Patents by Inventor Shigeru Ikai

Shigeru Ikai has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20140113985
    Abstract: To provide a process for producing a flexible polyurethane foam having a higher biomass degree than a conventional flexible polyurethane foam and excellent in foam physical properties and its appearance. A polymer-dispersed polyol obtained by polymerizing a vinyl monomer in the presence of the following polyol (a1) derived from a natural fat/oil and/or the following polyoxyalkylene polyol (a2) is used: Polyol (a1) derived from a natural fat/oil: a polyol derived from a natural fat/oil, which is obtained by providing a natural fat/oil with hydroxy groups by chemical reaction, and which has a hydroxy value of from 20 to 250 mgKOH/g and a molecular weight distribution of at least 1.
    Type: Application
    Filed: December 20, 2013
    Publication date: April 24, 2014
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Takayuki SASAKI, Yasuyuki Sasao, Naohiro Kumagai, Chitoshi Suzuki, Shigeru Ikai
  • Patent number: 8642668
    Abstract: To provide a process for producing a flexible polyurethane foam having a higher biomass degree than a conventional flexible polyurethane foam and excellent in foam physical properties and its appearance. A polymer-dispersed polyol obtained by polymerizing a vinyl monomer in the presence of the following polyol (a1) derived from a natural fat/oil and/or the following polyoxyalkylene polyol (a2) is used: Polyol (a1) derived from a natural fat/oil: a polyol derived from a natural fat/oil, which is obtained by providing a natural fat/oil with hydroxy groups by chemical reaction, and which has a hydroxy value of from 20 to 250 mgKOH/g and a molecular weight distribution of at least 1.
    Type: Grant
    Filed: December 22, 2009
    Date of Patent: February 4, 2014
    Assignee: Asahi Glass Company, Limited
    Inventors: Takayuki Sasaki, Yasuyuki Sasao, Naohiro Kumagai, Chitoshi Suzuki, Shigeru Ikai
  • Patent number: 8530602
    Abstract: A polyether polyol composition comprising: a polyether polyol, a phosphoric acid compound selected from the group consisting of at least one of orthophosphoric acid, polyphosphoric acid, polymetaphosphoric acid, and partial esters thereof in an amount raning from 0.5 to 100 ppm based on the polyether polyol metals derived from a composite metal cyanide complex catalyst in an amount ranging from 1 to 30 ppm based on the polyether polyol; a method for producing this polyether polyol composition; and methods of making polyurethane or isocyanate group-terminated prepolymers.
    Type: Grant
    Filed: April 30, 2009
    Date of Patent: September 10, 2013
    Assignee: Asahi Glass Company, Limited
    Inventors: Chitoshi Suzuki, Hiroki Fukuda, Shigeru Ikai
  • Patent number: 8354559
    Abstract: A polyether is synthesized by ring opening polymerization of an alkylene oxide with an initiator having at least one hydroxyl group, in the presence of a double metal cyanide complex catalyst, then a powder of an inorganic adsorbent containing at least 50 vol % of fine particles having a particle size of at most 26 ?m and further containing at least 90 vol % of fine particles having a particle size of at most 44 ?m, is added to the crude polyether, and a metal derived from the above double metal cyanide complex catalyst is adsorbed on the powder, followed by separating the powder from the crude polyether.
    Type: Grant
    Filed: March 2, 2009
    Date of Patent: January 15, 2013
    Assignee: Asahi Glass Company, Limited
    Inventors: Chitoshi Suzuki, Tomoyuki Suzuki, Shigeru Ikai
  • Patent number: 7786251
    Abstract: To provide a process for producing a polyester ether poly- or mono-ol having a narrow molecular weight distribution, which is obtained by copolymerizing an initiator having hydroxyl groups with a cyclic ester compound and an alkylene oxide. It is possible to produce a polyester ether poly- or mono-ol having a molecular distribution (Mw/Mn) of from 1.02 to 1.4 by copolymerizing a cyclic ester compound which carbon number is from 3 to 9 and an alkylene oxide which carbon number is from 2 to 20 with an initiator having from 1 to 12 hydroxyl groups and having a number average molecular weight (Mn) of from 18 to 20,000 in the presence of a double-metal cyanide complex catalyst is having tert-butyl alcohol as at least a part of an organic ligand.
