Abstract: A method for producing high-purity nickel, which involves using a hydrochloric acid solution system to electro-deposit high-purity nickel, characterized in that, it includes the following steps sequentially: 3N-grade-grade electrolytic nickel was used as anode and the electro-deposition was carried out in a hydrochloric acid system, the solution obtained from the electro-deposition was extracted by a three-level countercurrent extraction using anion extraction solvents, and then back-extracted and degreased. After that, the solution was passed through the anion exchange resin to be further purified by ion exchange, and finally put into the electrolytic cell to deposit nickel.