desired product.

Abstract: The topology of a digital subscriber line loop can play an important role in provisioning service. For example, knowledge of certain topological features in a loop can enable telecommunications companies to make better decisions about the kinds of services that can be provisioned on that loop. Additionally, knowledge of those topological features can also assist field engineers in troubleshooting problems in the field. A topology recognition engine can provide key topological features such as the loop length, presence of single and multiple bridge taps and the length of single bridge taps on a loop.

Abstract: Disclosed herein is a process for recovery of pyridine and/or its derivatives from their aqueous mass and/or manufacturing reaction mass by liquid-liquid extraction employing an environmentally non-hazardous organic solvent. The process further comprising effective recovering and recycle of solvents from the aqueous phase and the other waste obtained during the process.

Abstract: A telecommunication receiver provided according to the present invention is implemented to receive a first signal containing information and noise on a first set of sensors and a second signal containing only noise on a second set of sensors. Receiver then decodes the information using first signal and second signal. In one embodiment, a bonded DSL receiver with k signals sensors is implemented with additional s number of noise only sensors to receive only noise. Accordingly, joint demodulation is performed using signals received on k signals sensors and s noise only sensors. The noise sensor is implemented in common mode.

Abstract: Methods, compositions, and kits for coloring hair and maintaining the color between oxidative dyeing procedures.

Abstract: The invention discloses an improved process for producing an intermediate to produce large quantity of 2-(Phenyl methyl thio)-3-pyridine carboxylic acid. The process comprises reacting 2-chloro-3-cyanopyridine with benzyl mercaptan in presence of a base and an aprotic solvent. The resulting intermediate 2-(phenyl methyl thio)-3-cyanopyridine is hydrolyzed in presence of a base in an autoclave and isolated under acidic condition to get the desired product.

Abstract: An improved process for producing 4-dimethyl amino pyridine is provided. The process comprises quaternizing pyridine with a suitable quaternizing agent in the presence of organic solvent, isolating the resulting salt and aminating the salt, N-[4-pyridyl] pyridinium chloride hydrochloride, with N,N-dimethyl formamide. The resultant reaction mass is hydrolysed in the presence of a base, extracted with an aromatic solvent and distilled under vacuum to produce 4-dimethyl amino pyridine.

Abstract: Methods, compositions, and kits for coloring hair and maintaining the color between oxidative dyeing procedures.

Abstract: An improved process for producing 4-dimethyl amino pyridine is provided. The process comprises quaternizing pyridine with a suitable quaternizing agent in the presence of organic solvent, isolating the resulting salt and aminating the salt, N-[4-pyridyl] pyridinium chloride hydrochloride, with N,N-dimethyl formamide. The resultant reaction mass is hydrolysed in the presence of a base, extracted with an aromatic solvent and distilled under vacuum to produce 4-dimethyl amino pyridine.

Abstract: The present invention relates to an improved and industrially advantageous process for the preparation of N-(5-methylnicotinoyl)-4-hydroxypiperidine of Formula I, as shown in the accompanied drawings. This compound is a key intermediate for the synthesis of rupatadine, a potent dual antagonist of histamine and platelet-activating factor (PAF).

Abstract: An aqueous hair color composition for oxidatively coloring hair in twelve minutes or less, wherein said composition is prepared by combining a dye mixture and a developer mixture, said aqueous hair color composition comprising 0.01-2.0% (combined weight) of the total composition of primary intermediates and couplers, a free alkalinity concentration of 0.20-0.75 meq/gram, and a hydrogen peroxide concentration of 4-6% by weight of the total composition; and a hair coloring kit containing separate containers of an aqueous dye mixture and an aqueous developing mixture for use with said dye mixture.

Abstract: A single composition for simultaneous coloring and highlighting hair to provide hair fibers having variations in tonality and hue, comprising, 1-10% inorganic persulfate, 1-20% hydrogen peroxide, 0.001-20% of at least one primary intermediate and, optionally, at least one coupler for the formation of oxidation dyes; and 0.01-20% of one or more surfactants; as well as a one step method for simultaneously color and highlighting hair to provide hair fibers having variations in tonality and hue comprising, combining, immediately prior to use, a powder composition comprised of at least one alkali metal or alkaline earth metal persulfate, an aqueous developer composition comprised of hydrogen peroxide; and an aqueous based colorant composition comprised of at least one primary intermediate and, optionally, at least one coupler for the formation of oxidation dyes; and applying the mixture to the hair for a period of time sufficient to cause coloration and highlighting of the hair.

Abstract: An aqueous hair color composition for oxidatively coloring hair in twelve minutes or less, wherein said composition is prepared by combining a dye mixture and a developer mixture, said aqueous hair color composition comprising 0.01-2.0% (combined weight) of the total composition of primary intermediates and couplers, a free alkalinity concentration of 0.20-0.75 meq/gram, and a hydrogen peroxide concentration of 4-6% by weight of the total composition; and a hair coloring kit containing separate containers of an aqueous dye mixture and an aqueous developing mixture for use with said dye mixture.

Abstract: A method for preparing crystalline cefadroxil hemihydrate from cefadroxil dimethyl formamide solvate using a mixture of a lower alkanol and water.

Abstract: A single composition for simultaneous coloring and highlighting hair to provide hair fibers having variations in tonality and hue, comprising, 1-10% inorganic persulfate, 1-20% hydrogen peroxide, 0.001-20% of at least one primary intermediate and, optionally, at least one coupler for the formation of oxidation dyes; and 0.01-20% of one or more surfactants; as well as a one step method for simultaneously color and highlighting hair to provide hair fibers having variations in tonality and hue comprising, combining, immediately prior to use, a powder composition comprised of at least one alkali metal or alkaline earth metal persulfate, an aqueous developer composition comprised of hydrogen peroxide; and an aqueous based colorant composition comprised of at least one primary intermediate and, optionally, at least one coupler for the formation of oxidation dyes; and applying the mixture to the hair for a period of time sufficient to cause coloration and highlighting of the hair.