    Type: Grant
    Filed: February 15, 2008
    Date of Patent: August 31, 2010
    Assignee: Asahi Glass Company, Limited
    Inventors: Shigeki Uemori, Shigeru Ikai, Chitoshi Suzuki
  • Publication number: 20100096768
    Abstract: To provide a process for producing a flexible polyurethane foam having a higher biomass degree than a conventional flexible polyurethane foam and excellent in foam physical properties and its appearance. A polymer-dispersed polyol obtained by polymerizing a vinyl monomer in the presence of the following polyol (a1) derived from a natural fat/oil and/or the following polyoxyalkylene polyol (a2) is used: Polyol (a1) derived from a natural fat/oil: a polyol derived from a natural fat/oil, which is obtained by providing a natural fat/oil with hydroxy groups by chemical reaction, and which has a hydroxy value of from 20 to 250 mgKOH/g and a molecular weight distribution of at least 1.
    Type: Application
    Filed: December 22, 2009
    Publication date: April 22, 2010
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Takayuki SASAKI, Yasuyuki Sasao, Naohiro Kumagai, Chitoshi Suzuki, Shigeru Ikai
  • Publication number: 20100041864
    Abstract: To provide a process for producing, simply and with high reproducibility, a double metal cyanide complex catalyst having an organic ligand, which has a high catalytic activity, a small particle size and a high particle size uniformity. A process for producing a double metal cyanide complex catalyst having an organic ligand, comprising (a) a step of contacting an aqueous metal halide compound solution and an aqueous transition metal cyanide compound solution in a laminar flow state to obtain a liquid containing a double metal cyanide complex, and (b) a step of mixing the liquid containing a double metal cyanide complex, and an organic ligand, to obtain a dispersion containing a double metal cyanide complex catalyst having an organic ligand.
    Type: Application
    Filed: October 8, 2009
    Publication date: February 18, 2010
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Yoshinobu KADOWAKI, Shigeru Ikai, Yasuyuki Sasao, Kazuhiko Yamada, Kenji Yamada
  • Publication number: 20090239964
    Abstract: To provide a process for producing a flexible polyurethane foam, which can suitably form a flexible polyurethane foam having a good cushioning characteristic by using a raw material derived from a natural fat/oil. The process comprises a step of reacting a polyoxyalkylene polyol (A) containing the first polyoxyalkylene polyol (A1) obtained by ring-opening polymerization of an alkylene oxide (c) with an initiator (b) in the presence of a polymerization catalyst (a), with a polyisocyanate compound (B) in the presence of a catalyst (C) and a blowing agent (D).
    Type: Application
    Filed: March 27, 2009
    Publication date: September 24, 2009
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Takayuki SASAKI, Naohiro Kumagai, Yasuyuki Sasao, Shigeru Ikai, Chitoshi Suzuki
  • Publication number: 20090215935
    Abstract: To provide a polyether polyol composition, whereby the reaction rate with a polyisocyanate can be controlled, and an isocyanate group-terminated prepolymer excellent particularly in storage stability can be given. A polyether polyol composition comprising a polyether polyol obtained by ring-opening polymerization of an alkylene oxide in the presence of a composite metal cyanide complex catalyst, and a phosphoric acid compound comprising a phosphoric acid selected from orthophosphoric acid, polyphosphoric acid and polymetaphosphoric acid, and/or a partial ester of such a phosphoric acid, characterized in that the polyether polyol composition contains metals derived from the composite metal cyanide complex catalyst in an amount of from 1 to 30 ppm based on the polyether polyol, and the above phosphoric acid compound in an amount of from 0.5 to 100 ppm based on the polyether polyol.
    Type: Application
    Filed: April 30, 2009
    Publication date: August 27, 2009
    Applicant: Asahi Glass Company, Limited
    Inventors: Chitoshi SUZUKI, Hiroki FUKUDA, Shigeru IKAI
  • Publication number: 20090203875
    Abstract: To provide a purification process which makes it possible to reduce the amount of an inorganic adsorbent to be used, shorten the time for separating a polyether and the inorganic adsorbent by filtration, and further reduce the amount of a metal derived from a double metal cyanide complex catalyst in a purified polyether thereby obtained. A polyether is synthesized by ring opening polymerization of an alkylene oxide with an initiator having at least one hydroxyl group, in the presence of a double metal cyanide complex catalyst, then a powder of an inorganic adsorbent containing at least 50 vol % of fine particles having a particle size of at most 26 ?m is and further containing at least 90 vol % of fine particles having a particle size of at most 44 ?m, is added to the above polyether, and a metal derived from the above double metal cyanide complex catalyst is adsorbed on the above powder, followed by separating the above powder from the above polyether.
    Type: Application
    Filed: March 2, 2009
    Publication date: August 13, 2009
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Chitoshi Suzuki, Tomoyuki Suzuki, Shigeru Ikai
  • Patent number: 7553921
    Abstract: A polyether polyol composition, the reactivity of which with a polyisocyanate can be controlled, to thereby obtain an isocyanate group-terminated prepolymer having excellent storage stability. A polyether polyol composition comprising a polyether polyol obtained by a ring-opening polymerization of an alkylene oxide in the presence of a composite metal cyanide complex catalyst, and a phosphoric acid compound comprising a phosphoric acid selected from orthophosphoric acid, polyphosphoric acid and polymetaphosphoric acid, and/ or a partial ester of such a phosphoric acid, wherein the polyether polyol composition contains metals derived from the composite metal cyanide complex catalyst in an amount of from 1 to 30 ppm based on the polyether polyol, and the above phosphoric acid compound in an amount of from 0.5 to 100 ppm based on the polyether polyol.
    Type: Grant
    Filed: July 26, 2005
    Date of Patent: June 30, 2009
    Assignee: Asahi Glass Company, Limited
    Inventors: Chitoshi Suzuki, Hiroki Fukuda, Shigeru Ikai
  • Publication number: 20080146775
    Abstract: To provide a process for producing a polyester ether poly- or mono-ol having a narrow molecular weight distribution, which is obtained by copolymerizing an initiator having hydroxyl groups with a cyclic ester compound and an alkylene oxide. It is possible to produce a polyester ether poly- or mono-ol having a molecular distribution (Mw/Mn) of from 1.02 to 1.4 by copolymerizing a cyclic ester compound which carbon number is from 3 to 9 and an alkylene oxide which carbon number is from 2 to 20 with an initiator having from 1 to 12 hydroxyl groups and having a number average molecular weight (Mn) of from 18 to 20,000 in the presence of a double-metal cyanide complex catalyst is having tert-butyl alcohol as at least a part of an organic ligand.
    Type: Application
    Filed: February 15, 2008
    Publication date: June 19, 2008
    Applicant: Asahi Glass Company, Limited
    Inventors: Shigeki UEMORI, Shigeru Ikai, Chitoshi Suzuki
  • Patent number: 7169956
    Abstract: Provided is a double metal cyanide complex catalyst with a high activity which is readily produced on an industrial scale. The double metal cyanide complex catalyst is of a fine particle form and contains t-butyl alcohol or, t-butyl alcohol and another organic compound as an organic ligand. The catalyst of the fine particle form has a volume-average particle size in a range of from 3 to 20 ?m, based on measurement by a light scattering method for measuring fine particles having particle sizes of at least 0.15 ?m. A particle content of the catalyst in a particle size range of at least 0.15 ?m and at most 1 ?m is less than 5% by volume, and a particle content of the catalyst over a particles size of 1 ?m is in a range of more than 95% and at most 100% by volume.
    Type: Grant
    Filed: August 26, 2005
    Date of Patent: January 30, 2007
    Assignee: Asahi Glass Company, Limited
    Inventors: Chitoshi Suzuki, Hiroki Fukuda, Yoshinori Toyota, Shigeru Ikai, Hideo Sakurai
  • Patent number: 7012164
    Abstract: A method for precisely producing a polyether having a relatively high molecular weight by means of a double metal cyanide complex catalyst is provided. A method for continuously producing a polyether, which comprises ring opening addition polymerization of an alkylene oxide in the presence of a double metal cyanide complex catalyst, wherein substantially no vapor phase part is present in a reactor.
    Type: Grant
    Filed: July 21, 2004
    Date of Patent: March 14, 2006
    Assignee: Asahi Glass Company, Limited
    Inventors: Kazuhiko Yamada, Nobuyuki Kasahara, Yoshinori Toyota, Chitoshi Suzuki, Shigeru Ikai, Hiroshi Hatano
  • Publication number: 20060004233
    Abstract: Provided is a double metal cyanide complex catalyst with a high activity which is readily produced on an industrial scale. The double metal cyanide complex catalyst is of a fine particle form and contains t-butyl alcohol or, t-butyl alcohol and another organic compound as an organic ligand. The catalyst of the fine particle form has a volume-average particle size in a range of from 3 to 20 ?m, based on measurement by a light scattering method for measuring fine particles having particle sizes of at least 0.15 ?m. A particle content of the catalyst in a particle size range of at least 0.15 ?m and at most 1 ?m is less than 5% by volume, and a particle content of the catalyst over a particles size of 1 ?m is in a range of more than 95% and at most 100% by volume.
    Type: Application
    Filed: August 26, 2005
    Publication date: January 5, 2006
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Chitoshi Suzuki, Hiroki Fukuda, Yoshinori Toyota, Shigeru Ikai, Hideo Sakurai
  • Publication number: 20050267279
    Abstract: To provide a polyether polyol composition, whereby the reaction rate with a polyisocyanate can be controlled, and an isocyanate group-terminated prepolymer excellent particularly in storage stability can be given. A polyether polyol composition comprising a polyether polyol obtained by ring-opening polymerization of an alkylene oxide in the presence of a composite metal cyanide complex catalyst, and a phosphoric acid compound comprising a phosphoric acid selected from orthophosphoric acid, polyphosphoric acid and polymetaphosphoric acid, and/or a partial ester of such a phosphoric acid, characterized in that the polyether polyol composition contains metals derived from the composite metal cyanide complex catalyst in an amount of from 1 to 30 ppm based on the polyether polyol, and the above phosphoric acid compound in an amount of from 0.5 to 100 ppm based on the polyether polyol.
    Type: Application
    Filed: July 26, 2005
    Publication date: December 1, 2005
    Applicant: Asahi Glass Company, Limited
    Inventors: Chitoshi Suzuki, Hiroki Fukuda, Shigeru Ikai
  • Publication number: 20040260056
    Abstract: A method for precisely producing a polyether having a relatively high molecular weight by means of a double metal cyanide complex catalyst is provided. A method for continuously producing a polyether, which comprises ring opening addition polymerization of an alkylene oxide in the presence of a double metal cyanide complex catalyst, wherein substantially no vapor phase part is present in a reactor.
    Type: Application
    Filed: July 21, 2004
    Publication date: December 23, 2004
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventors: Kazuhiko Yamada, Nobuyuki Kasahara, Yoshinori Toyota, Chitoshi Suzuki, Shigeru Ikai, Hiroshi Hatano
  • Patent number: 6627576
    Abstract: A process for producing a double metal cyanide complex catalyst for ring opening polymerization of alkylene oxide, which comprises subjecting a substantially crystalline double metal cyanide compound to a contact treatment by heating at from 45 to 125° C. with an aqueous solution containing an organic ligand and a metal salt, and then separating the resulting solid from the obtained slurry.
    Type: Grant
    Filed: August 28, 2002
    Date of Patent: September 30, 2003
    Assignee: Asahi Glass Company, Limited
    Inventors: Kayoko Sugiyama, Shigeru Ikai
  • Publication number: 20030100444
    Abstract: A process for producing a double metal cyanide complex catalyst for ring opening polymerization of alkylene oxide, which comprises subjecting a substantially crystalline double metal cyanide compound to a contact treatment by heating at from 45 to 125° C. with an aqueous solution containing an organic ligand and a metal salt, and then separating the resulting solid from the obtained slurry.
    Type: Application
    Filed: August 28, 2002
    Publication date: May 29, 2003
    Applicant: Asahi Glass Company, Limited
    Inventors: Kayoko Sugiyama, Shigeru Ikai
  • Patent number: 6376628
    Abstract: A method for preparing an &agr;-olefin polymer comprising the step of polymerizing or copolymerizing an &agr;-olefin in the presence of a catalyst containing a solid catalyst constituent (A) which contains magnesium, titanium, a halogen element and an electron donor, an organoaluminum compound constituent (B), an organosilicon compound constituent (C) represented by the following general formula (1); and an organosilicon compound constituent (D) represented by the following general formulas (2) or (3) to prepare an &agr;-olefin polymer RnSi(OR)4−n  (1) wherein R is a hydrocarbon group having 1 to 8 carbon atoms, n is integer of 1 or 2; wherein R1 is a hydrocarbon group having 1 to 8 carbon atoms, R2 is a hydrocarbon group having 1 to 8 carbon atoms, a hydrocarbylamino group having 2 to 24 carbon atoms, or a hydrocarbylalkoxy group having 1 to 24 carbon atoms, R3N is a polycyclic amino group having 7 to 40 carbon atoms, wherein the carbon atoms and the nitrogen atom form a c
    Type: Grant
    Filed: May 19, 1999
    Date of Patent: April 23, 2002
    Assignee: Grand Polymer Co., Ltd.
    Inventors: Shigeru Ikai, Hiroyuki Ikeuchi, Yasuhisa Sakakibara, Hiroshi Satoh